B01_Attachment_3_Limits_of_Quantitation.xlsx
XLSX spreadsheet 30 KB Posted
- Attached to
- Lab Industrial Hygiene (IH) Sample Analysis Federal contract opportunity
- Solicitation number
- HT942524Q0030
- Issued by
- Defense Health Agency
About this file
This document contains limits of quantitation for sample analysis methods and hazardous drugs. The Defense Health Agency requires analysis of industrial hygiene and occupational health samples for various compounds through its solicitation HT942524Q0030 for lab industrial hygiene sample analysis services. Analysis must be performed for over 150 organic and inorganic compound groups using methods such as NIOSH, OSHA, EPA, and ASTM. Detection limits are provided for each analyte and method. The document also lists biological analysis methods and detection limits for hazardous drugs.
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Other files for this federal contract opportunity
| File | Type | Posted |
|---|---|---|
| B01. HT942524Q0030 0005.pdf | ||
| B01. HT942524Q0030 0004.pdf | ||
| B01. HT942524Q0030 0003.pdf | ||
| HT942524Q0030 0002.pdf | ||
| B01. Combined Synopsis_Solicitation HT942524Q0030.pdf | ||
| B01_Attachment_6_Price_Sheet.xlsx | XLSX spreadsheet | |
| B01_Acronyms_List_PWS_Attachment_1.pdf | ||
| B01_Attachment_7_DHA_Form_41.docx | DOCX document | |
| B01_Attachment_2_QASP.pdf | ||
| HT942524Q0030 0001.pdf | ||
| B01_Attachment_5_Past_Performance_Information_Sheet.docx | DOCX document | |
| B01_Attachment_4_Final_Reporting_Requirements_v2.docx | DOCX document |
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Text version
IH FY24 Base + 4OYs
| National Lead Lab Accreditation Program (NLLAP) Sample Analysis | Method | LIMITS | Units |
| Lead Prep/Paint Chip | Accredited NLLAP/EPA Method | ||
| Lead Prep/Soil | Accredited NLLAP/EPA Method | ||
| Lead Prep/Wipe | Accredited NLLAP/EPA Method | 10 | micrograms |
| Organic/Inorganic Compound Groups | Method | LIMITS | Units | |
| Alcohols I | NIOSH | 1400 | ||
| Ethyl Alcohol | 30 | micrograms | ||
| Isopropyl Alcohol | 30 | micrograms | ||
| Tert-Butyl Alcohol | 20 | micrograms | ||
| Alcohols II | NIOSH | 1401 | ||
| n-Butyl Alcohol | 20 | micrograms | ||
| sec-Butyl Alcohol | ||||
| Isobutyl Alcohol | ||||
| n-Propyl Alcohol | 30 | micrograms | ||
| Alcohols III | NIOSH | 1402 | ||
| Allyl Alcohol | ||||
| Diacetone Alcohol | 10 | micrograms | ||
| Cyclohexanol | ||||
| Isoamyl Alcohol | ||||
| Methyl Isobutyl Carbinol | ||||
| Alcohols IV | NIOSH | 1403 | ||
| 2-Methoxyethanol | ||||
| 2-Ethoxyethanol | 20 | micrograms | ||
| 2-Butoxyethanol | 20 | micrograms | ||
| Acid Gases | NIOSH | 7903 | ||
| Hydrogen Bromide | 1 | micrograms | ||
| Hydrogen Chloride | 2 | micrograms | ||
| Hydrogen Cyanide | 2 | micrograms | ||
| Hydrogen Fluoride | 2 | micrograms | ||
| Nitric Acid | 5 | micrograms | ||
| Phosphoric Acid | 5 | micrograms | ||
| Sulfuric Acid | 1 | micrograms | ||
| Dibromoethane | NIOSH | 1008 1003 | ||
| Hydrocarbons | NIOSH | 1500 | ||
| Cyclohexane | 5 | micrograms | ||
| Cyclohexene | 5 | micrograms | ||
| n-Decane | 5 | micrograms | ||
| n-Dodecane | 5 | micrograms | ||
| n-Heptane | 10 | micrograms | ||
| n-Hexane | 10 | micrograms | ||
| Methylcyclohexane | 5 | micrograms | ||
| n-Nonane | 5 | micrograms | ||
| n-Octane | 5 | micrograms | ||
| n-Pentane | 30 | micrograms | ||
| n-Undecane | 10 | micrograms | ||
| Hydrocarbons, Aromatic | NIOSH | 1501 | ||
| Benzene | 2 | micrograms | ||
| Ethyl Benzene | 10 | micrograms | ||
| Styrene | 10 | micrograms | ||
| Toluene | 10 | micrograms | ||
| Xylenes (Total) | 20 | micrograms | ||
| Hydrocarbons, Halogenated | NIOSH | 1003 | ||
| Carbon Tetrachloride | 50 | micrograms | ||
| Chlorobenzene | 50 | micrograms | ||
| Chloroform | 40 | micrograms | ||
| 1,1-Dichloroethane | 10 | micrograms | ||
| 1,2-Dichloroethane | 20 | micrograms | ||
| Hexachloroethane | 50 | micrograms | ||
| Tetrachloroethylene | 20 | micrograms | ||
| Trichloroethylene | 20 | micrograms | ||
| 1,1,1-Trichloroethane | 20 | micrograms | ||
| 1,1,2-Trichloroethane | 10 | micrograms | ||
| 1,2-Dichlorobenzene (o-) | 60 | micrograms | ||
| 1,4-Dichlorobenzene (p-) | 60 | micrograms | ||
| Isocyanates | OSHA | 42/47 | ||
| 1,6-HDI | 0.1 | micrograms | ||
| HMDI | 0.1 | micrograms | ||
| IPDI | 0.1 | micrograms | ||
| MDI | 0.1 | micrograms | ||
| 2,4-TDI | 0.1 | micrograms | ||
| 2,6-TDI | 0.1 | micrograms | ||
| Isocyanates | Isocheck | 0.03 | micrograms | |
| Ketones I | NIOSH | 1300 | ||
| Acetone | 30 | micrograms | ||
| 2-Hexanone | 20 | micrograms | ||
| Cyclohexnone | 20 | micrograms | ||
| Methyl Isobutyl ketone | 20 | micrograms | ||
| Diisobutyl Ketone | 20 | micrograms | ||
| 2-pentanone | 5 | micrograms | ||
| Ketones II | NIOSH | 1301 | ||
| Camphor | ||||
| Mesityl oxide | ||||
| 5-methyl-3-heptanone | ||||
| Methyl-(n-amyl)-ketone | 20 | micrograms | ||
| Ethyl buytl ketone | ||||
| Inorganic Acids | NIOSH | 7903 7907 | ||
| Hydrogen Bromide | 1 | micrograms | ||
| Hydrogen Chloride | 2 | micrograms | ||
| Hydrogen Fluoride | 2 | micrograms | ||
| Nitric Acid | 5 | micrograms | ||
| Phosphoric Acid | 5 | micrograms | ||
| Sulfuric Acid | 1 | micrograms | ||
| Metals (Welding Metals Group) | NIOSH/OSHA 7300/7303/125 | |||
| Aluminum | 2.5 | micrograms | ||
| Antimony | 0.5 | micrograms | ||
| Arsenic | 0.5 | micrograms | ||
| Barium | 0.5 | micrograms | ||
| Beryllium | 0.005 | micrograms | ||
| Cadmium | 0.25 | micrograms | ||
| Chromium | 1 | micrograms | ||
| Cobalt | 0.5 | micrograms | ||
| Copper | 0.5 | micrograms | ||
| Iron | 2.5 | micrograms | ||
| Lead | 0.1 | micrograms | ||
| Magnesium | 2.5 | micrograms | ||
| Manganese | 0.5 | micrograms | ||
| Molybdenum | 0.5 | micrograms | ||
| Nickel | 0.5 | micrograms | ||
| Selenium | 1 | micrograms | ||
| Silver | 0.5 | micrograms | ||
| Strontium | 0.5 | micrograms | ||
| Thallium | 0.5 | micrograms | ||
| Titanium | 2.5 | micrograms | ||
| Vanadium | 0.5 | micrograms | ||
| Zinc | 2.5 | micrograms | ||
| Metals Wipe Sample | NIOSH/EPA/ASTM | 9102/6010/1613 | ||
| Aluminum | ||||
| Antimony | ||||
| Arsenic | ||||
| Barium | ||||
| Beryllium | ||||
| Cadmium | ||||
| Chromium | ||||
| Cobalt | ||||
| Copper | ||||
| Iron | ||||
| Lead | ||||
| Magnesium | ||||
| Manganese | ||||
| Molybdenum | ||||
| Nickel | ||||
| Strontium | ||||
| Vanadium | ||||
| Zinc | ||||
| Esters 1 | NIOSH | 1450 | ||
| n-Amyl Acetate | 40 | micrograms | ||
| 2-Ethoxyethyl acetate | 20 | micrograms | ||
| n-Propyl acetate | 5 | micrograms | ||
| 1-Butyl Acetate | ||||
| Methyl isoamyl acetate | ||||
| sec-Butyl Acetate | 20 | micrograms | ||
| Isobutyl Acetate | 20 | micrograms | ||
| n-Butyl Acetate | 50 | micrograms | ||
| Isoamyl Acetate | 20 | micrograms | ||
| Ethyl acrylate | ||||
| Organophosphorus Pesticides | OSHA | 62 | ||
| Chlorpyrifos | 1.6 | micrograms | ||
| Diazinon | 1.5 | micrograms | ||
| Dichlorvos | 0.9 | micrograms | ||
| Malathion | 1.8 | micrograms | ||
| Parathion | 1.5 | micrograms | ||
| Isoflurane | OSHA | 103 | 5 | micrograms |
| Sevoflurane | OSHA | 103 | 5 | micrograms |
| Desflurane | OSHA | 106 | 5 | micrograms |
| Naphthas | NIOSH | 1550 | 100 | micrograms |
| 1- Bromopropane | OSHA | PV 2061 | ||
| 1-methoxy-2-propanol | OSHA | 99 | ||
| 1,2,4-Trimethyl benzene | OSHA | 07 2091 | ||
| 2,4-Dichlorophenoxyacetic Acid (2, 4-D) | NIOSH | 5001 | ||
| 2,4-Dinitrotoluene (2,4-DNT) | OSHA | 44 | 0.04 | micrograms |
| 2-Methoxyethylacate | NIOSH | 1451 | ||
| 2-Methoxymethylethoxy propanol (PPG-2 methyl ether) | OSHA | 101 | ||
| Acetic Acid | OSHA/NIOSH/In-house | ID 186 PV2119/2011/as applicable | 10 | micrograms |
| Acetonitrile | NIOSH | 1606 | 10 | micrograms |
| Acrolein | OSHA | 52 | 1 | micrograms |
| Amines, Aliphatic | NIOSH | 2010 | ||
| Ammonia | OSHA -ID | 186 188 | 25 | micrograms |
| Asbestos Fiber Count | NIOSH | 7400 | 7 | fibers/mm2 |
| Asbestos by TEM | NIOSH | 7402 | 7 | fibers/mm2 |
| Asbestos by TEM Full Quant - Bulk | TEMELAP | 198.4 | NA | NA |
| Benzene Solubles | OSHA | 58 | ||
| Anthracene | 0.1 | micrograms | ||
| Benzo(a)pyrene | 0.3 | micrograms | ||
| Chrysene | 0.3 | micrograms | ||
| Phenanthrene | 1 | micrograms | ||
| Pyrene | 1 | micrograms | ||
| Benzene Solubles (all of the above) | 50 | micrograms | ||
| Bisphenol A | NIOSH | 333 | ||
| Bulk Asbestos | EPA | 600.0/R93/116 | ||
| Organic/Inorganic Compound Groups | Method | LIMITS | Units | |
| Butyl Acetate | NIOSH | 1450 | 50 | micrograms |
| Butyl Cellosolve Acetate | OSHA | 83 | ||
| Carbon Disulfide | NIOSH | 1600 | 20 | micrograms |
| Chlordane | NIOSH | 5510 | 0.1 | micrograms |
| Chlorine | NIOSH | 6011 | ||
| Chromium, Hexavalent (Cr VI), plating/welding | OSHA- ID | 215 | 0.03 | micrograms |
| Chromium, Hexavalent (Cr VI), painting | OSHA- ID | 215 | 0.075 | micrograms |
| Coal Tar Pitch | OSHA | 58 | ||
| Anthracene | 0.1 | micrograms | ||
| Benzo(a)pyrene | 0.3 | micrograms | ||
| Chrysene | 0.3 | micrograms | ||
| Phenanthrene | 1 | micrograms | ||
| Pyrene | 1 | micrograms | ||
| Benzene Solubles | 50 | micrograms | ||
| Cresol, Modified | OSHA | 32 | 1.1 | micrograms |
| Cyanide | NIOSH | 6010 | 1 | micrograms |
| Cyanide | NIOSH | 7904 | 2.5 | micrograms |
| Dibromoethane | NIOSH | 1008 | 0.01 | micrograms |
| DichlorodifluoroMethane | NIOSH | 1018 | ||
| Diethylene glycol methyl ether (Methyl Carbitol) | OSHA | Mod. 101 | ||
| Dimethyformamide | NIOSH | 2004 | ||
| Dioctyl Phthalate | NIOSH | 5020 104 | ||
| Dipropylene glycol methyl ether | OSHA | 53 101 | ||
| Di-sec-octylphalate | NIOSH | 5020 | ||
| Elemental Carbon | NIOSH | 5040 | 0.3 | micrograms |
| Endrin | NIOSH | 5519 | 0.02 | micrograms |
| Epichlorohydrin | NIOSH | 1010 | 1 | micrograms |
| Ethanolamine | NIOSH/OSHA | 2007/60 | ||
| Ethyl 2-Cyanoacrylate | OSHA | 55 | 0.8 | micrograms |
| Ethyl Acetate | NIOSH | 1457 | 50 | micrograms |
| Ethyl Ether | NIOSH | 1610 | 20 | micrograms |
| Ethylene Dibromide | NIOSH | 1008 1003 | 0.1 | micrograms |
| Ethylene Glycol | NIOSH | 5523 | 5 | micrograms |
| Ethylene glycol dinitrate (EGDN) | NIOSH | 2507 | 0.3 | micrograms |
| Ethylene Oxide (ETO) | 3M & NIOSH / OSHA | 1614 1010 | 0.5 | micrograms |
| Fiber Count "B Counting Rules" | NIOSH | 7400 | ||
| Fluoride (Water soluble particulate and Gaseous) | NIOSH | 7902 | 10 | micrograms |
| Fluorides (Total Aero&Gas ) (Hydrogen Fluoride & Fluoride (F)) | NIOSH | 7902 | 400 | micrograms |
| Formaldehyde | NIOSH | 2016 | 0.5 | micrograms |
| Formaldehyde | NIOSH/OSHA | 2016/ID-205 | ||
| Formic Acid | NIOSH | 2011 | ||
| Gluteraldehyde | NIOSH | 2532 | 0.3 | micrograms |
| Glycols (each glycol) | NIOSH | 5523 | ||
| Hydroquinone | NIOSH OSHA | 5004 PV2094 | 3 | micrograms |
| Hydrogen Sulfide | NIOSH | 6013 | 11 | micrograms |
| Isobutyl Isobutyrate | NIOSH OSHA | 1550/1501 PV2090 | ||
| Isophorone | NIOSH | 2508 | 50 | micrograms |
| Isophorone diisocyanate (IPDI) | OSHA | PV2034 | ||
| Isopropyl Acetate | NIOSH | 1454 | ||
| Limonene | OSHA | PV2036 | ||
| Lindane | NIOSH | 5502 | ||
| Mercaptans | NIOSH | 2542 | ||
| Mercury | NIOSH | 6009 | ||
| Methanol (Methyl Alcohol) | NIOSH | 2000 | 30 | micrograms |
| Organic/Inorganic Compounds | Method | LIMITS | Units | |
| Methyl Acetate | NIOSH | 1458 | 20 | micrograms |
| Methyl Chloroform | NIOSH | 1003 | ||
| Methyl Ethyl Ketone (MEK) (2-Butanone) | NIOSH | 2500 1300 | ||
| Methyl ethyl ketone peroxide (MEKP) | NIOSH/OSHA | 3508/77 | ||
| Methyl Isocyanate | OSHA | 54 | ||
| Methyl Methacrylate | NIOSH | 2537 | 20 | micrograms |
| Methylene Chloride | NIOSH | 1005 | 5 | micrograms |
| Mineral Oil | NIOSH | 5026 | 100 | micrograms |
| Morpholine | NIOSH OSHA | 5150 60 | ||
| Nitric Oxide | NIOSH | 6014 | ||
| Nitric Oxide/Nitrogen Dioxide | OSHA | ID-190/ ID-182 | ||
| Nitrogen Dioxide | NIOSH | 6014 | ||
| N-Methyl-2-pyrrolidone | NIOSH | 1302 | ||
| Oil Mist | NIOSH | 500 | 100 | micrograms |
| Ozone | OSHA | ID-214 | 5 | micrograms |
| Particulates N.O.R (Resp) | NIOSH | 0600 | 100 | micrograms |
| Particulates N.O.R (Total) | NIOSH | 0500 | 100 | micrograms |
| PCBs (Aroclor 1221, 1260, 1262, 1268, 1016, 1242, 1254, 1248) | NIOSH | 5503 | ||
| Pentachlorophenol | OSHA | 39 | 2 | micrograms |
| Permethrin | OSHA | 70 | ||
| Phenol | OSHA | 32 | 10 | micrograms |
| Phenyl Glycidyl Ether | NIOSH | 1619 | ||
| Phosgene | OSHA | 61 | ||
| Phosphine | OSHA | 1003 | ||
| Phosphorus, White/Yellow | NIOSH | 7905 | 0.05 | micrograms |
| Potassium Hydroxide | NIOSH | 7401 | 30 | micrograms |
| Propyl Bromide | OSHA NIOSH | IMIS R290 PV2061 | ||
| Pyrethrum | NIOSH | 5008 | ||
| Silica, Crystalline (Respirable) | NIOSH | 7500 | 10 | micrograms |
| Silica, Crystalline (Total) | NIOSH | 7500 | 10 | micrograms |
| Sodium Hydroxide | NIOSH | 7401 | 30 | micrograms |
| Sulfur Dioxide | OSHA | 200 | ||
| Sulfuric Acid | OSHA | ID-113 | ||
| Tetrahydrofuran | NIOSH | 1609 | 100 | micrograms |
| 2,4,6-Trinitrotoluene (TNT) | OSHA | 44 | 0.05 | micrograms |
| Trichloroethylene (TCE) | NIOSH | 1022 | 20 | micrograms |
| Trichlorofluoromethane | NIOSH | 1006 | ||
| Triethanolamine | OSHA | PV2141 | ||
| Triethylenetetramine | NIOSH OSHA | 2540 60 | ||
| Vinyl Acetate | NIOSH | 1453 | ||
| Vinyl Chloride | NIOSH | 1007 | ||
| Welding Fumes, Total | NIOSH | 0500 | 100 | micrograms |
| Biological Analysis | Method | LIMITS | Units |
| Biological Micro Examination (bulk and wipes) | Micro | ||
| Spore Count (Air) | Micro |
| Hazardous Drugs (USP 800) | Method | LIMITS | Units |
| 5-Fluorouracil | Accredited Method | 30 | nanograms |
| Methotrexate | Accredited Method | 30 | nanograms |
| Ifosfamide | Accredited Method | 30 | nanograms |
| Cyclophosphamide | Accredited Method | 30 | nanograms |
| Doxorubicin | Accredited Method | 30 | nanograms |
| Paclitaxel | Accredited Method | 60 | nanograms |
| Red font indicates updates |
&"Arial,Bold"PWS ATTACHMENT 3 - Limits of Quantitation (LOQs) &KFF0000as of July 2023 &K000000
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