A02_Statement_of_Work_Purchase_of_GCMS_Spectrophotometer_CBC_Redacted.pdf

Statement of Work Purchase of a Gas Chromatograph Mass Spectrometer

Detection System GC/MSD System

1. Requirement. The contractor shall provide timely delivery of Government requested material to the address provided below unless otherwise specified by the Government. The Government is procuring one (1) Gas Chromatograph Mass Spectrometer Detection System as specified below.

Line

Part

Number

Part Description

Total Quantity

1 G7077BA 5977B Inert Plus MSD Tubro EI Bundle w/Extractor EI Source and Data System (Software, PC and Monitor), and additional G1710FA Data License With the following configuration:

Ship-to Country : USA Add ChemStation DA w/ CS Fam MSD for 7890 GC Add Laser Printer Substitute Oil Free Diaphragm Pump Installation (44K) Familiarization at Installation (44L) 1 Year SW Update/Phone Assist (44W)

2 G3397B Ion Gauge Kit for 5977 MSD With the following configuration: Ship-to Country : USA Installation (44K)

3 G1035F Wiley 11th w/NIST 2017 MS Library includes combined Wiley and NIST Libraries on both NIST and must be applicable with the Agilent Technologies format plus NIST MS Search and AMDIS applications.

With the following configuration: Ship-to Country : USA Installation (44K)

4 G3440B 7890B Series GC Custom, includes LAN Interface, 7693 Interface .20-ramp oven programming, 6 heated zones, 2 analog out, keyboard and display pressure setpoints to 0.001 psi (0-99 psi).

With the following configuration:

Ship-to Country : USA Aux. pneumatics cntr (301-309) : 3 Channel EPC (301) Country of Origin : United States INERT Cap S/SL inlet with EPC-100psi INERT Cap S/SL inlet with EPC-100psi Mass Spectrometer Detector Interface Three channels of auxiliary EPC Factory plumbing For quick installation Oven exhaust deflector Purged Union, Backflush Ready 7890B with USA Country of Origin Installation (44K) Familiarization at Installation (44L)

5 G4513A 7693A Autoinjector Includes transfer turret, 16-sample turret, mounting post, parking post for GC. 10ul syringe, and solvent bottles.

With the following configuration: Ship-to Country : USA 7693A ALS with USA Country of Origin Installation (44K) Familiarization at Installation (44L)

6 G4514A 7693 Tray, 150 vial includes three removable 50-vial racks and GC mounting bracket.

With the following configuration:

Ship-to Country : USA 7693A Tray with USA Country of Origin Installation (44K) Familiarization at Installation (44L)

7 H5949A Supplemental Installation One Hour Labor for Chemical Analysis products.

Labor only; no travel included.

Requires installation - bundled, or as 44N or 44K.

8 H2149A Method and Application Consulting On-site consulting for a maximum of 4 participants. Certificates and manuals not included.

With the following configuration: Ship-to Country : USA Three Day On-site (Includes Travel)

a. The items listed above shall be received approximately 50 days after award or sooner.

2. Government Furnished Property or Assistance. Not applicable. No requirement for Government Furnished Property.

3. DELIVERY/LOGISTICS.

3.1 The contractor shall deliver the data/supplies/services approximately 25 days after award to:

U.S. Army, CCDC 8222 Blackhawk Road

BLDG E5179

Gunpowder, MD 21010

3.2 Inspection and Acceptance of the items will be conducted at destination by authorized ECBC government personnel.

4. Safety Security Considerations. None

5. Security Considerations. None

6. Government Point of Contact.

U.S. Army - RDECOM

RDCB-DRC

Bldg E3400 8198 Blackhawk Road

APG, MD 21010-5424

Specifications for GC/MSD System Mass Spectrometer (MS)

Ion source temperature

A 350C limit. A higher source temperature would allow greater flexibility in analysis and can be kept clean longer.

Quadrupole temperature

Ability to heat the quadrupole MS to 106-200C.

Monolithic Quadrupole

Monolithic one pieces quadrupoles (not ion traps).

Mass filter protection

Some type of filter to aid in keeping the main quadrupole cleaner.

Detector Detector replacement that requires little to no tools.

Scan rate (electronic) and Write-to-disk rate

A scan rate is of up to 12,500 u/s and a disk write speed of up to 8,000 u/s.

SIM An ability to watch up to 60 ions in up to 100 groups.

Instrument control Having a local user interface that allows the PC to be located some distance away from the instrument. Also, software that can control two GC/MSs that are not next to each other and have to the ability to operate a LAN.

Maintenance access

A design to simplify maintenance and service.

Maintenance scheduling

Early maintenance feedback to alert multiple users that service is required.

Gas Chromatograph (GC) & Auto Sampler

EPC gas/flow control

Control all injection port and detector gases at a precision specification of pressure set-points of

0.001 PSI with typical control of +/- 0.001 – 99.999 PSI

Safety shut-down Safety features that could potentially show column breakage, leaks in the injection port or the detector or for that matter anywhere along the flow path within the instrument.

Automatic injector Dual tower injection ports that allow for dual injections when dual towers are installed.

Autosampler tray A sample tray of at least 100 samples preferably more if possible.

Autosampler bar code reader – optional and added as upgrade later it needed.

A bar code reader as part of the GC AutoSampler so samples could be tracked all through the lab and make the bar code label number part of the GCMS report.

Liner replacement A standard twist top inlet cover so inlet maintenance is tool free.

Retention time locking

Retention Time Locking software for quicker column changes and sample identification.

Data System Simultaneous MS and GC

Software capable of collecting GC signals from the std GC detectors (if installed) as well as the MS signal within one software package. Also the potential to control/collect data from 2 GCMS systems from a single computer.

SIM/scan The ability to collect SIM and scan data together during an entire run.

Application auto-tune

Auto-tune protocols for DFTPP and BFB.

Quantitation setup A target compound list can be set up by injecting a standard and allowing the software to locate the compounds and suggest the ions to use for identification.

Application reports The ability to optimize reports suited for individual customer’s needs.

File import/export The ability to accept properly formatted sample lists from a LIMS or other computer to build a sequence list. Also to export files with user-selected fields.

Customization Allows for extensive software modification and automation.

Spectral libraries Ability to use the latest NIST or Wiley sample libraries. We need the Wiley database library included.

Spectral and RTL databases

Libraries that include both spectral and retention time data.

21CFR11

Compliance Qualification

Ability to meet this specification.

Previous data files transportable

Backwards compatible with our older Agilent systems would be a plus.

Supplies Majority of the existing supplies already stocked in our lab would be usable saving large amounts of funding for research.