Analytics_Tank_152-19.pdf

November 08, 2024

GES

Michael Rohrer

Dear Michael Rohrer:

RE: Blending Facility

Order No.: 24110446

FAX:

TEL: (252) 447-1700

1 Cherry Point Traiker Bldg4376T

MCAS Cherry Point, NC 28533

Summit Environmental Technologies, Inc.

3310 Win St.

Cuyahoga Falls, Ohio 44223

Website: http://www.settek.com

TEL: (330) 253-8211 FAX: (330) 253-4489

Jennifer Woolf

Project Manager

3310 Win St.

Cuyahoga Falls, Ohio 44223

There were no problems with the analytical events associated with this report unless noted in the Case Narrative.

Quality control data is within laboratory defined or method specified acceptance limits except where noted.

If you have any questions regarding these tests results, please feel free to call the laboratory.

Sincerely, Summit Environmental Technologies, Inc. received 1 sample(s) on 11/7/2024 for the analyses presented in the following report.

Arkansas 88-0735, California 2943, Colorado, Connecticut PH-0108, Florida NELAC E87688, Idaho OH00923, Illinois 200061, Indiana C-OH-13, ISO/IEC 17025:2017 119125 L22-544, Kansas E-10347, Kentucky (Underground Storage Tank) 3, Kentucky 90146, Maryland 339, Michigan 9988, Minnesota 1780279, Nevada OH009232020-1, New Hampshire 2996, New Jersey OH006, New York 11777, North Carolina 39705 and 631, North Dakota

R-201, Ohio DW, Ohio VAP CL0052, Oklahoma 2019-155, Oregon OH200001, Pennsylvania 68-01335, Rhode Island LA000317, South Carolina

92016001, Texas T104704466-19-16, Utah OH009232020-12, Virginia VELAP 10381, West Virginia 9957C

Project: Blending Facility

CLIENT: GES

11/8/2024

Case Narrative

24110446

Date:

WO#:

Summit Environmental Technologies, Inc.

3310 Win St.

Cuyahoga Falls, Ohio 44223

Website: http://www.settek.com

TEL: (330) 253-8211 FAX: (330) 253-4489

WorkOrder Narrative:

24110446: This report in its entirety consists of the following documents: Cover Letter, Case Narrative, Analytical Results, QC Summary Report, Applicable Accreditation Information, Chain-of-Custody, Cooler Receipt Form, and other applicable forms as necessary. All documents contain the Summit

Environmental Technologies, Inc., Work Order Number assigned to this report.

Summit Environmental Technologies, Inc., holds the accreditations/certifications listed at the bottom of the cover letter that may or may not pertain to this report. Please refer to the "Accreditation Program

Analytes Report" for accredited analytes list.

The information contained in this analytical report is the sole property of Summit Environmental

Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of

Summit Environmental Technologies, Inc. or the customer for which this report was issued. The results contained in this report are only representative of the samples received. Conditions can vary at different times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible for use or interpretation of the data included herein.

All results for Solid Samples are reported on an "as received" or "wet weight" basis unless indicated as

"dry weight" using the "-dry" designation on the reporting units.

This report is believed to meet all of the requirements of the accrediting agency, where applicable. Any comments or problems with the analytical events associated with this report are noted below.

WorkOrder Comments:

Summit Environmental Technologies does not hold certification in the state of NC for several analyses requested.

Analytical Sequence Sample Notes:

24110446-001A PCB_OIL(8082): Cleanup was performed on sample extract by SW846 method 3665 in order to minimize matrix interferences.

Analytical Sequence QC Notes:

MB/LCS-241107B PCB_OIL(8082): Cleanup was performed on sample extract by SW846 method

3665 in order to minimize matrix interferences.

Original

11/8/2024

Case Narrative

24110446

Date:

WO#:

Summit Environmental Technologies, Inc.

3310 Win St.

Cuyahoga Falls, Ohio 44223

Website: http://www.settek.com

TEL: (330) 253-8211 FAX: (330) 253-4489

MB-241107B PCB_OIL(8082): Opening CCV exhibited high recoveries indicating potential high bias.

MB is ND for all reported aroclors.

11/8/2024

Qualifiers and Acronyms

24110446

Date:

WO#:

These commonly used Qualifiers and Acronyms may or may not be present in this report.

Summit Environmental Technologies, Inc.

3310 Win St.

Cuyahoga Falls, Ohio 44223

Website: http://www.settek.com

TEL: (330) 253-8211 FAX: (330) 253-4489

This list of Qualifiers and Acronyms reflects the most commonly utilized Qualifiers and Acronyms for reporting.

Please refer to the Analytical Notes in the Case Narrative for any Qualifiers or Acronyms that do not appear in this list or for additional information regarding the use of these Qualifiers on reported data.

Qualifiers

U The compound was analyzed for but was not detected above the MDL.

J The reported value is greater than the Method Detection Limit but less than the Reporting Limit.

H The hold time for sample preparation and/or analysis was exceeded. Not Clean Water Act compliant.

D The result is reported from a dilution.

E The result exceeded the linear range of the calibration or is estimated due to interference.

MC The result is below the Minimum Compound Limit.

* The result exceeds the Regulatory Limit or Maximum Contamination Limit.

m Manual integration was used to determine the area response.

d Manual integration in which peak was deleted

N The result is presumptive based on a Mass Spectral library search assuming a 1:1 response.

P The second column confirmation exceeded 25% difference.

C The result has been confirmed by GC/MS.

X The result was not confirmed when GC/MS Analysis was performed.

B The analyte was detected in the Method Blank at a concentration greater than the RL.

MB+ The analyte was detected in the Method Blank at a concentration greater than the MDL.

G The ICB or CCB contained reportable amounts of analyte.

QC-/+ The CCV recovery failed low (-) or high (+).

R/QDR The RPD was outside of accepted recovery limits.

QL-/+ The LCS or LCSD recovery failed low (-) or high (+).

QLR The LCS/LCSD RPD was outside of accepted recovery limits.

QM-/+ The MS or MSD recovery failed low (-) or high (+).

QMR The MS/MSD RPD was outside of accepted recovery limits.

QV-/+ The ICV recovery failed low (-) or high (+).

S The spike result was outside of accepted recovery limits.

W Samples were received outside temperature limits (0° – 6° C). Not Clean Water Act compliant.

Z Deviation; A deviation from the method was performed; Please refer to the Case Narrative for additional information

Acronyms

ND Not Detected RL Reporting Limit

QC Quality Control MDL Method Detection Limit

MB Method Blank LOD Level of Detection

LCS Laboratory Control Sample LOQ Level of Quantitation

LCSD Laboratory Control Sample Duplicate PQL Practical Quantitation Limit

QCS Quality Control Sample CRQL Contract Required Quantitation Limit

DUP Duplicate PL Permit Limit

MS Matrix Spike RegLvl Regulatory Limit

MSD Matrix Spike Duplicate MCL Maximum Contamination Limit

RPD Relative Percent Different MinCL Minimum Compound Limit

ICV Initial Calibration Verification RA Reanalysis

ICB Initial Calibration Blank RE Reextraction

CCV Continuing Calibration Verification TIC Tentatively Identified Compound

CCB Continuing Calibration Blank RT Retention Time

RLC Reporting Limit Check CF Calibration Factor

DF Dilution Factor RF Response Factor

Lab SampleID Client Sample ID Tag No Date ReceivedDate Collected

08-Nov-24

Workorder

Sample Summary

24110446WO#:

Matrix

Summit Environmental Technologies, Inc.

3310 Win St.

Cuyahoga Falls, Ohio 44223

Website: http://www.settek.com

TEL: (330) 253-8211 FAX: (330) 253-4489

24110446-001 152-19 11/5/2024 2:50:00 PM 11/7/2024 9:05:00 AM Oil

Sample ID Client Sample ID Collection Date Matrix Analysis Date

Client: GES

Project: Blending Facility

Test Name Prep DateLeachate Date

08-Nov-24

DATES REPORT

24110446WO#:

Summit Environmental Technologies, Inc.

3310 Win St.

Cuyahoga Falls, Ohio 44223

Website: http://www.settek.com

TEL: (330) 253-8211 FAX: (330) 253-4489

24110446-001A 152-19 11/5/2024 2:50:00 PM Oil Determination of °API (ASTM D-4052) 11/7/2024 1:35:51 PM

Flashpoint Determination (1010) 11/8/2024 3:38:39 PM

Halogens Analysis by X-Ray (9075) 11/8/2024 12:32:54 PM

Metals Analysis in Oil (6010) 11/7/2024 2:33:18 PM

PCB Analysis for Oils (8082) 11/7/2024 7:42:00 PM

Pecent Water in Oil by Distillation (D-95) 11/7/2024 2:24:57 PM

Percent Sulfur by X-Ray (D-4294) 11/8/2024 12:35:25 PM

Percentage of Ash in Petroleum Products (D-

482)

11/7/2024 5:01:22 PM

Client Sample ID: 152-19

Collection Date: 11/5/2024 2:50:00 PM

Matrix: OIL

CLIENT: GES

Lab ID: 24110446-001

11/8/2024

Analytical Report

24110446

Date Reported:

WO#:

(consolidated)

Analyses Result Qual Units Date AnalyzedDFRL

Summit Environmental Technologies, Inc.

3310 Win St.

Cuyahoga Falls, Ohio 44223

Website: http://www.settek.com

TEL: (330) 253-8211 FAX: (330) 253-4489

METALS ANALYSIS IN OIL (6010) SW6010 Analyst: OK

Arsenic(As) 11/7/2024 2:33:18 PM1.00 ppm 1< 1.00

Cadmium(Cd) 11/7/2024 2:33:18 PM0.100 ppm 10.158

Chromium(Cr) 11/7/2024 2:33:18 PM4.00 ppm 1< 4.00

Lead(Pb) 11/7/2024 2:33:18 PM1.00 ppm 13.67

DETERMINATION OF °API (ASTM D-4052) ASTM-D4052 Analyst: JA

API Gravity 11/7/2024 1:35:51 PM°API@60ºF 133.1

PERCENTAGE OF ASH IN PETROLEUM PRODUCTS (D-482) ASTM-D482 Analyst: TAH

Ash 11/7/2024 5:01:22 PM0.10 % 10.24

FLASHPOINT DETERMINATION (1010) SW1010 Analyst: TAH

Flash Point 11/8/2024 3:38:39 PM°F 1166

HALOGENS ANALYSIS BY X-RAY (9075) SW9075 Analyst: TAH

Chlorine, Total 11/8/2024 12:32:54 PM200 ppm 1<200

PECENT WATER IN OIL BY DISTILLATION (D-95) ASTM-D95 Analyst: JA

Water 11/7/2024 2:24:57 PM0.200 wt% 110.1

PERCENT SULFUR BY X-RAY (D-4294) ASTM-D4294 Analyst: TAH

% Sulfur 11/8/2024 12:35:25 PM0.1000 % 1< 0.1000

PCB ANALYSIS FOR OILS (8082) SW8082 Analyst: PJB

Aroclor 1016 11/7/2024 7:42:00 PM1.00 ppm 1< 1.00

Aroclor 1221 11/7/2024 7:42:00 PM1.00 ppm 1< 1.00

Qualifiers:

Original

E Value above quantitation range H Holding times for preparation or analysis exceeded

M Manual Integration used to determine area response ND Not Detected

PL Permit Limit R RPD outside accepted recovery limits

RL Reporting Detection Limit W Sample container temperature is out of limit as specified at testcode

Client Sample ID: 152-19

Collection Date: 11/5/2024 2:50:00 PM

Matrix: OIL

CLIENT: GES

Lab ID: 24110446-001

11/8/2024

Analytical Report

24110446

Date Reported:

WO#:

(consolidated)

Analyses Result Qual Units Date AnalyzedDFRL

Summit Environmental Technologies, Inc.

3310 Win St.

Cuyahoga Falls, Ohio 44223

Website: http://www.settek.com

TEL: (330) 253-8211 FAX: (330) 253-4489

PCB ANALYSIS FOR OILS (8082) SW8082 Analyst: PJB

Aroclor 1232 11/7/2024 7:42:00 PM1.00 ppm 1< 1.00

Aroclor 1242 11/7/2024 7:42:00 PM1.00 ppm 1< 1.00

Aroclor 1248 11/7/2024 7:42:00 PM1.00 ppm 1< 1.00

Aroclor 1254 11/7/2024 7:42:00 PM1.00 ppm 1< 1.00

Aroclor 1260 11/7/2024 7:42:00 PM1.00 ppm 1< 1.00

Total PCBs 11/7/2024 7:42:00 PM1.00 ppm 1< 1.00

Surr: TCMX 11/7/2024 7:42:00 PM10 - 168 %Rec 1104

Qualifiers:

Original

E Value above quantitation range H Holding times for preparation or analysis exceeded

M Manual Integration used to determine area response ND Not Detected

PL Permit Limit R RPD outside accepted recovery limits

RL Reporting Detection Limit W Sample container temperature is out of limit as specified at testcode

Program Name:

Matrix Status

Client: GES

Project: Blending Facility

Test Name Analyte

08-Nov-24

Accreditation Program

Analytes Report

24110446WO#:

NWState:

NC_WW_SCM

Summit Environmental Technologies, Inc.

3310 Win St.

Cuyahoga Falls, Ohio 44223

Website: http://www.settek.com

TEL: (330) 253-8211 FAX: (330) 253-4489

OilDetermination of °API (ASTM D-4052) NAPI Gravity

OilFlashpoint Determination (1010) NFlashpoint (200°F)

OilHalogens Analysis by X-Ray (9075) NChlorine, Total

OilMetals Analysis in Oil (6010) AArsenic

OilMetals Analysis in Oil (6010) ACadmium

OilMetals Analysis in Oil (6010) AChromium

OilMetals Analysis in Oil (6010) ALead

OilPCB Analysis for Oils (8082) AAroclor 1016

OilPCB Analysis for Oils (8082) AAroclor 1221

OilPCB Analysis for Oils (8082) AAroclor 1232

OilPCB Analysis for Oils (8082) AAroclor 1242

OilPCB Analysis for Oils (8082) AAroclor 1248

OilPCB Analysis for Oils (8082) AAroclor 1254

OilPCB Analysis for Oils (8082) AAroclor 1260

OilPCB Analysis for Oils (8082) ATotal PCBs

OilPecent Water in Oil by Distillation (D-95) NPercent Water

OilPercent Sulfur by X-Ray (D-4294) NSulfur

OilPercentage of Ash in Petroleum Products (D-482) NAsh

Original #1

AL UnavailableU AR AccreditedA AR Not AccreditedN

CA-NELAP AccreditedA CA-NELAP Not AccreditedN CA-NELAP UnavailableU

CO UnavailableU CT AccreditedA CT Not AccreditedN

FL-NELAP AccreditedA FL-NELAP Not AccreditedN HI-DW Not AccreditedN

HI-DW UnavailableU IA AccreditedA IA Not AccreditedN

BatchID: 241107B

08-Nov-24

QC SUMMARY REPORT

24110446WO#:

Summit Environmental Technologies, Inc.

3310 Win St.

Cuyahoga Falls, Ohio 44223

Website: http://www.settek.com

TEL: (330) 253-8211 FAX: (330) 253-4489

Sample ID: LCS-241107B

Batch ID: 241107B TestNo: SW8082 Analysis Date: 11/7/2024

Prep Date:

Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual

Units: ppm

PQL

Client ID: LCSW

RunNo: 196602

SeqNo: 5317525

LCSSampType: TestCode: PCB_OIL(808

Aroclor 1016 20.00 81.4 40.4 1301.00 016.3

Aroclor 1260 20.00 78.4 58.9 1301.00 015.7

Total PCBs 40.01 79.9 44.1 1301.00 032.0

Surr: TCMX 6.000 107 10 1686.39

Qualifiers:

Original

E Value above quantitation range H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response

ND Not Detected PL Permit Limit R RPD outside accepted recovery limits

RL Reporting Detection Limit S Spike Recovery outside accepted recovery limits W Sample container temperature is out of limit as specified at testcode

BatchID: 241107B

08-Nov-24

QC SUMMARY REPORT

24110446WO#:

Summit Environmental Technologies, Inc.

3310 Win St.

Cuyahoga Falls, Ohio 44223

Website: http://www.settek.com

TEL: (330) 253-8211 FAX: (330) 253-4489

Sample ID: 24110313-001AMS

Batch ID: 241107B TestNo: SW8082 Analysis Date: 11/7/2024

Prep Date:

Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual

Units: ppm

PQL

Client ID: BatchQC

RunNo: 196599

SeqNo: 5317494

MSSampType: TestCode: PCB_OIL(808

Aroclor 1016 20.00 60.6 55.8 130 QMR1.00 012.1

Aroclor 1260 20.00 79.0 67.4 1301.00 16.8532.6

Total PCBs 40.01 69.8 64.7 1301.00 16.8544.8

Surr: TCMX 6.000 96.4 10 1685.78

Sample ID: 24110313-001AMSD

Batch ID: 241107B TestNo: SW8082 Analysis Date: 11/7/2024

Prep Date:

Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual

Units: ppm

PQL

Client ID: BatchQC

RunNo: 196599

SeqNo: 5317495

MSDSampType: TestCode: PCB_OIL(808

Aroclor 1016 20.00 86.0 55.8 130 30 R1.00 0 12.13 34.617.2

Aroclor 1260 20.00 80.1 67.4 130 301.00 16.85 32.65 0.68132.9

Total PCBs 40.01 83.0 64.7 130 301.00 16.85 44.77 11.250.1

Surr: TCMX 6.000 96.2 10 168 05.77

Qualifiers:

Original

E Value above quantitation range H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response

ND Not Detected PL Permit Limit R RPD outside accepted recovery limits

RL Reporting Detection Limit S Spike Recovery outside accepted recovery limits W Sample container temperature is out of limit as specified at testcode

BatchID: 241107B

08-Nov-24

QC SUMMARY REPORT

24110446WO#:

Summit Environmental Technologies, Inc.

3310 Win St.

Cuyahoga Falls, Ohio 44223

Website: http://www.settek.com

TEL: (330) 253-8211 FAX: (330) 253-4489

Sample ID: MB-241107B

Batch ID: 241107B TestNo: SW8082 Analysis Date: 11/7/2024

Prep Date:

Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual

Units: ppm

PQL

Client ID: PBW

RunNo: 196598

SeqNo: 5317478

MBLKSampType: TestCode: PCB_OIL(808

Aroclor 1016 0 QC+1.00 0< 1.00

Aroclor 1221 01.00 0< 1.00

Aroclor 1232 01.00 0< 1.00

Aroclor 1242 01.00 0< 1.00

Aroclor 1248 01.00 0< 1.00

Aroclor 1254 01.00 0< 1.00

Aroclor 1260 0 QC+1.00 0< 1.00

Total PCBs 0 QC+1.00 0< 1.00

Surr: TCMX 6.000 227 10 168 S13.6

Qualifiers:

Original

E Value above quantitation range H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response

ND Not Detected PL Permit Limit R RPD outside accepted recovery limits

RL Reporting Detection Limit S Spike Recovery outside accepted recovery limits W Sample container temperature is out of limit as specified at testcode

BatchID: R196566

08-Nov-24

QC SUMMARY REPORT

24110446WO#:

Summit Environmental Technologies, Inc.

3310 Win St.

Cuyahoga Falls, Ohio 44223

Website: http://www.settek.com

TEL: (330) 253-8211 FAX: (330) 253-4489

Sample ID: LCS-R196566

Batch ID: R196566 TestNo: ASTM-D4052 Analysis Date: 11/7/2024

Prep Date:

Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual

Units: °API@60ºF

PQL

Client ID: LCSW

RunNo: 196566

SeqNo: 5316822

LCSSampType: TestCode: API_Oil(D405

API Gravity 9.600 101 70 13009.70

Qualifiers:

Original

E Value above quantitation range H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response

ND Not Detected PL Permit Limit R RPD outside accepted recovery limits

RL Reporting Detection Limit S Spike Recovery outside accepted recovery limits W Sample container temperature is out of limit as specified at testcode

BatchID: R196579

08-Nov-24

QC SUMMARY REPORT

24110446WO#:

Summit Environmental Technologies, Inc.

3310 Win St.

Cuyahoga Falls, Ohio 44223

Website: http://www.settek.com

TEL: (330) 253-8211 FAX: (330) 253-4489

Sample ID: RLC 0.1

Batch ID: R196579 TestNo: SW6010 Analysis Date: 11/7/2024

Prep Date:

Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual

Units: ppm

PQL

Client ID: BatchQC

RunNo: 196579

SeqNo: 5317095

RLCSampType: TestCode: Mtl-ICP_Oil(6

Arsenic(As) 0.1000 110 50 1501.00 0< 1.00

Cadmium(Cd) 0.1000 114 50 1500.100 00.114

Chromium(Cr) 0.1000 114 50 1504.00 0< 4.00

Lead(Pb) 0.1000 114 50 1501.00 0< 1.00

Sample ID: MB196579

Batch ID: R196579 TestNo: SW6010 Analysis Date: 11/7/2024

Prep Date:

Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual

Units: ppm

PQL

Client ID: PBW

RunNo: 196579

SeqNo: 5317096

MBLKSampType: TestCode: Mtl-ICP_Oil(6

Arsenic(As) 1.00< 1.00

Cadmium(Cd) 0.100< 0.100

Chromium(Cr) 4.00< 4.00

Lead(Pb) 1.00< 1.00

Sample ID: LCS

Batch ID: R196579 TestNo: SW6010 Analysis Date: 11/7/2024

Prep Date:

Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual

Units: ppm

PQL

Client ID: LCSW

RunNo: 196579

SeqNo: 5317097

LCSSampType: TestCode: Mtl-ICP_Oil(6

Arsenic(As) 5.000 94.5 80 1201.00 04.72

Cadmium(Cd) 5.000 95.1 80 1200.100 04.75

Qualifiers:

Original

E Value above quantitation range H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response

ND Not Detected PL Permit Limit R RPD outside accepted recovery limits

RL Reporting Detection Limit S Spike Recovery outside accepted recovery limits W Sample container temperature is out of limit as specified at testcode

BatchID: R196579

08-Nov-24

QC SUMMARY REPORT

24110446WO#:

Summit Environmental Technologies, Inc.

3310 Win St.

Cuyahoga Falls, Ohio 44223

Website: http://www.settek.com

TEL: (330) 253-8211 FAX: (330) 253-4489

Sample ID: LCS

Batch ID: R196579 TestNo: SW6010 Analysis Date: 11/7/2024

Prep Date:

Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual

Units: ppm

PQL

Client ID: LCSW

RunNo: 196579

SeqNo: 5317097

LCSSampType: TestCode: Mtl-ICP_Oil(6

Chromium(Cr) 5.000 94.2 80 1204.00 04.71

Lead(Pb) 5.000 94.4 80 1201.00 04.72

Sample ID: 24110321-001AMS

Batch ID: R196579 TestNo: SW6010 Analysis Date: 11/7/2024

Prep Date:

Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual

Units: ppm

PQL

Client ID: BatchQC

RunNo: 196579

SeqNo: 5317099

MSSampType: TestCode: Mtl-ICP_Oil(6

Arsenic(As) 20.00 87.4 70 1301.00 0.134017.6

Cadmium(Cd) 20.00 84.2 70 1300.100 0.750017.6

Chromium(Cr) 20.00 88.8 70 1304.00 0.518018.3

Lead(Pb) 20.00 86.8 70 1301.00 7.30024.6

Sample ID: 24110321-001AMSD

Batch ID: R196579 TestNo: SW6010 Analysis Date: 11/7/2024

Prep Date:

Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual

Units: ppm

PQL

Client ID: BatchQC

RunNo: 196579

SeqNo: 5317100

MSDSampType: TestCode: Mtl-ICP_Oil(6

Arsenic(As) 20.00 85.3 70 130 201.00 0.1340 17.61 2.4117.2

Cadmium(Cd) 20.00 82.0 70 130 200.100 0.7500 17.60 2.5317.2

Chromium(Cr) 20.00 85.6 70 130 204.00 0.5180 18.28 3.6217.6

Lead(Pb) 20.00 85.4 70 130 201.00 7.300 24.65 1.0624.4

Qualifiers:

Original

E Value above quantitation range H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response

ND Not Detected PL Permit Limit R RPD outside accepted recovery limits

RL Reporting Detection Limit S Spike Recovery outside accepted recovery limits W Sample container temperature is out of limit as specified at testcode

BatchID: R196579

08-Nov-24

QC SUMMARY REPORT

24110446WO#:

Summit Environmental Technologies, Inc.

3310 Win St.

Cuyahoga Falls, Ohio 44223

Website: http://www.settek.com

TEL: (330) 253-8211 FAX: (330) 253-4489

Sample ID: 24110321-001AMSD

Batch ID: R196579 TestNo: SW6010 Analysis Date: 11/7/2024

Prep Date:

Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual

Units: ppm

PQL

Client ID: BatchQC

RunNo: 196579

SeqNo: 5317100

MSDSampType: TestCode: Mtl-ICP_Oil(6

Qualifiers:

Original

E Value above quantitation range H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response

ND Not Detected PL Permit Limit R RPD outside accepted recovery limits

RL Reporting Detection Limit S Spike Recovery outside accepted recovery limits W Sample container temperature is out of limit as specified at testcode

BatchID: R196593

08-Nov-24

QC SUMMARY REPORT

24110446WO#:

Summit Environmental Technologies, Inc.

3310 Win St.

Cuyahoga Falls, Ohio 44223

Website: http://www.settek.com

TEL: (330) 253-8211 FAX: (330) 253-4489

Sample ID: MB-R196593

Batch ID: R196593 TestNo: ASTM-D482 Analysis Date: 11/7/2024

Prep Date:

Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual

Units: %

PQL

Client ID: PBW

RunNo: 196593

SeqNo: 5317419

MBLKSampType: TestCode: Ash_Oil(D482

Ash 0.10< 0.10

Qualifiers:

Original

E Value above quantitation range H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response

ND Not Detected PL Permit Limit R RPD outside accepted recovery limits

RL Reporting Detection Limit S Spike Recovery outside accepted recovery limits W Sample container temperature is out of limit as specified at testcode

BatchID: R196649

08-Nov-24

QC SUMMARY REPORT

24110446WO#:

Summit Environmental Technologies, Inc.

3310 Win St.

Cuyahoga Falls, Ohio 44223

Website: http://www.settek.com

TEL: (330) 253-8211 FAX: (330) 253-4489

Sample ID: LCS-R196649

Batch ID: R196649 TestNo: SW9075 Analysis Date: 11/8/2024

Prep Date:

Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual

Units: ppm

PQL

Client ID: LCSW

RunNo: 196649

SeqNo: 5318417

LCSSampType: TestCode: Halogens_Oil

Chlorine, Total 1000 99.3 80 120200 0993

Sample ID: MB-R196649

Batch ID: R196649 TestNo: SW9075 Analysis Date: 11/8/2024

Prep Date:

Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual

Units: ppm

PQL

Client ID: PBW

RunNo: 196649

SeqNo: 5318418

MBLKSampType: TestCode: Halogens_Oil

Chlorine, Total 200ND

Sample ID: 24110446-001ADUP

Batch ID: R196649 TestNo: SW9075 Analysis Date: 11/8/2024

Prep Date:

Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual

Units: ppm

PQL

Client ID: 152-19

RunNo: 196649

SeqNo: 5318420

DUPSampType: TestCode: Halogens_Oil

Chlorine, Total 20200 0 0<200

Qualifiers:

Original

E Value above quantitation range H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response

ND Not Detected PL Permit Limit R RPD outside accepted recovery limits

RL Reporting Detection Limit S Spike Recovery outside accepted recovery limits W Sample container temperature is out of limit as specified at testcode

BatchID: R196652

08-Nov-24

QC SUMMARY REPORT

24110446WO#:

Summit Environmental Technologies, Inc.

3310 Win St.

Cuyahoga Falls, Ohio 44223

Website: http://www.settek.com

TEL: (330) 253-8211 FAX: (330) 253-4489

Sample ID: LCS-R196652

Batch ID: R196652 TestNo: ASTM-D4294 Analysis Date: 11/8/2024

Prep Date:

Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual

Units: %

PQL

Client ID: LCSW

RunNo: 196652

SeqNo: 5318475

LCSSampType: TestCode: Sulfur_Oil(D4

% Sulfur 0.5000 92.7 70 1300.1000 00.4633

Sample ID: MB-R196652

Batch ID: R196652 TestNo: ASTM-D4294 Analysis Date: 11/8/2024

Prep Date:

Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual

Units: %

PQL

Client ID: PBW

RunNo: 196652

SeqNo: 5318476

MBLKSampType: TestCode: Sulfur_Oil(D4

% Sulfur 0.1000< 0.1000

Sample ID: 24110446-001ADUP

Batch ID: R196652 TestNo: ASTM-D4294 Analysis Date: 11/8/2024

Prep Date:

Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual

Units: %

PQL

Client ID: 152-19

RunNo: 196652

SeqNo: 5318478

DUPSampType: TestCode: Sulfur_Oil(D4

% Sulfur 200.1000 0 0< 0.1000

Qualifiers:

Original

E Value above quantitation range H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response

ND Not Detected PL Permit Limit R RPD outside accepted recovery limits

RL Reporting Detection Limit S Spike Recovery outside accepted recovery limits W Sample container temperature is out of limit as specified at testcode

BatchID: R196667

08-Nov-24

QC SUMMARY REPORT

24110446WO#:

Summit Environmental Technologies, Inc.

3310 Win St.

Cuyahoga Falls, Ohio 44223

Website: http://www.settek.com

TEL: (330) 253-8211 FAX: (330) 253-4489

Sample ID: LCS-R196667

Batch ID: R196667 TestNo: SW1010 Analysis Date: 11/8/2024

Prep Date:

Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual

Units: °F

PQL

Client ID: LCSW

RunNo: 196667

SeqNo: 5318969

LCSSampType: TestCode: FlashPt_Oil(1

Flash Point 140.0 102 98 1040142

Sample ID: LCSD-R196667

Batch ID: R196667 TestNo: SW1010 Analysis Date: 11/8/2024

Prep Date:

Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual

Units: °F

PQL

Client ID: LCSS02

RunNo: 196667

SeqNo: 5318970

LCSDSampType: TestCode: FlashPt_Oil(1

Flash Point 140.0 100 98 104 200 142.3 1.42140

Sample ID: 24110446-001ADUP

Batch ID: R196667 TestNo: SW1010 Analysis Date: 11/8/2024

Prep Date:

Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual

Units: °F

PQL

Client ID: 152-19

RunNo: 196667

SeqNo: 5318972

DUPSampType: TestCode: FlashPt_Oil(1

Flash Point 20166.2 0166

Qualifiers:

Original

E Value above quantitation range H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response

ND Not Detected PL Permit Limit R RPD outside accepted recovery limits

RL Reporting Detection Limit S Spike Recovery outside accepted recovery limits W Sample container temperature is out of limit as specified at testcode

RcptNo: 1Client Name: GES-NC- 28533 Work Order Number: 24110446

Sample Log-In Check List

Summit Environmental Technologies, Inc.

3310 Win St.

Cuyahoga Falls, Ohio 44223

Website: http://www.settek.com

TEL: (330) 253-8211 FAX: (330) 253-4489

Cooler Information

11/7/2024 9:05:00 AM

How was the sample delivered? FedEx

Is Chain of Custody complete? Yes No Not Present

Was an attempt made to cool the samples? Yes No NA

Are samples (except VOA and ONG) properly preserved? Yes No

Was preservative added to bottles? Yes No NA

Were any sample containers received broken? Yes No

Does paperwork match bottle labels? Yes No

Are matrices correctly identified on Chain of Custody? Yes No

Is it clear what analyses were requested? Yes No

Is the headspace in the VOA vials less than 1/4 inch or 6 mm? Yes No No VOA Vials

1.

2.

5.

9.

10.

11.

12.

13.

14.

15.

16.

(Note discrepancies on chain of custody)

Were all holding times able to be met? Yes No

Chain of Custody

Log In

(If no, notify customer for authorization.)

6. Were all samples received at a temperature of >0° C to 6.0°C Yes No NA

7. Sample(s) in proper container(s)? Yes No

8. Sufficient sample volume for indicated test(s)? Yes No

Not required

Logged by:

Completed By:

Reviewed By:

11/7/2024 11:12:31 AM

11/7/2024 3:34:35 PM

Anthony W. Britton

Anthony W. Britton

Jennifer Woolf

Special Handling (if applicable)

17.

18.

Was client notified of all discrepancies with this order? Yes No NA

Person Notified: Date:

Regarding:

Via: eMail Phone Fax In Person

Additional remarks:

Client Instructions:

By Whom:

Coolers are present? Yes No NA3.

Shipping container/cooler in good condition? Yes No4.

Custody seals intact on shipping container/cooler? Yes No Not Present

No. Seal Date: Signed By:

Seal No Seal Date Signed ByCondition Seal IntactCooler No Temp ºC

16.6box Good