Final NB646020-23-00438 SOR - Mass Spectrometer .1691175248848.pdf

STATEMENT OF REQUIREMENTS

TITLE: Triple quadrupole mass spectrometry detector

I. SPECIFICATIONS

The Contractor shall provide one (1) refurbished Ultivo Triple Quadrupole Mass Spectrometer that meets or exceeds the following requirements:

System

• The Mass Spectrometer shall have a dedicated Electrospray Ionization (ESI) source.

• The Mass Spectrometer shall have a mass resolution of at least 0.7 Dalton (determined at

FWHM).

• The Mass Spectrometer shall have a mass range of at least 5 to 1400 m/z.

• The Mass Spectrometer shall have a mass accuracy of at least 0.1 Dalton from 5 to 1000 m/z, and 0.2 Dalton from 1000 to 1400 m/z.

• The Mass Spectrometer shall have a linear dynamic range of at least > 6 × 106 (counts).

• The Mass Spectrometer shall have polarity switching ≤ 20 ms.

• The Mass Spectrometer shall have acquisition scan modes that include MS2 scan, product ion scan, neutral ion scan, SIM, MRM (static, dynamic, triggered), and mixed mode (simultaneous acquisition of various scan modes in one time).

• The Mass Spectrometer shall have a maximum scan rate of at least 15,000 Dalton/second with a maximum MRM acquisition rate of 500 MRMs/second.

• The Mass Spectrometer shall have MRM transitions of at least 500 MRMs/time segment and 33,000 MRMs/method.

• The Mass Spectrometer shall have Dynamic MRM transitions of at least 4,000 dynamic transitions/method.

• The Mass Spectrometer shall have Triggered MRM transitions of up to 10 MRM transitions (primary and secondary) for library search and compound confirmation.

• The Mass Spectrometer shall have a collision cell ion clearance < 1 ms.

• The Mass Spectrometer shall have a single point of control.

• The Mass Spectrometer shall have a data system capable of full system control through

Agilent MassHunter software (already in function at NIST) which can store and process spectral data from the detector.

• The Mass Spectrometer shall be capable of connecting to an already existing Agilent

Infinity II Series HPLC/UHPLC system.

Manual

• The Mass Spectrometer shall come with two (2) operations and maintenance manuals which cover proper operation, routine maintenance, and troubleshooting for all instrument components controlling software (supplied in hard copy or electronic format, or both)

Installation:

The Contractor shall install the instrument at 100 Bureau Drive, Gaithersburg, MD 20899, Building 227, Room B133. Installation shall include, at a minimum, uncrating/unpacking of all equipment, set-up and hook-up of all equipment, start-up, demonstration of specifications, and removal of all trash. Instrument shall operate to manufacturer’s specifications upon installation.

Installation shall take place during normal business hours, between 8:30 am and 5:00 pm Eastern

Time, Monday through Friday except Federal Holidays, and shall be coordinated with the NIST

Contracting Officer Representative (COR). Installation shall occur within 10 days after receipt of Mass Spectrometer.

Training:

The Contractor shall provide training for up to four (4) NIST personnel at 100 Bureau Drive, Gaithersburg, MD 20899, Building 227, Room B133. Training shall cover normal operation, demonstration of specifications, operation of software, troubleshooting, and routine maintenance.

Training shall be provided during normal business hours, between 8:30am and 5:00pm Eastern

Time, Monday through Friday, except Federal Holidays, and shall be coordinated with the NIST

COR to ensure maximum availability of NIST personnel. Training shall occur within 10 days of installation.

Warranty:

The Contractor shall provide, at a minimum, a one-year warranty for the equipment. The warranty shall cover all parts, labor and travel. The warranty shall commence upon successful completion of delivery, installation, training and demonstration of all required specifications.

II. DELIVERY

The address for the delivery of the instrument is detailed below. Normal duty hours are Monday through Friday, 8:30 a.m. to 5:00 p.m. with the exception of Federal holidays.

National Institute of Standards and Technology

100 Bureau Drive

MS 8392

Gaithersburg, MD 20899

Attn: COR

III. DELIVERABLES

Description Quantity Recipient Due Date

Refurbished Ultivo Triple

Quadrupole Mass Spectrometer One (1) COR

Within 120 days after award of requirement

Operations and maintenance manual Two (2) COR Within 120 days after award of requirement.

Installation Once COR Within 10 days after receipt of Mass

Spectrometer

Training (up to four personnel) Once COR Within 10 days after installation

Delivery of a refurbished Ultivo Triple Quadrupole Mass Spectrometer to NIST, installation, and training to be completed within 120 calendar days after contract award. One-year warranty shall begin upon NIST acceptance of equipment, installation, and training. All work shall be completed at the Contractor’s facility. Installation of the instrument and training shall be accomplished at NIST, Gaithersburg, Maryland. Normal duty hours are Monday through Friday, 8:30 a.m. to 5:00 p.m. with the exception of Federal holidays

IV. ACCEPTANCE CRITERIA

After installation, the Contractor shall demonstrate that all performance specifications are met.

V. GENERAL INFORMATION

Safety: The Contractor employee shall be responsible for knowing and complying with commercial installation safety prevention regulations. Such regulations include, but are not limited to, general safety, fire prevention, and waste disposal.

Security: NIST is a restricted campus. An identification badge is required for access for entry into buildings and also is shown to the armed Security Police when entering the campus.

Identification Badges: Contractor employees shall comply with NIST identification and access requirements. The Contractor shall provide the name and citizenship information of employees for on-site visits to the NIST Contracting Officer Representative (COR) prior to arrival. The

COR will submit the name(s) and citizenship information to the NIST Office of Security in order for a given Contractor employee to enter the NIST campus. The Contractor employee is responsible for absences due to missing or expired identification and access documents. Each

Contractor employee shall wear a visible identification badge provided by the NIST Security

Office.

Vehicle Registration: All Contractor employees must register their vehicles with the NIST

Security Office to gain access to the campus. A valid driver’s license, Government-furnished civilian ID (which in most cases can be a valid driver's license), proof of insurance and current registration must be presented to the NIST Security Office.