NIR_Specifications Document.pdf

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Near-infrared Spectrophotometer with calibrations
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1232SA26Q1289
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This is a Specifications Document for a near-infrared spectrophotometer with calibrations for oat quality analysis. The instrument must quantitatively measure six oat quality traits (protein, moisture, oil/fat, starch, beta-glucan, and total digestible fiber) using vendor-supplied calibration models, with capability to analyze at least one of four sample types: whole oats, oat groats, oat flour, or oat flakes. The spectrophotometer must operate in the 900–1700 nm wavelength range using reflectance measurement mode, with a benchtop footprint of approximately 20 inches width by 24 inches depth, and complete sample analysis in 30 seconds or less.

Key required features include magnetically positioned and 360-degree rotating sample dishes, very low operator-dependent measurement variation, operation by non-scientifically trained personnel, multiple reusable sample presentation formats accommodating 1.5–180 grams, non-destructive sample analysis, minimum 10-year instrument lifespan with regular maintenance, ability to export spectra data in non-vendor-specific formats, unrestricted sharing of in-lab-developed calibrations with other researchers, automatic outlier detection, automated wavelength standardization, automatic lamp and spectrophotometer stability monitoring, user-replaceable lamp, vibration resistance, at least three USB connections, and vendor-provided software for in-lab calibration development as a one-time purchase rather than subscription. Additional requirements include barcode reader compatibility for future implementation, vendor technician installation and training, 1–2 years of unlimited support for instrument use and calibration development, and vendor focus on the agricultural sector. Preferred features include reflectance-based diode array detectors without moving parts, sample dishes requiring no cleaning, internal NIST-standard detector calibration, and continuous wavelength data acquisition.

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Specifications Document Product Description: Near-infrared Spectrophotometer with calibrations for oat quality analysis

1) Can quantitatively measure the following oat quality traits using vendor supplied calibration models:

a. Protein

b. Moisture

c. Oil or fat

d. Starch

e. Beta-glucan

f. Total digestible fiber

2) Can quantitatively measure the above sample traits using vendor supplied calibration models in at least 1 of the following sample types:

a. Whole oats

b. Oat groats (hulled oats)

c. Oat flour

d. Oat flakes

3) Wavelength range approximately 900 – 1700 nm

4) Measurement mode: reflectance

5) Benchtop footprint, approximately 20 inches (width) x 24 inches (depth)

6) Analysis time per sample 30 seconds or less. Shorter analysis times strongly preferred

7) Samples presented in magnetically positioned and 360 degree rotating sample dish

8) Very low measurement variation due to operator differences

9) Can be operated effectively by person without scientific training

10) Multiple sample presentation dish/cup formats available for sample quantities ranging from approximately 1.5 g – 180 g. Sample dishes/cups must be reusable

11) Non-destructive analysis of samples

12) Instrument expected to last at least 10 years when used in a lab environment and when regular maintenance is performed

13) Collected spectra data files can be exported in non-vendor specific file formats and can be analyzed outside of vendor software if desired

14) Calibrations developed in-lab (not those provided by vendor) may be shared without vendor restrictions with other researchers

15) Automatic outlier detection implemented for each measurement

16) Automated wavelength standardization

17) Automatic monitoring of lamp and spectrophotometer stability

18) Lamp is changeable/replaceable by user

19) Vibration resistant spectrophotometer

20) At least 3 USB connections for computer accessories (mouse and keyboard) and data transfer off instrument

21) Vendor software available to allow in-lab calibration development. Software may not be subscription based but rather must be a one-time cost to purchase software. Software will not be purchase now, but compatible and capable software must be available from vendor for possible future purchase

22) Sample data file tagging by barcode reader possible. Not for purchase now, but this must be possible for potential future purchase/set up

23) Instrument installation and training by Vendor technicians and product specialists

24) 1-2 years of unlimited support for using instrument, refining calibrations purchased from vendor, and technical assistance in developing new calibrations with user supplied spectra and reference parameter measurements

25) Vendor focused on instruments and technical support for agricultural sector including researchers, producers, and buyers

Preferred Technical Features:

1) Reflectance-based diode array detector without moving parts for greater stability of detector and stability of measurements across lab environment (temperature and humidity) and time (months, years)

2) Sample dishes that do not require cleaning

3) Internal, self-adjusting/calibration of detector to NIST standard

4) Continuous data acquisition at all wavelengths

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