Perk Pond Sample Result.pdf

5/6/2010

SP-Analytica, Inc. - Fairbanks 475 Hall St.

Fairbanks, AK 99701 907-456-3116 Fax: 907-456-3125

354 CES/CEOI

2310 Central Ave.

Eielson AFB, AK 99702-2299 Attn: Master Sgt. Justin Porter

Work Order #: F1004160 Date: 5/6/2010 Work ID: Sludge from Perk Pond Date Received: 4/8/2010

Client DescriptionLab Sample Number

Sample Identification

Lab Sample Number Client Description

F1004160-01 Perk Pond

Enclosed are the analytical results for the submitted sample(s). Please review the CASE NARRATIVE for a discussion of any data and/or quality control issues. Listings of data qualifiers, analytical codes, key dates, and QC relationships are provided at the end of the report.

Sincerely, Carissa Seltrecht Project Manager

"The Science of Analysis, The Art of Service" cseltrecht

Case Narrative Analytica International - Fairbanks

Work Order: F1004160

Samples were prepared and analyzed according to EPA or equivalent methods outlined in the following references:

Test Methods for Evaluating Solid Waste, USEPA SW-846, Third Edition, Revision 4, December 1996.

SAMPLE RECEIPT:

One (1) sample was received on 4/8/2010 at 4:50:00 PM at Analytica International - Fairbanks. The sample was received in good condition and in order per chain of custody.

Comments:

The samples was transferred for analysis to Analytica Environmental Laboratories (AEL), 12189 Pennsylvania St., Thornton, Colorado 80241, where it was received in good condition and in order per chain of custody.

REVIEW FOR COMPLIANCE WITH ANALYTICA QA PLAN

A summary of our review is shown below.

All analytical results contained in this report have been reviewed under Analytica's internal quality assurance and quality control program. Any deviations in quality control parameters for specific analyses are noted in the following text. A complete quality assurance report, including laboratory control, matrix spike, and sample duplicate recoveries, is kept on file in our office and is available upon request.

All method specifications were met for the following tests, unless otherwise noted:

Test Method: SW7470A - Mercury in Liquid Waste by CVAA (TCLP Extracted) - 1311-Hg - Waste Water

The following are subcontracted tests and have been represented to us as having met criteria:

Test Method: SW6010B - ICP (TCLP Extracted) - 1311-metals - Waste Water

SP-Analytica, Inc. - Fairbanks 475 Hall St.

Fairbanks, AK 99701 Phone: 907-456-3116 Fax: 907-456-3125

COC #:

Client Sample ID:

Waste WaterSample Matrix:

Sampling Location:

73824

5/6/2010Report Date:

Receipt Date:

Sample Date:

Sample Time:

Collected By:

4/6/2010

1:00:00PM

RH

4/8/2010

Flag Definitions:

MRL = Method Reporting Limit MCL = Maximum Contaminant Limit B = Present also in Method Blank H = Exceeds Regulatory Limit M = Matrix Interference J = Estimated Value D = Lost to Dilution ** = RL higher than MCL; target not detected

PWS#:

2310 Central Ave.

Eielson AFB, AK 99702-2299 907-377-2264 Fax: 907-377-4718

Client Project: Sludge from Perk Pond

Comments:

354 CES/CEOI

Attn: Master Sgt. Justin Porter

Residual Chlorine:

TNC = Too Numerous to Count - result rejected CF = Confluent Growth - result rejected TCNG = Turbid Culture No Growth - rejected

Perk Pond

Lab#: F1004160-01A Analysis Method

Parameter Result Units Flags MRL Prep Method

Analysis Date Analyst

Prep Date

Test was conducted by: Analytica - Thornton6010B/3010A (TCLP) - 1311-metals Arsenic 3010Amg/L

Barium 3010Amg/L

Cadmium 3010Amg/L

Chromium 3010Amg/L

Lead 3010Amg/L

Selenium 3010Amg/L

Silver 3010Amg/L Test was conducted by: Analytica - Thornton7470A/7470A (TCLP) - 1311-Hg

Mercury 0.00020 4/22/2010 4/22/2010 AT7470Amg/L<MRL cseltrecht Please refer to the Sub- Contractor report.

Owner

Owner F1004160