Atch_11_TEKLAB_Sample_Results-B861.pdf

http://www.teklabinc.com/

February 25, 2013

WorkOrder: 13020814Drinking Water LeadRE:

Dear SrA Timothy Burnett:

TEKLAB, INC received 2 samples on 2/19/2013 8:45:00 AM for the analysis presented in the following report.

Samples are analyzed on an as received basis unless otherwise requested and documented. The sample results contained in this report relate only to the requested analytes of interest as directed on the chain of custody. NELAP accredited fields of testing are indicated by the letters NELAP under the Certification column.

Unless otherwise documented within this report, Teklab Inc. analyzes samples utilizing the most current methods in compliance with 40CFR.

All tests are performed in the Collinsville, IL laboratory unless otherwise noted in the Case Narrative.

All quality control criteria applicable to the test methods employed for this project have been satisfactorily met and are in accordance with NELAP except where noted. The following report shall not be reproduced, except in full, without the written approval of Teklab, Inc.

If you have any questions regarding these tests results, please feel free to call.

Sincerely, 375 AMDS/SGPB

310 West Losey Street Scott AFB, IL 62225

(618) 256-7307

(618) 256-7090

TEL:

FAX:

SrA Timothy Burnett Scott Air Force Base

Shelly A. Hennessy Project Manager (618)344-1004 ex 36 SHennessy@teklabinc.com

____TeklabHdrP

Definitions

Client Project: Drinking Water Lead

Client: Scott Air Force Base

Report Date: 25-Feb-13

Work Order: 13020814 http://www.teklabinc.com/

Abbr Definition CCV Continuing calibration verification is a check of a standard to determine the state of calibration of an instrument between recalibration.

DF Dilution factor is the dilution performed during analysis only and does not take into account any dilutions made during sample preparation. The reported result is final and includes all dilutions factors.

DNI Did not ignite

DUP Laboratory duplicate is an aliquot of a sample taken from the same container under laboratory conditions for independent processing and analysis independently of the original aliquot.

ICV Initial calibration verification is a check of a standard to determine the state of calibration of an instrument before sample analysis is initiated.

IDPH IL Dept. of Public Health

LCS Laboratory control sample, spiked with verified known amounts of analytes, is analyzed exactly like a sample to establish intra-laboratory or analyst specific precision and bias or to assess the performance of all or a portion of the measurement system. The acceptable recovery range is in the QC Package (provided upon request).

LCSD Laboratory control sample duplicate is a replicate laboratory control sample that is prepared and analyzed in order to determine the precision of the approved test method. The acceptable recovery range is listed in the QC Package (provided upon request).

MB Method blank is a sample of a matrix similar to the batch of associated sample (when available) that is free from the analytes of interest and is processed simultaneously with and under the same conditions as samples through all steps of the analytical procedures, and in which no target analytes or interferences should present at concentrations that impact the analytical results for sample analyses.

MDL Method detection limit means the minimum concentration of a substance that can be measured and reported with 99% confidence that the analyte concentration is greater than zero and is determined from analysis of a sample in a given matrix type containing the analyte.

MS Matrix spike is an aliquot of matrix fortified (spiked) with known quantities of specific analytes that is subjected to the entire analytical procedures in order to determine the effect of the matrix on an approved test method’s recovery system. The acceptable recovery range is listed in the QC Package (provided upon request).

MSD Matrix spike duplicate means a replicate matrix spike that is prepared and analyzed in order to determine the precision of the approved test method.

The acceptable recovery range is listed in the QC Package (provided upon request).

MW Molecular weight

ND Not Detected at the Reporting Limit

NELAP NELAP Accredited

PQL Practical quantitation limit means the lowest level that can be reliably achieved within specified limits of precision and accuracy during routine laboratory operation conditions. The acceptable recovery range is listed in the QC Package (provided upon request).

RL The reporting limit the lowest level that the data is displayed in the final report. The reporting limit may vary according to customer request or sample dilution. The reporting limit may not be less than the MDL.

RPD Relative percent difference is a calculated difference between two recoveries (ie. MS/MSD). The acceptable recovery limit is listed in the QC Package (provided upon request).

SPK The spike is a known mass of target analyte added to a blank sample or sub-sample; used to determine recovery deficiency or for other quality control purposes.

Surr Surrogates are compounds which are similar to the analytes of interest in chemical composition and behavior in the analytical process, but which are not normally found in environmental samples.

TNTC Too numerous to count ( > 200 CFU )

Qualifiers # - Unknown hydrocarbon B - Analyte detected in associated Method Blank

E - Value above quantitation range H - Holding times exceeded

M - Manual Integration used to determine area response ND - Not Detected at the Reporting Limit

R - RPD outside accepted recovery limits S - Spike Recovery outside recovery limits

X - Value exceeds Maximum Contaminant Level http://www.teklabinc.com/ AbbrDefinition CCVContinuing

Case Narrative

Client Project: Drinking Water Lead

Client: Scott Air Force Base

Report Date: 25-Feb-13

Work Order: 13020814 http://www.teklabinc.com/

Cooler Receipt Temp: 0.4 °C

NELAPState Cert # Exp Date LabDept

Locations and Accreditations

____________________________________Collinsville

Address 5445 Horseshoe Lake Road

Collinsville, IL 62234-7425

Phone (618) 344-1004

Fax (618) 344-1005

Email jhriley@teklabinc.com

____________________________________Springfield

Address 3920 Pintail Dr

Springfield, IL 62711-9415

Phone (217) 698-1004

Fax (217) 698-1005

Email KKlostermann@teklabinc.com

____________________________________Kansas City

Address 8421 Nieman Road

Lenexa, KS 66214

Phone (913) 541-1998

Fax (913) 541-1998

Email dthompson@teklabinc.com

Illinois 100226 1/31/2014 CollinsvilleNELAPIEPA

Kansas E-10374 1/31/2014 CollinsvilleNELAPKDHE

Louisiana 166493 6/30/2013 CollinsvilleNELAPLDEQ

Louisiana 166578 6/30/2013 SpringfieldNELAPLDEQ

Texas T104704515-12-1 7/31/2013 CollinsvilleNELAPTCEQ

Arkansas 88-0966 3/14/2013 CollinsvilleADEQ

Illinois 17584 4/30/2013 CollinsvilleIDPH

Kentucky 0073 5/26/2013 CollinsvilleUST

Missouri 00930 4/13/2013 CollinsvilleMDNR

Oklahoma 9978 8/31/2013 CollinsvilleODEQ

TeklabHdrP

Laboratory Results

Client Project: Drinking Water Lead

Client: Scott Air Force Base

Report Date: 25-Feb-13

Work Order: 13020814 http://www.teklabinc.com/

Analyses Result Units Date AnalyzedRL DFCertification Qual

Collection Date: 02/13/2013 9:05

Lab ID: 13020814-001 Client Sample ID: 861 Hydrant

Matrix: DRINKING WATER

Batch

EPA 600 4.1.4, 200.7R4.4, METALS BY ICP (TOTAL)

Copper 02/20/2013 15:080.0100 mg/L 1< 0.0100NELAP 85897

STANDARD METHODS 3030 E, 3113 B, METALS BY GFAA

Lead 02/22/2013 11:200.0020 mg/L 1< 0.0020NELAP 85898

TeklabHdrP

Laboratory Results

Client Project: Drinking Water Lead

Client: Scott Air Force Base

Report Date: 25-Feb-13

Work Order: 13020814 http://www.teklabinc.com/

Analyses Result Units Date AnalyzedRL DFCertification Qual

Collection Date: 02/16/2013 7:55

Lab ID: 13020814-002 Client Sample ID: 861 Womens Bathroom

Matrix: DRINKING WATER

Batch

EPA 600 4.1.4, 200.7R4.4, METALS BY ICP (TOTAL)

Copper 02/20/2013 15:140.0100 mg/L 10.331NELAP 85897

STANDARD METHODS 3030 E, 3113 B, METALS BY GFAA

Lead 02/22/2013 11:300.0040 mg/L 20.0510NELAP 85898

Receiving Check List

Client Project: Drinking Water Lead

Client: Scott Air Force Base

Report Date: 25-Feb-13

Work Order: 13020814 http://www.teklabinc.com/

Received By: SRHCarrier: Rick Schmidt

Completed by: Reviewed by:

On:

19-Feb-13

On:

19-Feb-13

Shipping container/cooler in good condition? Yes No Not Present

Chain of custody present? Yes No

Chain of custody signed when relinquished and received? Yes No

Chain of custody agrees with sample labels? Yes No

Samples in proper container/bottle? Yes No

Sample containers intact? Yes No

Sufficient sample volume for indicated test? Yes No

All samples received within holding time? Yes No

Container/Temp Blank temperature in compliance? Yes No

Temp °C 0.4

When thermal preservation is required, samples are compliant with a temperature between 0.1°C - 6.0°C, or when samples are received on ice the same day as collected.

Any No responses must be detailed below or on the COC.

Water – at least one vial per sample has zero headspace? Yes No No VOA vials

Water - pH acceptable upon receipt? Yes No

Type of thermal preservation? None Ice Blue Ice Dry Ice

Chain of custody 1 Extra pages included 0

Reported field parameters measured: Field Lab NA

Pages to follow:

Water - TOX containers have zero headspace? Yes No No TOX containers

NPDES/CWA TCN interferences checked/treated in the field? Yes No NA

Emily E. Pohlman Shelly A. Hennessy