Z2-LAB-ANALYSIS-RECOVERY-TANK_-_Copy.pdf

15011317

10100 East Freeway, Suite 100, Houston, TX 77029 tel: 713-453-6060, fax: 713-453-6091, http://www.ablabs.com

Laboratory Analysis Report

Job ID :

Total Number of Pages: 9

City, State, Zip:

C.O.H. Sampling - Underground Holding Tank-1178 Ellington Field Road.

Saul A. Estupinian

Client Address:

Client Name:

Client Project Name :

P.O.#.:

Sample Collected By:

1178 Ellington Field Rd.

USCG Air Station HoustonReport To :

Attn:

Houston, Texas, 77034

Date Collected: 01/29/15

Client Sample ID A&B Sample ID

A&B Labs has analyzed the following samples...

Matrix

Deludge Tank 15011317.01Water

This report cannot be reproduced, except in full, without prior written permission of A&B Labs. Results shown relate only to the items tested. Samples are assumed to be in acceptable condition unless otherwise noted. Blank correction is not made unless otherwise noted. Air concentrations reported are based on field sampling information provided by client. Soil samples are reported on a wet weight basis unless otherwise noted. Uncertainty estimates are available on request.

2/5/2015

Title:

Released By:

Jr. Project Manager

Karin Underbrink

Date Received : 01/29/2015 16:00

This Laboratory is NELAP (T104704213-14-12) accredited. Effective: 11/21/2014; Expires: 03/31/2015

I am the laboratory manager, or his/her designee, and I am responsible for the release of this data package. This laboratory data package has been reviewed and is complete and technically compliant with the requirements of the methods used, except where noted in the attached exception reports.

I affirm, to the best of my knowledge that all problems/anomalies observed by this laboratory (and if applicable, any and all laboratories subcontracted through this laboratory) that might affect the quality of the data, have been identified in the Laboratory Review Checklist, and that no information or data have been knowingly withheld that would affect the quality of the data.

Date:

Scope: Non-Potable Water, Drinking Water, Air, Solid, Biological Tissue, Hazardous Waste

General Term Definition

BRL

Front-Wt

Below Reporting Limit

Front Weight

Back WeightBack-Wt cfu colony-forming units

Conc. Concentration

D.F. Dilution Factor

LCS Laboratory Check Standard

LCSD Laboratory Check Standard Duplicate

MS Matrix Spike

MSD Matrix Spike Duplicate

Molecular WeightMW

RPD

ppm parts per million

Relative Percent Difference

TNTC Too numerous to count

Post-Wt

Pre-Wt Previous Weight

Q Qualifier

RegLimit Regulatory Limit

RptLimit Reporting Limit

T Time

Post Weight surr Surrogate

SDL Sample Detection Limit

15011317

L A B O R A T O R Y T E R M A N D Q U A L I F I E R D E F I N I T I O N R E P O R T

Date:Job ID : 2/5/2015

Qualifier Definition

Insufficient sample for analysis of matrix spike. QC Batch reported with LCS/LCSD.Q11

L A B O R A T O R Y T E S T R E S U L T S

Water

15011317.01

Sample Matrix

Job Sample ID:

AnalystDate TimeQReg LimitRpt LimitDFUnitsResultParameter/Test DescriptionTest Method

Deludge Tank

Other Information:

Time Collected:

Client Sample ID:

Date Collected:

Saul A. EstupinianAttn:

C.O.H. Sampling - Underground Holding Tank-1178 Ellington Field Road.Project Name:

USCG Air Station HoustonClient Name:

Date 15011317Job ID :

2/5/2015

01/29/15

11:52

Oil & Grease, Hexane ExtractablesEPA 1664B

SG02/03/15 07:00Q112.781.11mg/LBRLOil & Grease

Total Recoverable MetalsEPA 200.7

GG01/30/15 14:260.011mg/LBRLArsenic

GG01/30/15 14:260.011mg/LBRLCadmium

GG01/30/15 14:260.011mg/LBRLChromium

GG01/30/15 14:260.011mg/L0.017Copper

GG01/30/15 14:260.011mg/LBRLLead

GG01/30/15 14:260.011mg/LBRLNickel

GG01/30/15 14:260.051mg/LBRLSelenium

GG01/30/15 14:260.011mg/L0.042Zinc

Total Metals - MercuryEPA 245.1

SRG01/30/15 14:140.00021mg/LBRLMercury

Chemical Oxygen DemandSM 5220D

AJ02/03/15 10:10101mg/L131.0COD

Q U A L I T Y C O N T R O L C E R T I F I C A T E

Date :15011317Job ID :

Ggorane

Samples in This QC Batch :

Qb15013057

Total Recoverable Metals

15011317.01

Reporting Units :

01/30/15QC Batch ID :

Method :

Created Date :

Analysis :

Created By :

mg/LEPA 200.7

2/5/2015

Prep Date : 01/30/15 08:44EPA 200.7Prep Method :PB15013039Digestion : EperezPrep By :

QC Type: Method Blank

D.F. RptLimitParameter Result Units QualCAS # mg/L 0.01BRL 1Arsenic 7440-38-2 mg/L 0.01BRL 1Cadmium 7440-43-9 mg/L 0.01BRL 1Chromium 7440-47-3 mg/L 0.01BRL 1Copper 7440-50-8 mg/L 0.01BRL 1Lead 7439-92-1 mg/L 0.01BRL 1Nickel 7440-02-0 mg/L 0.05BRL 1Selenium 7782-49-2 mg/L 0.01BRL 1Zinc 7440-66-6

%Recovery CtrlLimit

LCSD

Result

LCS

Result

RPD

CtrlLimitRPD

LCS

Spk Added

LCSD

% Rec

LCS

% RecParameter

LCSD

Spk Added

QC Type: LCS and LCSD

Qual

1.41021 85-115100 201.003Arsenic 1 1.018

1.41011 85-11599.4 200.994Cadmium 1 1.008

0.399.91 85-11599.7 200.997Chromium 1 0.999

0.81011 85-115100 201.001Copper 1 1.009

1.299.21 85-11598 200.980Lead 1 0.992

1.41001 85-11598.7 200.987Nickel 1 1.001

1.91041 85-115102 201.022Selenium 1 1.041

0.5991 85-11598.6 200.986Zinc 1 0.990

QC Type: MS and MSD

15011307.01QC Sample ID:

Parameter Sample Result

RPD

CtrlLimit

MS

Result

MS

Spk Added RPD Qual

MS

% Rec

MSD

Spk Added

MSD

% Rec

%Rec CtrlLimit

MSD

Result

BRLArsenic 1 1161.158 75-125

0.173Cadmium 1 1081.257 75-125

0.274Chromium 1 99.81.272 75-125

0.160Copper 1 1061.225 75-125

BRLLead 1 86.40.864 75-125

0.147Nickel 1 92.21.069 75-125

BRLSelenium 1 1171.173 75-125

0.077Zinc 1 1031.105 75-125

Refer to the Definition page for terms.

SRGade

Samples in This QC Batch :

QB15013089

Total Metals - Mercury

15011317.01

Reporting Units :

01/30/15QC Batch ID :

Method :

Created Date :

Analysis :

Created By :

mg/LEPA 245.1

2/5/2015

Prep Date : 01/30/15 10:00EPA 245.1Prep Method :PB15013056Digestion : EperezPrep By :

QC Type: Method Blank

D.F. RptLimitParameter Result Units QualCAS # mg/L 0.0002BRL 1Mercury 7439-97-6

%Recovery CtrlLimit

LCSD

Result

LCS

Result

RPD

CtrlLimitRPD

LCS

Spk Added

LCSD

% Rec

LCS

% RecParameter

LCSD

Spk Added

QC Type: LCS and LCSD

Qual

4.31080.005 80-120113 350.0057Mercury 0.005 0.0054

QC Type: MS and MSD

15011244.01QC Sample ID:

Parameter Sample Result

RPD

CtrlLimit

MS

Result

MS

Spk Added RPD Qual

MS

% Rec

MSD

Spk Added

MSD

% Rec

%Rec CtrlLimit

MSD

Result

BRLMercury 0.005 99.60.0050 80-120

Sgarcia

Samples in This QC Batch :

Qb15020302

Oil & Grease, Hexane Extractables

15011317.01

Reporting Units :

02/03/15QC Batch ID :

Method :

Created Date :

Analysis :

Created By :

mg/LEPA 1664B

2/5/2015

Prep Date : 02/03/15 06:50EPA 1664BPrep Method :PB15020301Sample Preparation : SgarciaPrep By :

QC Type: Method Blank

D.F. RptLimitParameter Result Units QualCAS # mg/L 2.48BRL 0.990Oil & Grease

%Recovery CtrlLimit

LCSD

Result

LCS

Result

RPD

CtrlLimitRPD

LCS

Spk Added

LCSD

% Rec

LCS

% RecParameter

LCSD

Spk Added

QC Type: LCS and LCSD

Qual

0.593.140 78-11493.5 1137.4Oil & Grease 40 37.2

Ajohn

Samples in This QC Batch :

Qb15020344

Chemical Oxygen Demand

15011317.01

Reporting Units :

02/03/15QC Batch ID :

Method :

Created Date :

Analysis :

Created By :

mg/LSM 5220D

2/5/2015

Prep Date : 02/03/15 10:00SM 5220DPrep Method :PB15020327Sample Preparation : AjohnPrep By :

QC Type: Method Blank

D.F. RptLimitParameter Result Units QualCAS # mg/L 10BRL 1COD

%Recovery CtrlLimit

LCSD

Result

LCS

Result

RPD

CtrlLimitRPD

LCS

Spk Added

LCSD

% Rec

LCS

% RecParameter

LCSD

Spk Added

QC Type: LCS and LCSD

Qual

2.497300 80-12094.7 20284COD 300 291

QC Type: MS and MSD

15011317.01QC Sample ID:

Parameter Sample Result

RPD

CtrlLimit

MS

Result

MS

Spk Added RPD Qual

MS

% Rec

MSD

Spk Added

MSD

% Rec

%Rec CtrlLimit

MSD

Result

131.0COD 400 105 2.4400 540550 20 80-120102

Sample Condition Checklist pH Paper ID : 58986 Thermometer ID : 140539697

Sample pH : <2 COD, Metals Temperature : 1.0+0.7cf=1.7°C

Client Name : USCG Air Station Houston

Time Received : 4:00PMDate Received : 01/29/2015 A&B JobID : 15011317

Comments : Include actions taken to resolve discrepancies/problem:

X Sample accepted.17.

X VOA vials completely filled.16.

X Samples were received within the hold time.15.

X Sample volume is sufficient for analyses requested.14.

X Bottle count on C-O-C matches bottles found.13.

X Sample ID labels match C-O-C ID's12.

X All samples were logged or labeled.11.

X Sample(s) were received with proper preservative10.

X Sample(s) were received in appropriate container(s).9.

Matrix

Sludge Cassette Tube BulkSolidLiquidSoilWater Badge Food Other 8.

X Sample containers arrived intact. (If no comment).7.

X Sample(s) received with signed sample custody seal.6.

X C-O-C signed and dated.5.

X Sample(s) received with chain-of-custody.4.

X If yes, ice in cooler.3.

X Sample(s) in a cooler.2.

X Cooler seal present and signed.1.

N/ANoYesCheck Points

Received by : Check in by/date : AHall / 01/29/2015AHall

Phone : www.ablabs.com 713-453-6060