Attach_4_EDD_example.pdf

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BPA Setup - Analysis of Low Level Selenium
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140R2021Q0016
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Attachment 4 - Condensed to One Page

LAB_NAME LAB_REPORT_NUM LAB_REPORT_DATE LAB_SMPL_NUM SMPL_FIELD_NUM LAB_QC_BATCH_NUM

DATE_TIME_

PRESERVED

DATE_TIME_

PREPARED

DATE_TIME_

ANALYZED

SAMPLE_RESULT_S

YMBOL

SAMPLE_RESULT_

VALUE

SAMPLE_RESULT

_UNIT_NAME

American Contract Lab 18B480-04 addendum 2018-05-14 18B480-01 GBW1005 18B480GH 2018-03-14 20:18:05-7 2018-03-19 09:18:05-7 2018-04-12 10:18:05-7 < 12.4 ng/L

American Contract Lab 18B480-04 addendum 2018-05-14 18B480-02 GBW1006 18B480GH 2018-03-14 20:18:05-7 2018-03-19 09:18:05-7 2018-04-12 10:18:05-7 21.2 ng/L

American Contract Lab 18B480-04 addendum 2018-05-14 18B480-03 18B480GH 2018-03-14 20:18:05-7 2018-03-19 09:18:05-7 2018-04-12 10:18:05-7 ng/L

American Contract Lab 18B480-04 addendum 2018-05-14 18B480-04 18B480GH 2018-03-14 20:18:05-7 2018-03-19 09:18:05-7 2018-04-12 10:18:05-7 ng/L

American Contract Lab 18B480-04 addendum 2018-05-14 18B480-05 18B480GH 2018-03-14 20:18:05-7 2018-03-19 09:18:05-7 2018-04-12 10:18:05-7 ng/L

American Contract Lab 18B480-04 addendum 2018-05-14 18B480-06 18B480GH 2018-03-14 20:18:05-7 2018-03-19 09:18:05-7 2018-04-12 10:18:05-7 ng/L

ANALYTE_NAME

ANALYTE_ADDITIONAL_I

NFO_DESCRIPTION

ANALYTE_CAS

METHOD_CODE_P

REPARATION

METHOD_CODE_

EXTRACTION

METHOD_CODE_

ANALYSIS

RESULT_RL

RESULT_RL_UNIT

_NAME

RESULT_MDL

RESULT_MDL_

UNIT_NAME

SMPL_DIL_

FACTOR

LAB_QC_SMPL

_NUM

Mercury Dissolved 7439-97-6 EPA 200.8 EPA 200.8 EPA 200.8 12.4 ng/L 4.5 ng/L 1

Mercury Dissolved 7439-97-6 EPA 200.8 EPA 200.8 EPA 200.8 12.4 ng/L 4.5 ng/L 1

Mercury Dissolved 7439-97-6 EPA 200.8 EPA 200.8 EPA 200.8 12.4 ng/L 4.5 ng/L 1 18B480GH-01

Mercury Dissolved 7439-97-6 EPA 200.8 EPA 200.8 EPA 200.8 12.4 ng/L 4.5 ng/L 2 18B480GH-02

Mercury Dissolved 7439-97-6 EPA 200.8 EPA 200.8 EPA 200.8 12.4 ng/L 4.5 ng/L 2 18B480GH-03

Mercury Dissolved 7439-97-6 EPA 200.8 EPA 200.8 EPA 200.8 12.4 ng/L 4.5 ng/L 2 18B480GH-04

LAB_QA_SUBTYPE

_NAME

LAB_REPLICATE

UNSPIKED_RESULT_S

YMBOL

UNSPIKED_

RESULT_VALUE

UNSPIKED_RESULT_

UNIT_NAME

UNSPIKED_

SMPL_NUM

SPIKE_VALUE SPIKE_UNIT_NAME

SPIKE_

COMMENT

MEASURED_

RESULT_SYMBOL

MEASURED_

RESULT_VALUE

MEASURED_RESULT

_UNIT_NAME

Method Blank 1 < 12.4 ng/L

Lab Control Spike 1 40 45.3 ng/L Lab Control Spike Duplicate 2 40 42.8 ng/L

Matrix Spike 1 21.2 ng/L 18B480-02 40 ng/L Spiked before digestion 67.5 ng/L

LAB_ACCURACY

_RESULT

LAB_ACCURACY_

RESULT_L_LIMIT

LAB_ACCURACY_

RESULT_U_LIMIT

LAB_PRECISION_R

ESULT

LAB_PRECISION_

RESULT_LIMIT

LAB_CONTAMINATION

_RESULT

LAB_CONTAMINATION

_RESULT_LIMIT

LAB_QC_

COMMENT

LAB_QULFR_CODE

LAB_QULFR_

DESCRIPTION

LAB_QULFR_

ADDITIONAL_INFO

Sample broken in transit

10.2 24.8 DI water

113 80 120

107 80 120 5.68 20

116 75 125 C3 Spike > 4x background.

Background 21.2 ng/L.

EDD example

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