Charleston_Hazardous_Waste_SOW.docx

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Chemical and Biological Waste Disposal - SC
Solicitation number
1305M224Q0298
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This document is a Statement of Work (SOW) for chemical and biological waste disposal services at the National Oceanic and Atmospheric Administration (NOAA) Hollings Marine Laboratory in Charleston, SC.

The SOW covers the requirements to remove and properly dispose of chemical and biological wastes generated by the research facility, including hazardous materials classified under various DOT hazard classes. The contractor must provide all labor, services, and materials to package, label, manifest, transport, and dispose of the wastes using approved methods prioritizing recycling, fuels blending, and waste-to-energy. The contractor must have at least 5 years' experience, own a compliant Transportation, Storage, and Disposal Facility (TSDF), and provide documentation of licenses, permits, and insurance. Pickup and disposal is required quarterly, with detailed reporting and certificates of destruction provided. The contractor will be selected through a competitive solicitation process, with award under Solicitation #1305M224Q0298 for the NOAA Hollings Marine Laboratory in Charleston, SC.

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STATEMENT OF WORK

CHEMICAL AND BIOLOGICAL WASTE DISPOSAL

NATIONAL CENTERS FOR COASTAL OCEAN SCIENCE

NOAA Hollings Marine Laboratory

Background:

NCCOS Charleston Hollings Marine Laboratory (HML) is a collaboration among five partners; NOS, the Medical University of South Carolina, National Institute of Standards and Technology, College of Charleston, and South Carolina Department of Natural Resources. The facility produces wastes from marine research processes involved with providing science and biotechnology applications to forecast, sustain, protect, and restore coastal ecosystems, with emphasis on links between environmental condition and the health of marine organisms and humans, chemical, molecular, toxicological, microbiological, and marine mammal research used to describe, evaluate, and predict natural and human influences on marine and estuarine habitats.

This includes interdisciplinary research to resolve issues related to coastal ecosystem health, environmental quality, and related public health impacts. Research at HML is focused in the following core areas: genomics; environmental chemistry and toxicology; and pathogen source tracking, monitoring, and assessment.

Purpose This statement of work covers requirements to remove chemical and biological wastes at the NOAA Hollings Marine Laboratory located in Charleston, SC. The facility is a research laboratory owned and operated by the U.S. Department of Commerce, National Oceanic and Atmospheric Administration (NOAA), National Ocean Service (NOS), National Centers for Coastal Ocean Science (NCCOS). The laboratory is an EPA “Small Quantity” Generator of chemical wastes that also generate biological materials from various marine and wildlife research processes and are legally held to uphold state and federal EPA and other environmental code requirements for the disposal of chemical and biological wastes.

NOAA's Environmental, Safety, and Sustainability Office (NESSO) establishes NOAA's policy to ensure compliance with regulatory, internal, and drive toward continuous improvement in Environment, and Sustainability performance. Environmental guidance requires NOAA facilities to conduct business in the most environmentally responsible manner possible, including the generation and disposal of chemical and biological wastes. To limit environmental liability and maximize environmental sustainability, the preferred method of disposal of all NCCOS generated waste is to recycle/reclaim/recover whenever possible. When recycling is not possible, to dispose of chemical and biological materials using fuels blending by cement kilns, and lastly disposed of by a waste to energy process as fuel for beneficial incineration. NO waste is permitted to be disposed of by burial, ground injection, landfill, unauthorized or illegal means, or shipped outside the United States. All wastes removed from the facilities must be handled according to applicable local, state, and federal regulations.

Location of Work:

The Hollings Marine Laboratory (HML) campus is located at 331 Fort Johnson Rd., Charleston, SC 29412.

Client Information:

The customer is identified as the National Centers for Coastal Ocean Science (NCCOS), Hollings Marine Laboratory (HML) represented by Randy Grady, NCCOS Facilities Operations Chief and Eric Skinner, Safety Officer at HML.

Central Contractor Registration:

1. In order to comply with the Debt Collection Improvement Act of 1966, all Contractors must be registered in System for Award Management (SAM) to be considered for an award of a federal contact. Information regarding registration in SAM can be found at https://www.sam.gov.

2. The Contractor must note on the quotation if credit cards are an accepted method of payment.

3. The Contractor must include their DUN and Bradstreet Number with their bid proposal.

4. The Contractor must have their online Representations and Certifications (Reps & Certs) completed.

5. The Contractor must have a unique entity identifier used in SAM.gov. New entities can get their Unique Entity ID at SAM.gov and, if required, complete and entity registration.

Contractor Requirements:

In accordance with the FAR 9.103 and 9.104, the Contracting Officer shall make a determination of responsibility. The Contract Officer shall take inconsideration the following factors, while making the determination:

1. Proof of and assurance that the Contractor can provide the service promptly or within the time specified, without delay or interference.

2. The selected Contractor and subcontractor(s) must show documented competency and experience with:

· Hazardous waste disposal associated with laboratory, commercial, institutional, medical and /or academic facilities

· The Contractor has been in business for at least 10 years.

· The Contractor has successfully performed federal government projects in the past.

3. The Contractor shall perform the work with trained, skilled, professional technicians who are familiar with this scope of work.

4. The quality of performance of previous contracts and services will be considered.

5. In performing this work, the Contractor shall comply with all applicable federal, state and local laws and regulations, which includes building and energy codes.

6. The Contractor must have, at the time of proposal, all applicable license and/ or registrations as required under the laws of the federal government, State of South Carolina and local ordinances for the performance of work under this agreement.

Site Visit: Contract - (843) 790-3381 - eric.skinner@noaa.gov

1. The Contractor and subcontractors are highly encouraged to attend a site visit at the Hollings Marine Laboratory (HML) to fully understand the complexities of the project.

2. Prior to the site visit/review, the Contractor is to sign-in at the front desk located on the main entrance of HML.

3. During the site visit, the contractor and subcontractors will have the opportunity to review the architectural and engineering drawings pertaining to the scope requirements, and inspect locations around the facility where the work and upgrade are proposed.

4. The Facility Manager and pertinent government personnel will be available to answer any questions, however any changes or new information will be documented and submitted in writing for official purposes.

OBJECTIVES

To provide quarterly (once every 90 days) services to properly and legally dispose of all chemical, biological, and universal wastes generated by the NCCOS Charleston, SC facility. The entirety of wastes for disposal are identified in the thousands of chemicals specifically listed in the 2021 DOT Transportation Regulations 49 CFR Part 172.101 Hazardous Materials Table pages 157-310. For legal purposes of this contract, these chemical wastes are generically identified by official DOT hazard classes or Division as: Class 1 Explosives; Class 2 Flammable, Non-flammable, and Poison Gases; Class 3. Flammable Liquids; Class 4. Flammable solids, Spontaneously Combustible, and Dangerous When Wet; Class 5. Oxidizers; Class 6. Poison, Toxic, and infectious Substances; Class 7. Radioactive; Class 8. Corrosives; Class 9 Miscellaneous Hazardous Materials. Universal wastes including hazardous waste batteries, Mercury-containing equipment, pesticides, and lamps. All specific chemicals for disposal by the generator under this contract are found within these classes and divisions and otherwise are not able to be specifically identified by proper shipping name until generated and requesting a pickup. General information regarding typical chemicals for disposal are identified later in this document.

Wastes shall be disposed of by the following prioritized list of disposal methods:

1. recycling/reclaiming/recovery, 2. fuels blending, 3. waste to energy process, or 4. other recognized methods of beneficial reuse wherever possible to maintain the highest level of NCCOS commitment to environmental management.

Failure to adhere to agreed contract terms and conditions may result in contract termination.

A minimum of five (5) years’ experience in hazardous waste pickup, transport, management and disposal with a clean and unblemished environmental record from the applicable US and state EPAs is required. This contract requires the successful vendor to own and operate a regulatory compliant Transportation, Storage, and Disposal facility (TSDF). Due to federal environmental regulations for NOAA facilities, brokers will not be considered for this contract. Contractors shall submit past performance information, evidence of business experience, current insurance documents, EPA permits, notification of environmental or safety regulatory deficiencies within the past five years, and appropriate audit letters with bid package. Upon determination by the EH&S contact listed for the facility, prospective bidders are invited to visit the NCCOS site where services are to be performed to satisfy themselves regarding general and local conditions that may affect the cost of contract performance under the terms of this Statement of Work. A site request may be made of the EH&S contact listed for the facility. It is the Contractor’s responsibility to confirm existing conditions. Failure to determine existing conditions will not be considered a basis for the granting of additional compensation.

SCOPE

The Contractor shall furnish all labor, services, and associated materials to package and label for transport, manifest, remove from the facility and properly, legally dispose of assigned chemical wastes in a timely manner, and provide prompt certificates of destruction for all hazardous wastes – including reporting summary of wastes removed from the facility and their disposal/treatment status. The Federal Government shall not provide any labor or components to fulfill the terms of this contract; however, NCCOS reserves the right to audit any and all facilities of the selected Contractor and Subcontractors.

Chemical / Biological Waste Inventories are included as Attachment A

GENERATOR BACKGROUNDS AND CONTACTS

EH&S Contact:

Eric Skinner HML Safety Officer

(843) 790-3381 eric.skinner@noaa.gov

CONTRACT REQUIREMENTS/TASKS

The Contractor shall provide all services necessary for the manifesting, bulking, packing, labeling, transport and final disposal of chemical, biological, universal, sharps, and medical wastes generated by the NCCOS Hollings Marine laboratory on a quarterly basis.

Task includes providing prompt certificates of destruction for all hazardous wastes, including the annual reporting summary of wastes removed from each facility and their disposal/treatment status for facility documentation and their use in filing EPA Biennial Reports. Frequency of disposal is expected to be every 90 days or less for each facility. All procedures involved with the disposal shall be in accordance with applicable local, state and federal policies, laws and regulations and the NCCOS EMS. Contractor will transport and dispose of wastes in bulk or as lab packs filled observing all DOT 49 CFR Transportation regulations, and according to hazard class and compatibility. Properly trained and certified or licensed employees of the contract vendor shall provide all contract services. The services shall include all personnel, equipment, labor, transportation, placarding, packaging, manifesting, temporary permits, analysis (if needed) and compilation and submission of all documentation including but not limited to properly prepared shipping documents, land bans, invoices, and a container inventory listing each container any consolidation information, information on where each container shipped, and the ultimate information on destruction (location, date, method, etc.). Total quantities listed on DOT manifests must accurately reflect proper compatibility and quantity of chemicals in a drum. All quantities are to be listed by weight. For customary EPA reporting purposes, Contractor shall list individual hazardous waste quantities shipped as weight of the waste only (total weight less weight of the drum). Accurate portable scales for weighing waste containers are to be provided on each transport vehicle used by Contractor.

Final disposal of bulk solvent waste streams shall be solvent reclamation by distillation or fuels blending by an NCCOS approved cement kiln. Final disposal of lab packs and other hazardous and nonhazardous wastes are to be consolidated and disposed of at approved facilities by the following order of priority: reclaimed, recycled, or recovered wherever possible, fuels blending at cement kilns, or fuel for waste to energy incinerators. Wastes shall be neutralized and then fuels blended or used in a waste to energy incineration process when either of the preferred disposal methods is not possible. Wastes are not permitted to be disposed of by: landfill, deep well injection methods, or at facilities outside the United States mainland. Wastes from NCCOS shall be sent only to disposal facilities that are in full compliance with federal, state, and local regulations. Contractor shall work with each NCCOS facility to recommend improvements in waste management and destruction technology that allows NCCOS to maintain the highest level of environmental management. Any and all permits, licenses or related fees are the responsibility of the Contractor.

Prior to disposal, the Contractor will be notified via telephone or email by the laboratory Environmental Health and Safety (EH&S) contact to negotiate a pickup date, followed by an email of the waste inventory to be removed. NOAA labs may add additional items for pickup until 48 hours prior to any pickup or at the time of pickup if additional items fall into an approved waste stream container. Prior to removal of any waste from an NCCOS facility, copies of the current annual vehicle inspection and commercial driver’s license with HAZMAT endorsement for the driver must be provided to the local onsite EH&S coordinator. This is mandatory for any vehicle used to remove wastes from an NCCOS site. Transport of waste from a facility will not be permitted until full compliance is met.

Contractor shall provide DOT-approved drums in good condition for shipping and the bulking or lab packing of wastes as needed. All activities shall be performed according to OSHA, EPA, RCRA, DOT, and all other applicable Federal, State, and local regulations. The Laboratories shall not furnish any equipment or personnel in performance of the Contractor’s responsibilities under this proposal and subsequent contract. Additionally, NCCOS does not warrant that waste holding containers are suitable for transport in accordance with DOT regulations; the Contractor will determine the need for container repacking or overpack based on the site visit.

When performing pickup at NCCOS facilities, the submission of the following shall apply:

Final signed manifests/or shipping papers.

Land disposal notifications.

Packing lists Detailed original signed Certificates of Destruction (COD) from final disposal site on Company letterhead (see COD requirements below) Copies of Contractor invoice and signed original CODs from the ultimate disposal facility must be submitted electronically to the local EH&S contact person. The CODs must be received from the final disposal facility in a timely manner.

Copies of all the above papers shall be submitted electronically to the Contracting Officer along with the original invoice

The pricing sheet included in this bid package sets forth the combination of costs to be evaluated. The best value responsive bidder will be determined by calculating all quotes requested on the bid form based upon previous annual disposal quantities. Failure to complete the bid form completely or correctly or the submission of disposal facilities that do not meet NOAA/NCCOS approval may result in declaring the bid non-responsive. Requesting a bid quote by Generator does not obligate NCCOS to use the services quoted.

Although every effort is made here, to clarify items generated as reasonably accurate, some variations are possible, from time to time based on DOT 49 CFR Part 172.101 Hazardous Materials Table and the EPA/RCRA standards.

DELIVERABLES

The Contractor shall furnish with bid submittal information establishing that Contractor is appropriately: licensed, permitted, and insured for the transport and temporary storage of hazardous waste involved in this contract and a list of intended temporary and final disposal sites for each category of waste. In the case of subcontracting work (Fuels Blending, Recycling, etc.), the primary Contractor shall provide proof of licensing, permits, insurance, and list of intended final disposal sites of all Subcontractors before contract execution. NCCOS reserves the right of refusal of any disposal site(s) or to request alternate disposal site(s). Only sites approved by the NCCOS and NOAA Environmental Compliance Officers will be allowed. Use of a disposal facility that is not on the Contractor’s list provided at bid time, or the use of unapproved disposal methods shall be cause for contract termination and forfeiture of payment(s) from NCCOS. A written request submitted to NCCOS (attention Ron Gagnon, with copy to the Contracting Officer) shall be required for NOAA to approve a new temporary storage or final disposal site. No changes may be made to this contract without written approval of the Contracting Officer.

Original copies of signed manifests from the designated disposal facility shall be mailed by the designated facility and received by the Generator within the required 30-day EPA time limit. If original manifest copies are required to be supplied to Generator and ship to states, the Contractor must mail by certified return receipt requested with the original return receipt returned to the Generator for their audit records.

Certificates of Final Destruction (COD) or Recycling (COR) are required for each manifested waste pickup. The certificates must specify the Generator facility, original manifest number, container identification number, contents, date of destruction, location of destruction facility, and method(s) of destruction/recycling. Certificates must be received by the Generator within 120 days of removal from an NCCOS Lab or within 30 days of waste destruction. Also, a written statement indicating that wastes are being handled in accordance with all local, state, and federal regulations and will be properly disposed of is appreciated, but does not meet the requirement of a COD or COR. An annual report shall be submitted to each laboratory contact detailing wastes disposed of at each pickup for the calendar year, final disposal process, disposal facility, and date of final destruction. These reports are expected by January 31 of each year so the data can be used to meet EPA Biennial Report requirements. Any outstanding submission for more than 12 months may result in termination of contract. In addition, any investigative work encountered on the part of NCCOS to procure these documents, may be invoiced to the Contractor.

A digital written report for each facility in a format usable for cutting and pasting to meet EPA biennial reporting requirements is required. In addition to requirements for EPA biennial reporting, written reports minimally shall summarize in table format the amount and type of wastes removed during the calendar year, waste manifest numbers, the extent of conformance with recycling/reuse/reclamation disposal objectives for EMS reporting, and graphic representation for each facility, and a combined NCCOS level report, to indicate the success of the NCCOS requirement to handle wastes in the most environmentally friendly manner with opportunities for improvement.

Note: Please provide a sample report for EPA biennial reporting requirements, adjusted to locality, in your submittal package.

Summary of Deliverables

The bid request should include the following:

Contractors shall submit past performance information, evidence of business experience, current insurance documents, EPA permits, notification of environmental or safety regulatory deficiencies within the past five years, and appropriate audit letters with bid package.

Proof that the contractor is appropriately: licensed, permitted, and insured for the transport and temporary storage of hazardous waste involved in this contract and a list of intended temporary and final disposal sites for each category of waste.

In case of subcontracting work, the primary Contractor shall provide proof of licensing, permits, insurance, and list of intended final disposal sites of all Subcontractors before contract execution.

A sample annual report for EPA biennial reporting requirements, adjusted to locality.

A completed pricing sheet

Summary of Specific Requirements/Tasks:

Contractor will transport and dispose of wastes in bulk or as lab packs filled observing all DOT 49 CFR Transportation regulations, and according to hazard class and compatibility The services shall include all personnel, equipment, labor, transportation, placarding, packaging, manifesting, temporary permits, analysis (if needed) and compilation and submission of all documentation including but not limited to properly prepared shipping documents, land bans, invoices, and a container inventory listing each container any consolidation information, information on where each container shipped, and the ultimate information on destruction (location, date, method, etc.).

Original copies of signed manifests from the designated disposal facility shall be mailed by the designated facility and received by the Generator within the required 30-day EPA time limit Certificates of Final Destruction (COD) or Recycling (COR) are required for each manifested waste pickup.

A written statement indicating that wastes are being handled in accordance with all local, state, and federal regulations and will be properly disposed of is appreciated, but does not meet the requirement of a COD or COR.

An annual report shall be submitted to each laboratory contact detailing wastes disposed of at each pickup for the calendar year, final disposal process, disposal facility, and date of final destruction. These reports are expected by January 31 of each year so the data can be used to meet EPA Biennial Report requirements.

SECURITY REQUIREMENTS

The Assessment and Authorization (A&A) requirements of Clause 48 CFR 1352.239-72 do not apply, and a Security Accreditation Package is not required.

The contractor will not access, store, process or transmit any government privileged information. The contractor will not have access to any non-public government systems or networks.

PERIOD OF PERFORMANCE

The period of performance for this contract is a reoccurring requirement.

HOURS OF OPERATION

Contractor employees shall generally perform all work during normal business hours, Monday through Friday (except Federal holidays). However, there may be occasions when Contractor employees shall be required to work other than normal business hours, including weekends and holidays, to fulfill requirements under this SOW. Prior to each disposal, the Contractor will be notified via telephone or email by the laboratory EH&S contact to negotiate a pickup date, followed by an email of the waste inventory to be removed.

GENERAL REPORT REQUIREMENTS

A report shall be submitted to each laboratory contact detailing wastes disposed of at each pickup for the calendar year, final disposal process, disposal facility, and date of final destruction. These reports are expected by January 31 of each year so the data can be used to meet EPA Biennial Report requirements. The report must be a digital written report for each facility in a format usable for cutting and pasting to meet EPA biennial reporting requirements is required.

In addition to requirements for EPA biennial reporting, written reports minimally shall summarize in table format the amount and type of wastes removed during the calendar year, waste manifest numbers, the extent of conformance with recycling/reuse/reclamation disposal objectives for EMS reporting, and graphic representation for each facility, and a combined NCCOS level report, to indicate the success of the NCCOS requirement to handle wastes in the most environmentally friendly manner with opportunities for improvement.

GOVERNMENT FURNISHED RESOURCES

The Government will not furnish any resources to the Contractor in support of this contract.

CONTRACTOR FURNISHED PROPERTY

The Contractor shall furnish all facilities materials, equipment and services necessary to fulfill the requirements of this contract.

GOVERNMENT ACCEPTANCE PERIOD

The COR will review deliverables prior to acceptance and provide the contractor with an e-mail that provides documented reasons for non-acceptance. If the deliverable is acceptable, the COR will send an e-mail to the Contractor notifying it that the deliverable has been accepted.

A. The COR will have the right to reject or require correction of any deficiencies found in the deliverables that are contrary to the information contained in the Contractor’s accepted proposal. In the event of a rejected deliverable, the Contractor will be notified in writing by the COR of the specific reasons for rejection. The Contractor may have an opportunity to correct the rejected deliverable and return it per delivery instructions.

ENVIRONMENTAL COMPLIANCE

Work must be completed observing all federal, state, and local laws and regulations and environmental compliance requirements, including applicable permitting requirements. Environmental compliance may include but is not limited to the National Environmental Policy Act, Endangered Species Act, Clean Water Act, National Historic Preservation Act, Essential Fish Habitat Provisions of the Magnuson- Stevens Act, Resource Conservation and Recovery Act (RCRA), etc.

Attachment A:

Item Quantity in Container (approx)

Container type & size

Containers

Total Quantity

Unit of Measure

Saltmarsh mud with seawater #2 fuel oil
55 gal
55 gal drum
6
330
gal
Saltmarsh mud with seawater #2 fuel oil
30 gal
30 gal drum
2
60
gal
Seawater #2 fuel oil
55 gal
55 gal drum
1
55
gal
NHS
25 g
25 g glass container
1
25
mL
NSB reducer with Sodium azide
10 mL
10 mL plastic container
2
80
mL
Acid Waste
15 gal
15 gal poly drum
1
15
gal
non-chlorinated solvent
30 gal
30 gal poly drum
1
30
gal
Ethanolamine
80 mL
100 mL pyrex jar
1
80
mL
EDC
4 g
5 g glass container
2
8
g
PBS AF3 solution
25mL
25 mL glass container
1
25
mL
Diethyl Pyrocarbonate
25 mL
25 mL glass container
1
25
mL
NHS
25 g
25 g glass container
1
25
g
NHS
115 g
115 g glass container
1
115
g
HEPES/CTAB
400 mL
Glass Jar
1
400
mL
B-mercaptoethanol
150 mL
glass jar
1
150
mL
Ethanol
5 gal.
5 gal. poly drum
1
5
gal
Chloroform
5 gal.
5 gal. poly drum
1
5
gal
Acid waste >10% nitric and hydrochloric
15 gal.
15 gal poly drum
2
15
gal
Isopropyl Alcohol
5 oz.
11 metal cans
2
11
oz.

Amoxicillin (500 mg/L), Dinotefuran (1ug/100ul), Thiamethoxamine (1ug/100ul), Acetamiprid (1ug/100ul) in seawater

2 liters

4 L glass amber jug

L

Formalin
4 liters
4 L glass amber jug
1
4
L
Acetone
4 liters
4 L glass amber jug
2
8
L
30% Acrylamide bis-acryl
100 ml
100 ml plastic bottle
6
600
ml
DNA Extractor TIS kit: alcohol solution
30 ml
50ml glass bottle
1
30
ml

DNA Extractor TIS kit: sodium iodide solution

15 ml

30 ml glass bottle ml

DNA Extractor TIS kit: oxidation inhibitor
300 ul
1.5 ml eppendorf tube
1
300
ul
Formamide
100 ml
100 ml glass bottle
6
600
ml

30% Electrophoresis Reagant: acrylamide / bis-acrylamide

100 ml

100 ml plastic bottle ml

Nickle-Metal Hylide batteries
2
plastic bag
1
2
batteries
Dimethyl sulfoxide
1 ml
centriguge tube
4
4
ml
Proprietary mutagen
1ml
centrifuge tube
1
1
ml
Acetamiprid
100mg
glass vial
1
100
mg
Bifenthrin
100 mg
glass vial
1
100
mg
70 % Isopropanol
4 Liters
4 L glass amber jug
1
4
liters
55w 4ft T-5 fluorecent light bulbs
ea
ea
10
10
light bulbs
Copper (I) oxide
500 g
plastic bottle
1
450
g
Potassium Chloride
500 g
plastic bottle
1
450
g
Ammonium acetate
500 g
plastic bottle
1
400
g
Sodium nitrate
250 g
plastic bottle
1
200
g
Chlorinated
4 liter
4-L glass bottle
12
48
L
Non chlorinated
4 liter
4-L glass bottle
5
12
L
Chlorinated
5 gal
5 gal metal drum
4
15
gal
forming foams)
30 gal
30 gal poly drum
3
90
gal
forming foams)
50 gal
55 gal poly drum
6
300
gal
Phenol/trizol/Ethanol
500 mL
glass 500 mL
1
1
mL
biohazard MiSeq Cartridges
7
Plastic cartridges with Fo
1
1
lg bag

assorted FF-AFFs (fluorine free - aqueous film-forming foams)

15 gal
15 gal poly drum
1
15
gal

assorted FF-AFFs (fluorine free - aqueous film-forming foams)

55 gal
55 gal poly drum
1
55
gal

Acetone (40%), Methanol (40%), Acetonitrile (10%), 25% aqueous pyridine (10%)

4.5 L
Amber glass bottle
7
31.5
L

Acetone (40%), Methanol (40%), Acetonitrile (10%), 25% aqueous pyridine (10%)

3 L
Clear glass bottle
2
6
L

Acetone (50%), Methanol (35%), Acetonitrile (8%), 25% aqueous pyridine (7%)

4.5 L
Amber glass bottle
1
4.5
L

Acetone (40%), Methanol (40%), Acetonitrile (10%), 25% aqueous pyridine (10%)

20 L
20 L poly drum
1
20
L
Methanol (80%), Acetone (20%)
2.5 L
Clear glass bottle
1
2.5
L

Sulfuric acid (20%), 2% Resorcinol (<1%), water (80%)

2.5 L
Clear glass bottle
2
5
L

Sulfuric acid (20%), 2% Resorcinol (<1%), water (80%)

4 L
Plastic bottle
1
4
L

Sulfuric acid (20%), 2% Resorcinol (<1%), water (80%)

2.5 L
Plastic bottle
1
2.5
L

Ammonium Molybdate (2%), Sulfuric acid (5%), Ascorbic acid (2%), Potassium antimonyl tartrate

4 L
Amber glass bottle
1
4
L

Ammonium Molybdate (2%), Sulfuric acid (5%), Ascorbic acid (2%), Potassium antimonyl tartrate

4.5 L
Plastic bottle
1
4.5
L

Ammonium Molybdate (2%), Sulfuric acid (5%), Ascorbic acid (2%), Potassium antimonyl tartrate

2.5 L
Glass bottle
1
2.5
L

2-propanol (95%), UV resin (contains polychloro copper phthalocyanine; 5%)

4 L
Plastic bottle
2
8
L

2-propanol (90%), UV resin (contains polychloro copper phthalocyanine; 10%)

4.5 L
Plastic bottle
2
9
L
Iodine potassium iodide (1%), Seawater (99%)
4.5 L
Amber glass bottle
1
4.5
L
Iron (III) Chloride
500 g
Plastic tub
1
500
g
non-chlorinated
15 gal
15 gal poly drum
1
15
gal
carbon tetrachloride
1 L
sealed container
1
1
L
methylamine
100 ml
glass bottle
1
100
ml
ethylene glycol
100 ml
glass bottle
1
100
ml
4-bromobenzoy lchloride
10 g
glass bottle
1
10
gal
bromine 1M
100 ml
glass bottle
1
100
ml
oleamide
100 mg
plastic bottle
2
200
mg
oxone monopersulfate
5 g
glass bottle
1
5
g
piperazine
5g
glass bottle
1
5
g
dihydroethidium
2 packs of

10mg

vials
2
20
mg
Diazald
500 g
plastic bottle
1
500
g
ammonium acetate
500 g
plastic bottle
1
500
g
MSTFA
10- 1 ml
vials
1
10
ml
FMOC-Cl,-9-fluorenylmethyl
5 g
glass bottle
1
5
g
o-tolidine
100 g
glass bottle
1
100
g
potassium dioxide
50 g
glass bottle
1
50
g
Diazald
25 g
plastic bottle
1
25
g
dihydroethidium
10 mg
vials
2
20
mg
nifedipine
1 g
glass bottle
1
1
g
phenyl isothiocyanate
5g
glass bottle
1
5
g
proteinase
100 mg
glass bottle
1
100
mg
methoxy tritluoro methyl
100 mg
glass bottle
2
200
mg
9-chloromethyl-anthracene
5 g
glass bottle
1
5
g
thiazolyl blue
500 mg
glass bottle
1
500
mg
diazald
25 g
plastic bottle
1
25
g
toluene sulfonic acid
5 g
glass bottle
1
5
g
disopropylamine
50 g
glass bottle
1
50
g
idomethane
100 g
glass bottle
1
50
g
perfluoroctannoic acid
5g
glass bottle
1
5
g
sebacoyl chloride
50 g
glass bottle
1
50
g
trifluoroacetic acid
50 ml
glass bottle
4
200
ml
formic acid
1L
plastic bottle
1
750
ml
nitric acid
1.5 L
plastic bottle
1
1.5
L
phosphoric acid
500 ml
glass bottle
1
500
ml
sulfuric acid
2.5 L
glass bottle
1
2.5
L
Nitric acid
500 ml
plastic bottle
1
500
ml

LC-MS waste containg about 30% acetonitrile, 15% methanol, 5% isopropanol, 50% water and less than 0.1% formic acid

4.25 gallon

5 gallon plastic bottle

4.25 gallon

Formalin (10%)
500 ml
1 qt plastic bucket
1
1
mL
ethanol
20000 ml
5 gallon plastic container
1
1
mL
alcohol-formol-acetic (AFA)
500 ml
500 mL plastic container
1
1
mL
sharps container
1 qt of used

sharps

1 qt plastic bucket
1
1
qt

Lab Pac Items Not Typical

Umbelliferon (flourescence indicator) (7- hydroxycoumarin)
10 g
plastic vial
1
1
g
Fluram (Fluorescamine)
1 g
glass vial
3
3
g
7-Ethoxycoumarin
100 mg
glass vial
2
200
mg

Tris(4,7-diphenyl-1,10- phenanthroline)ruthenium(II) bis(hexafluorophosphate) complex

1 mg plastic bottle mg

Fluram (Fluorescamine)
100 mg
glass bottle
1
100
mg
Trypan Blue (Cell Culture Tested)
5 gal
plastic bottle
1
5
g
3,4,4’ - trichlorocarbanilide (99%)
100 g
glass bottle
1
100
g
Glucose (D-(+) anhydrous)
250 g
plastic bottle
1
250
g
Oxytetracycline hydrochloride
10 g
glass bottle
2
20
g
Aprotinin
10 mg
glass bottle
5
25
g
Albumin
10 g
glass bottle
1
10
g
Fluorograde antifad reagent
5 mL
glass bottle
1
5
ml
FBS
100 mL
glass bottle
1
100
ml
Triolzin STDS chloroform and isoamyl
5 mL
glass bottle
1
5
ml
Ribonucleic Acid
100 mg
glass bottle
1
100
mg
Leupeptin hydrochloride
5 mg
glass bottle
3
15
mg
Luciferin multicyp
3 mg
plastic vial
1
3
mg
PFOS in seawater (99% seawater)
30 gal
15 gal Poly drum
1
30
gal
fluroscent bulbs
6 bulbs
glass
6
6
stick
BioRad protein reagent (50% phosphric acid; 25% methanol)
450 mL bottle
plastic bottle
2
900
ml
dead batteries
various

button and

plastic bag
25
various

size various size

SRM 3154 Sulfur Solution (10 mg/g of element in 10% Nitric Acid)

20mL

3"x4" Cardboard Box mL

SRM 3113 Cobalt Solution (10 mg/g of element in 10% Nitric Acid)

40mL

3"x4" Cardboard Box mL

SRM 3151 Silver Solution (10 mg/g of element in 10% Nitric Acid)

20mL

3"x4" Cardboard Box mL

SRM 3154 Sulfur Solution (10 mg/g of element in 10% Nitric Acid)

50mL

3"x4" Cardboard Box mL

SRM 3154 Sulfur Solution (10 mg/g of element in 10% Nitric Acid)

20mL

3"x4" Cardboard Box mL

SRM 3133 Mercury Solution (10 mg/g of element in 10% Nitric Acid)

40mL

3"x4" Cardboard Box mL

SRM 3128 Lead Solution (10 mg/g of element in 10% Nitric Acid)

30mL

3"x4" Cardboard Box mL

SRM 3165 Vanadium Solution (10 mg/g of element in 10% Nitric Acid)

50mL

3"x4" Cardboard Box mL

SRM 3109a Calcium Solution (10 mg/g of element in 10% Nitric Acid)

20mL

3"x4" Cardboard Box mL

SRM 31xx Tellurium Solution (10 mg/g of element in 10% Nitric Acid)

40mL

3"x4" Cardboard Box mL

SRM 3160a Thulium Solution (10 mg/g of element in 10% Nitric Acid)

30mL

3"x4" Cardboard Box mL

SRM 3112a Chromium Solution (10 mg/g of element in 10% Nitric Acid)

40mL

3"x4" Cardboard Box mL

SRM 3153a Strontium Solution (10 mg/g of element in 10% Nitric Acid)

20mL

3"x4" Cardboard Box mL

SRM 3184 Bromide Solution (10 mg/g of element in 10% Nitric Acid)

30mL

3"x4" Cardboard Box mL

SRM 3113 Cobalt Solution (10 mg/g of element in 10% Nitric Acid)

40mL

3"x4" Cardboard Box mL

SRM 3103a Arsenic Solution (10 mg/g of element in 10% Nitric Acid)

50mL

3"x4" Cardboard Box mL

SRM 3139a Phosphorus Solution (10 mg/g of element in 10% Nitric Acid)

20mL

3"x4" Cardboard Box mL

SRM 3132 Manganese Solution (10 mg/g of element in 10% Nitric Acid)

40mL

3"x4" Cardboard Box mL

SRM 3103 Arsenic Solution (10 mg/g of element in 10% Nitric Acid)

40mL

3"x4" Cardboard Box mL

SRM 3157a Terbium Solution (10 mg/g of element in 10% Nitric Acid)

30mL

3"x4" Cardboard Box mL

SRM 3147a Samarium Solution (10 mg/g of element in 10% Nitric Acid)

40mL

3"x4" Cardboard Box mL

SRM 3116a Erbium Solution (10 mg/g of element in 10% Nitric Acid)

20mL

3"x4" Cardboard Box mL

SRM 3166a Ytterbium Solution (10 mg/g of element in 10% Nitric Acid)

40mL

3"x4" Cardboard Box mL

SRM 3151 Silver Solution (10 mg/g of element in 10% Nitric Acid)

10mL

3"x4" Cardboard Box mL

SRM 3158 Thallium Solution (10 mg/g of element in 10% Nitric Acid)

40mL

3"x4" Cardboard Box mL

SRM 3115a Dysprosium Solution (10 mg/g of element in 10% Nitric Acid)

20mL

3"x4" Cardboard Box mL

SRM 3185 Nitrate Solution (10 mg/g of anion in 10% Nitric Acid)

10mL

3"x4" Cardboard Box mL

SRM 3135a Neodymium Solution (10 mg/g of element in 10% Nitric Acid)

20mL

3"x4" Cardboard Box mL

SRM 1641d Mercury Solution (10 mg/g of element in 2% Nitric Acid)

40mL

3"x4" Cardboard Box mL

SRM 3110 Cerium Solution (10 mg/g of element in 10% Nitric Acid)

30mL

3"x4" Cardboard Box mL

SRM 3127a Lanthanum Solution (10 mg/g of element in 10% Nitric Acid)

30mL

3"x4" Cardboard Box mL

SRM 3121 Gold Solution (10 mg/g of element in 10% Hydrochloric Acid)

20mL

3"x4" Cardboard Box mL

SRM 3138 Palladium Solution (10 mg/g of element in 10% Hydrochloric Acid)

30mL

3"x4" Cardboard Box mL

SRM 3162a Titanium Solution (10 mg/g of element in 10% Nitric Acid)

50mL

60 mL Plastic Bottle mL

SRM 3114 Copper Solution (10 mg/g of element in 10% Nitric Acid)

50mL

60 mL Plastic Bottle mL

SRM 3137 Niobium Solution (10 mg/g of element in 10% Nitric Acid)

50mL

60 mL Plastic Bottle mL

10% Formic Acid Solution

900mL

1 L Plastic Bottle mL

Previous Quarter Turn-in

Dicholormethane/Hexane 90%/10%
4L
4 L Glass bottle
4
16
L
Dicholormethane 100%
4L
4 L Glass bottle
18
192
L
Dichloromethane/Methanol 50%/50%
4L
4 L Glass bottle
2
8
L
Methanol/ Water 50%/50%
4 L
4 L Glass bottle
1
4
Lt
25%/25%/25%/25%
4L
4 L Glass bottle
6
24
L
Seawater/Formalin 95%/5%
4L
4 L Glass bottle
1
4
L
Dichloromethane/Acetone 90%/10%
4L
4 L Glass bottle
1
4
L
Methane/Acetone/Hexane 33%/33%/34%
4L
4 L Glass bottle
1
4
L
Non-Chlorinated Spent Waste
4L
4 L Glass bottle
2
8
L
10% Buffered Formalin/DI Water 5%/95%
4L
4 L Glass bottle
3
12
L
Chloroform
5Gal
5 Gal Poly Bottle
3
15
Gal

Oily Waste Filters

3 Filters sealed Hazardous waste bag

Filters

Acetone/Methanol 50%/50%
4L
4 L Glass bottle
2
8
L
Acetone
4L
4 L Glass bottle
1
4
L
Ethyl Acetate 100%
4L
4 L Glass bottle
8
32
L
Hexane
4L
4 L Glass bottle
1
4
L
Ethyl Acetate/Acetone/Methanol 33%/33%/33%
4L
4 L Glass bottle
1
4
L
Ethyl Acetate/Hexane 50%/50%
4L
4 L Glass bottle
3
12
L
Ethyle Acetate/Methanol 50%/50%
4L
4 L Glass bottle
2
8
L
Ethyle Acetate/Hexane/Methanol 30%/30%/30%
4L
4 L Glass bottle
1
4
L
Methylene/Chloride Waste
4L
4 L Glass bottle
4
16
L
Dichloromethane/Seawater
4L
4 L Glass bottle
1
4
L
Assorted FF-FFF/Seawater/Deionized Water
15Gal
15 Gal Poly Drum
2
30
Gal
Seawater/Crude Oil
5Gal
5 Gal Poly Bottle
2
10
Gal
Sulfosalicyic Acid/Hydrochloric Acid
4 L
4 L Glass bottle
1
4
L
Tetraetraxypropane/Thiobarbituratic
4 L
4 L Glass bottle
1
4
L
Acid/Trichloracetic Acid
4 L
4 L Glass bottle
1
4
L
Nitric Acid/ Water 20%/80%
4 L
4 L Glass bottle
4
16
L
Chrlorinated Waste
4 L
4 L Glass bottle
10
40
L
Methylene/Chloride Waste
4 L
4 L Glass bottle
1
4
L
10% Buffered Formalin/ DI Water 5%/95%
4 L
4 L Glass bottle
4
16
L
1%/99%
15Gal
15 Gal Poly Drum
1
15
Gal
foams
15Gal
15 Gal Poly Drum
3
45
Gal
Dichloromethane
5Gal
5 Gal Poly Bottle
4
20
Gal
Nitric Acid/Water 20%/80%
5Gal
5 Gal Poly Bottle
4
20
Gal
10% Nitric Acid Waste
15Gal
15 Gal Poly Drum
1
15
Gal
Spent Acetone
5Lt
4 Lt Glass bottle
1
5
Lt
Crude Oil/Seawater 1%/99%
15Gal
15 Gal Poly Drum
2
30
Gal
foams
30Gal
30 Gal Poly Drum
4
120
Gal
Zinc Chloride/DI Water/Seawater 1%/1%/98%
15Gal
15 Gal Poly Drum
2
30
Gal
Aqueous film forming foam/Seawater 1%/99%
55Gal
55 Gal Poly Drum
2
100
Gal
acid/Tetraehoxypropane
4L
4 Lt Glass bottle
1
4
L

Previous Quarter Lab Pack

Clofibric Acid
100 g
100 g container
1
100
g
Crude Oil
3 ml
3 ml container
1
3
ml
Gentamicin Sulfate
5 g
5 g container
1
5
g
Irgasan
5 g
5 g container
1
5
g
Fluoxetine Hydrochloride
10 ml
10 ml container
1
10
ml
Carbamazepine
1 g
1 g container
1
1
g
Carbamazepine
112.3 mg
112 3 mg container
1
112.3
mg
Caffeine in DMSO
1 ml
1 ml container
1
1
ml
Diclofenac Sodium
1 g
1 g container
1
1
g
Trclosan in Acetone
2 ml
2 ml container
1
2
ml
Clofibric Acid
111.8 mg
111 8 mg container
1
111.8
mg
Amoxicillin
200 mg
200 mg container
9
200
mg
Isopropanol 100%
4 L
4 L container
1
4
L
Acetone
4 L
4 L container
3
4
L
Imidacloprid/Acetamiprid/Amoxacillan/ Seawater
3.5 L
3 5 lt container
2
3.5
L
Caffine
100 mg
100 mg container
1
100
mg

Miscellaneous Waste

In addition to the above bulk waste streams, the laboratories generate miscellaneous waste on a smaller and less frequent basis which will be disposed of on an “as needed basis” at the same time as the above bulk waste streams. The entirety of these miscellaneous wastes are found in DOT 49CFR Part 172.101 Hazardous Materials Table, but are too numerous to list individually.

Universal Waste to be recycled – spent fluorescent light tubes (mostly green tipped mercury-free tubes); NiCad, lithium, alkaline, and lead acid batteries, & light ballasts.

Mercury (including mercury/mercuric compounds) and Potassium Dichromate containing materials (extremely rare occurrence) - ≤ 1 gal. yr; (mercuric solutions >35 ppm from tissue fixatives or laboratory assays, mercury contained in a manufactured item, i.e. broken thermometers, thermostats, etc.), Biological and Medical Waste (Non human tissues from marine mammals, fish and shellfish, or wildlife research, and syringes and needles) - approx. 70 lbs/yr (l case), Miscellaneous corrosives, poisons, oxidizers/reactives, flammables and non-hazardous/non- regulated lab packs from 49 CFR Part 172.101 Hazardous Materials Table

Toxic metal solutions and solids

Various wastes used in facility and vehicle maintenance including such items, but not limited to aerosol spray cans, oils, fuels, paints and adhesives.

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File details come from the government source that posted it. Updated .