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Table 1 List of pesticide active ingredients to be quantified by HRGC/HRMS

Target Pesticide

LOQ

(ng/g)

LOD

(ng/g)

Carbaryl 97.9 48.95 Malathion 3.92 1.96 Permethrin (cis) 2.09 1.96 Permethrin (trans) 3.92 1.96

4,4'‐DDT 3.92 1.96

4,4'‐DDD 3.92 1.96

4,4'‐DDE 3.92 1.96

Lindane 11.6 5.81 Heptachlor 3.92 1.96 Chlordane (cis/alpha) 3.92 1.96 Chlordane (trans/gamma) 3.92 1.96 Dieldrin 3.92 1.96 Aldrin 11.6 5.81 Endosulfan I 3.92 1.96 Endosulfan II 3.92 1.96 Endosulfan sulfate 3.92 1.96 Chlorpyrifos 15.5 7.75 Diazinon 15.5 7.75 Coumaphos 245 122.5 Carbofuran 97.9 48.95 Metolachlor 19.6 9.8 Acetochlor 97.9 48.95 Alachlor 97.9 48.95 Butylate 19.6 9.8 Atrazine 15.5 7.75 Cyanazine 15.5 7.75

EPTC 3.92 1.96

Simazine 15.5 7.75 Metribuzin 3.88 1.94 Dacthal 3.88 1.94 Chlorothalonil 7.75 3.88 Cyfluthrin 38.8 19.4

Piperonyl Butoxide 5.81 2.91

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