Appendix A-2 Cumberland_Phase1_Attachments.pdf

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Attached to
CP-24-001 Professional Services for River Park Improvements
Solicitation number
BPM043557
Issued by
Allegany County, Cumberland City, Maryland

About this file

Written by GovTribe AI ·

This document is a request for proposals from the Canal Place Preservation and Development Authority (CPPDA) for a Project Manager to oversee the River Park at Canal Place project in Cumberland, Maryland. The River Park project aims to create a whitewater park and associated amenities along the North Branch of the Potomac River, including the removal of the Cumberland Industrial Dam. The scope of work includes evaluating, proposing, and implementing plans for the dam removal, as well as the construction of in-stream whitewater features and other improvements. The project area spans approximately 1.75 miles along the river, parallel to the Chesapeake and Ohio Canal Towpath. Proposals are due by a specified date, and the selected firm will serve as the Project Manager for the duration of the project.

The document does not provide details on pricing terms, set asides, incumbents, funding requirements or sources, or other financial information. It focuses on the technical details of the project scope and the request for a qualified Project Manager to oversee its implementation.

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Other files

File Type Posted
Appendix A-5 Economic Impact Study WVU Extension Service.pdf PDF
Appendix D - Bid Proposal Affidavit.pdf PDF
Appendix C - Price Proposal.pdf PDF
Appendix A-3 Cumberland Dam Removal Letter Report.pdf PDF
Appendix A-4 190-376_RiverParkFeasibilityStudy_with_Appendix 2020.pdf PDF
Appendix B - General Contract Provisions -Project Manager.pdf PDF
Appendix E - Contract Affidavit.pdf PDF
Appendix A-6 328-386 River Park Preliminary Engineering Report_01152024_Draft.pdf PDF
Appendix A-1 CumberlandPhase1_Memo_20101109.pdf PDF
Project Mangement FIRM RFP.pdf PDF

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0 0

6.5

1.5

2.5

1.5

0.5

DAM

US-2

US-1

UPSTREAM EXTENT

OF IMPOUNDMENT

CUMBERLAND

INDUSTRIAL DAM

0 750 1,500 2,250 3,000375 Feet

File: P:\1033\Projects\1033001\GIS\MXD\SedimentProbing.mxd, May 2010, Copyright Princeton Hydro, LLC.

Sediment Sample Locations Sediment Probings (Depth - ft)

0.00 - 0.50

0.51 - 1.50

1.51 - 3.00

3.01 - 6.50

6.51 - 9.00

Project: 1033 T:1, City of Cumberland, Cumberland Feasibility Study Location: Cumberland, MD

Sample Depth % Moist. % Fines Plasticity USC Gravel USC Sand USC USC USCS

(D2216/2974) (D2974) (C117) (D4318) % Coarse % Fine % Coarse % Medium %Fine % Fines % Fineness Description Upstream, 1 0-2 30.0 NT 3.2 NT 0.0 5.2 8.0 66.8 16.9 3.2 2.4 SP - poorly graded sand Upstream, 2 0-2 33.0 NT 1.2 NT 0.0 3.6 8.0 77.9 10.5 1.2 2.5 SP - poorly graded sand

Dam, 1 0-2 26.0 NT 2.5 NT 0.0 14.9 15.1 57.4 12.6 2.5 5.0 SP - poorly graded sand

'file:///Q:/1033/Projects/1033001/Laboratory/C136_3samples.ods'#$ASTM C 136 Results

% Org.

0.010.101.0010.00100.00

GRAIN SIZE DISTRIBUTION

ASTM C136

Upstream, 1 Upstream, 2 Dam, 1

GRAIN SIZE (mm)

P E

R C

E N

T P

A S

S

IN

G

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METHODS SUMMARYMETHODS SUMMARY

C9K060597C9K060597

ANALYTICAL PREPARATION

PARAMETER__________________________________________________ METHOD_______________ METHOD_______________

Hexavalent Chromium SW846 7196A SW846 3060A Mercury in Solid Waste (Manual Cold-Vapor) SW846 7471A SW846 7471A Organochlorine Pesticides SW846 8081B PCBs by SW-846 8082A SW846 8082A Semivolatile Organics GCMS BNA 8270C SW846 8270C Total Residue as Percent Solids SM20 2540G Trace Inductively Coupled Plasma (ICP) Metals SW846 6010B SW846 3050B Trivalent Chromium Trivalent Chromium SW846 6010B WET NONE Volatile Organics by GC/MS SW846 8260B SW846 5030B

References:References:

SM20 "STANDARD METHODS FOR THE EXAMINATION OF WATER AND

WASTEWATER", 20TH EDITION."

SW846 "Test Methods for Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 and its updates.

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SAMPLE SUMMARYSAMPLE SUMMARY

C9K060597C9K060597

SAMPLED SAMP

WO #_____ SAMPLE#_______ CLIENT SAMPLE ID________________________________________________________________ DATE________ TIME_____

LN2ME 001 DAM 11/03/09

LN2MG 002 US1 11/03/09 16:00

LN2MK 003 US2 11/03/09 16:45

NOTE(S):NOTE(S):__________________________________________________________________________________________________________________________________________________________________________________________

- The analytical results of the samples listed above are presented on the following pages.

- All calculations are performed before rounding to avoid round-off errors in calculated results.

- Results noted as "ND" were not detected at or above the stated limit.

- This report must not be reproduced, except in full, without the written approval of the laboratory.

- Results for the following parameters are never reported on a dry weight basis: color, corrosivity, density, flashpoint, ignitability, layers, odor, paint filter test, pH, porosity pressure, reactivity, redox potential, specific gravity, spot tests, solids, solubility, temperature, viscosity, and weight.

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Cash in Advance / Prepaid SalesCash in Advance / Prepaid Sales

Client Sample ID: DAMClient Sample ID: DAM

GC/MS VolatilesGC/MS Volatiles

Lot-Sample #...:Lot-Sample #...: C9K060597-001 Work Order #...:Work Order #...: LN2ME1AC Matrix.........:Matrix.........: SOLID Date Sampled...:Date Sampled...: 11/03/09 Date Received..:Date Received..: 11/06/09 MS Run #.......:MS Run #.......: 9317032 Prep Date......:Prep Date......: 11/13/09 Analysis Date..:Analysis Date..: 11/13/09 Prep Batch #...:Prep Batch #...: 9317045 Analysis Time..:Analysis Time..: 09:17 Dilution Factor:Dilution Factor: 1 % Moisture.....:% Moisture.....: 26 Method.........:Method.........: SW846 8260B

REPORTING

PARAMETER______________________________ RESULT_______________ LIMIT_________ UNITS_________ MDL_______________ AcetoneAcetone 13 J,B13 J,B 2727 ug/kgug/kg 6.76.7 Benzene ND 6.7 ug/kg 0.91 Bromodichloromethane ND 6.7 ug/kg 0.75 Bromoform ND 6.7 ug/kg 0.59 Bromomethane ND 6.7 ug/kg 0.99 2-Butanone ND 6.7 ug/kg 1.2 Carbon disulfide ND 6.7 ug/kg 0.69 Carbon tetrachloride ND 6.7 ug/kg 0.60 Chlorobenzene ND 6.7 ug/kg 1.0 Chloroethane ND 6.7 ug/kg 2.1 Chloroform ND 6.7 ug/kg 0.79 Chloromethane ND 6.7 ug/kg 1.1 Cyclohexane ND 6.7 ug/kg 0.50 Dibromochloromethane ND 6.7 ug/kg 0.95 1,2-Dibromo-3-chloro- ND 6.7 ug/kg 1.0 propane 1,2-Dibromoethane ND 6.7 ug/kg 1.2 1,3-Dichlorobenzene ND 6.7 ug/kg 0.88 1,4-Dichlorobenzene ND 6.7 ug/kg 0.86 1,2-Dichlorobenzene ND 6.7 ug/kg 1.1 Dichlorodifluoromethane ND 6.7 ug/kg 0.89 1,1-Dichloroethane ND 6.7 ug/kg 0.77 1,2-Dichloroethane ND 6.7 ug/kg 0.82 1,1-Dichloroethene ND 6.7 ug/kg 1.1 cis-1,2-Dichloroethene ND 6.7 ug/kg 0.94 trans-1,2-Dichloroethene ND 6.7 ug/kg 0.80 1,2-Dichloropropane ND 6.7 ug/kg 0.73 cis-1,3-Dichloropropene ND 6.7 ug/kg 0.91 trans-1,3-Dichloropropene ND 6.7 ug/kg 0.80 Ethylbenzene ND 6.7 ug/kg 0.86 2-Hexanone ND 6.7 ug/kg 0.93 Isopropylbenzene ND 6.7 ug/kg 0.91 Methyl acetate ND 6.7 ug/kg 1.2 Methylene chloride ND 6.7 ug/kg 0.90 Methylcyclohexane ND 6.7 ug/kg 0.97 4-Methyl-2-pentanone ND 6.7 ug/kg 0.88 Methyl tert-butyl ether ND 6.7 ug/kg 1.0 Styrene ND 6.7 ug/kg 0.95

(Continued on next page)

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GC/MS VolatilesGC/MS Volatiles

Lot-Sample #...:Lot-Sample #...: C9K060597-001 Work Order #...:Work Order #...: LN2ME1AC Matrix.........:Matrix.........: SOLID

REPORTING

PARAMETER______________________________ RESULT_______________ LIMIT_________ UNITS_________ MDL_______________ 1,1,2,2-Tetrachloroethane ND 6.7 ug/kg 0.96 1,2,4-Trichloro- ND 6.7 ug/kg 1.2 benzene Tetrachloroethene ND 6.7 ug/kg 0.91 1,1,1-Trichloroethane ND 6.7 ug/kg 0.65 1,1,2-Trichloroethane ND 6.7 ug/kg 1.1 Trichloroethene ND 6.7 ug/kg 0.88 Trichlorofluoromethane ND 6.7 ug/kg 1.2 1,1,2-Trichloro- ND 6.7 ug/kg 1.4

1,2,2-trifluoroethane Toluene ND 6.7 ug/kg 0.98 Vinyl chloride ND 6.7 ug/kg 0.63 Xylenes (total) ND 20 ug/kg 3.0

PERCENT RECOVERY

SURROGATE______________________________ RECOVERY_______________ LIMITS__________

1,2-Dichloroethane-d4 101 (52 - 124) Toluene-d8 102 (72 - 127) 4-Bromofluorobenzene 93 (63 - 120) Dibromofluoromethane 104 (68 - 121)

NOTE(S):NOTE(S):______________________________________________________________________________________________________________________________________________________________________________ Results and reporting limits have been adjusted for dry weight.

J Estimated result. Result is less than RL.

B Method blank contamination. The associated method blank contains the target analyte at a reportable level.

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Client Sample ID: US1Client Sample ID: US1

GC/MS VolatilesGC/MS Volatiles

Lot-Sample #...:Lot-Sample #...: C9K060597-002 Work Order #...:Work Order #...: LN2MG1AL Matrix.........:Matrix.........: SOLID Date Sampled...:Date Sampled...: 11/03/09 Date Received..:Date Received..: 11/06/09 MS Run #.......:MS Run #.......: 9317032 Prep Date......:Prep Date......: 11/13/09 Analysis Date..:Analysis Date..: 11/13/09 Prep Batch #...:Prep Batch #...: 9317045 Analysis Time..:Analysis Time..: 09:40 Dilution Factor:Dilution Factor: 1 % Moisture.....:% Moisture.....: 26 Method.........:Method.........: SW846 8260B

REPORTING

PARAMETER______________________________ RESULT_______________ LIMIT_________ UNITS_________ MDL_______________ Acetone ND 27 ug/kg 6.8 Benzene ND 6.8 ug/kg 0.91 Bromodichloromethane ND 6.8 ug/kg 0.76 Bromoform ND 6.8 ug/kg 0.60 Bromomethane ND 6.8 ug/kg 1.0 2-Butanone ND 6.8 ug/kg 1.2 Carbon disulfide ND 6.8 ug/kg 0.69 Carbon tetrachloride ND 6.8 ug/kg 0.60 Chlorobenzene ND 6.8 ug/kg 1.0 Chloroethane ND 6.8 ug/kg 2.1 Chloroform ND 6.8 ug/kg 0.79 Chloromethane ND 6.8 ug/kg 1.2 Cyclohexane ND 6.8 ug/kg 0.50 Dibromochloromethane ND 6.8 ug/kg 0.96 1,2-Dibromo-3-chloro- ND 6.8 ug/kg 1.0 propane 1,2-Dibromoethane ND 6.8 ug/kg 1.2 1,3-Dichlorobenzene ND 6.8 ug/kg 0.89 1,4-Dichlorobenzene ND 6.8 ug/kg 0.86 1,2-Dichlorobenzene ND 6.8 ug/kg 1.1 Dichlorodifluoromethane ND 6.8 ug/kg 0.90 1,1-Dichloroethane ND 6.8 ug/kg 0.78 1,2-Dichloroethane ND 6.8 ug/kg 0.83 1,1-Dichloroethene ND 6.8 ug/kg 1.1 cis-1,2-Dichloroethene ND 6.8 ug/kg 0.95 trans-1,2-Dichloroethene ND 6.8 ug/kg 0.81 1,2-Dichloropropane ND 6.8 ug/kg 0.74 cis-1,3-Dichloropropene ND 6.8 ug/kg 0.92 trans-1,3-Dichloropropene ND 6.8 ug/kg 0.81 Ethylbenzene ND 6.8 ug/kg 0.87 2-Hexanone ND 6.8 ug/kg 0.93 Isopropylbenzene ND 6.8 ug/kg 0.92 Methyl acetate ND 6.8 ug/kg 1.2 Methylene chlorideMethylene chloride 5.7 J,B5.7 J,B 6.86.8 ug/kgug/kg 0.910.91 Methylcyclohexane ND 6.8 ug/kg 0.98 4-Methyl-2-pentanone ND 6.8 ug/kg 0.88 Methyl tert-butyl ether ND 6.8 ug/kg 1.0 Styrene ND 6.8 ug/kg 0.95

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GC/MS VolatilesGC/MS Volatiles

Lot-Sample #...:Lot-Sample #...: C9K060597-002 Work Order #...:Work Order #...: LN2MG1AL Matrix.........:Matrix.........: SOLID

REPORTING

PARAMETER______________________________ RESULT_______________ LIMIT_________ UNITS_________ MDL_______________ 1,1,2,2-Tetrachloroethane ND 6.8 ug/kg 0.97 1,2,4-Trichloro- ND 6.8 ug/kg 1.2 benzene Tetrachloroethene ND 6.8 ug/kg 0.92 1,1,1-Trichloroethane ND 6.8 ug/kg 0.66 1,1,2-Trichloroethane ND 6.8 ug/kg 1.1 Trichloroethene ND 6.8 ug/kg 0.89 Trichlorofluoromethane ND 6.8 ug/kg 1.2 1,1,2-Trichloro- ND 6.8 ug/kg 1.4

1,2,2-trifluoroethane Toluene ND 6.8 ug/kg 0.99 Vinyl chloride ND 6.8 ug/kg 0.64 Xylenes (total) ND 20 ug/kg 3.0

PERCENT RECOVERY

SURROGATE______________________________ RECOVERY_______________ LIMITS__________

1,2-Dichloroethane-d4 103 (52 - 124) Toluene-d8 98 (72 - 127) 4-Bromofluorobenzene 92 (63 - 120) Dibromofluoromethane 103 (68 - 121)

NOTE(S):NOTE(S):______________________________________________________________________________________________________________________________________________________________________________ Results and reporting limits have been adjusted for dry weight.

J Estimated result. Result is less than RL.

B Method blank contamination. The associated method blank contains the target analyte at a reportable level.

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Client Sample ID: US2Client Sample ID: US2

GC/MS VolatilesGC/MS Volatiles

Lot-Sample #...:Lot-Sample #...: C9K060597-003 Work Order #...:Work Order #...: LN2MK1AL Matrix.........:Matrix.........: SOLID Date Sampled...:Date Sampled...: 11/03/09 Date Received..:Date Received..: 11/06/09 MS Run #.......:MS Run #.......: 9317032 Prep Date......:Prep Date......: 11/13/09 Analysis Date..:Analysis Date..: 11/13/09 Prep Batch #...:Prep Batch #...: 9317045 Analysis Time..:Analysis Time..: 10:04 Dilution Factor:Dilution Factor: 1 % Moisture.....:% Moisture.....: 24 Method.........:Method.........: SW846 8260B

REPORTING

PARAMETER______________________________ RESULT_______________ LIMIT_________ UNITS_________ MDL_______________ AcetoneAcetone 14 J,B14 J,B 2626 ug/kgug/kg 6.66.6 Benzene ND 6.6 ug/kg 0.89 Bromodichloromethane ND 6.6 ug/kg 0.74 Bromoform ND 6.6 ug/kg 0.58 Bromomethane ND 6.6 ug/kg 0.97 2-Butanone ND 6.6 ug/kg 1.2 Carbon disulfide ND 6.6 ug/kg 0.67 Carbon tetrachloride ND 6.6 ug/kg 0.59 Chlorobenzene ND 6.6 ug/kg 1.0 Chloroethane ND 6.6 ug/kg 2.0 Chloroform ND 6.6 ug/kg 0.77 Chloromethane ND 6.6 ug/kg 1.1 Cyclohexane ND 6.6 ug/kg 0.49 Dibromochloromethane ND 6.6 ug/kg 0.94 1,2-Dibromo-3-chloro- ND 6.6 ug/kg 0.99 propane 1,2-Dibromoethane ND 6.6 ug/kg 1.1 1,3-Dichlorobenzene ND 6.6 ug/kg 0.86 1,4-Dichlorobenzene ND 6.6 ug/kg 0.84 1,2-Dichlorobenzene ND 6.6 ug/kg 1.1 Dichlorodifluoromethane ND 6.6 ug/kg 0.88 1,1-Dichloroethane ND 6.6 ug/kg 0.76 1,2-Dichloroethane ND 6.6 ug/kg 0.81 1,1-Dichloroethene ND 6.6 ug/kg 1.1 cis-1,2-Dichloroethene ND 6.6 ug/kg 0.93 trans-1,2-Dichloroethene ND 6.6 ug/kg 0.79 1,2-Dichloropropane ND 6.6 ug/kg 0.72 cis-1,3-Dichloropropene ND 6.6 ug/kg 0.89 trans-1,3-Dichloropropene ND 6.6 ug/kg 0.79 Ethylbenzene ND 6.6 ug/kg 0.85 2-Hexanone ND 6.6 ug/kg 0.91 Isopropylbenzene ND 6.6 ug/kg 0.89 Methyl acetate ND 6.6 ug/kg 1.2 Methylene chlorideMethylene chloride 4.1 J,B4.1 J,B 6.66.6 ug/kgug/kg 0.890.89 Methylcyclohexane ND 6.6 ug/kg 0.96 4-Methyl-2-pentanone ND 6.6 ug/kg 0.86 Methyl tert-butyl ether ND 6.6 ug/kg 0.99 Styrene ND 6.6 ug/kg 0.93

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GC/MS VolatilesGC/MS Volatiles

Lot-Sample #...:Lot-Sample #...: C9K060597-003 Work Order #...:Work Order #...: LN2MK1AL Matrix.........:Matrix.........: SOLID

REPORTING

PARAMETER______________________________ RESULT_______________ LIMIT_________ UNITS_________ MDL_______________ 1,1,2,2-Tetrachloroethane ND 6.6 ug/kg 0.95 1,2,4-Trichloro- ND 6.6 ug/kg 1.2 benzene Tetrachloroethene ND 6.6 ug/kg 0.90 1,1,1-Trichloroethane ND 6.6 ug/kg 0.64 1,1,2-Trichloroethane ND 6.6 ug/kg 1.1 Trichloroethene ND 6.6 ug/kg 0.87 Trichlorofluoromethane ND 6.6 ug/kg 1.2 1,1,2-Trichloro- ND 6.6 ug/kg 1.4

1,2,2-trifluoroethane Toluene ND 6.6 ug/kg 0.96 Vinyl chloride ND 6.6 ug/kg 0.62 Xylenes (total) ND 20 ug/kg 3.0

PERCENT RECOVERY

SURROGATE______________________________ RECOVERY_______________ LIMITS__________

1,2-Dichloroethane-d4 102 (52 - 124) Toluene-d8 98 (72 - 127) 4-Bromofluorobenzene 92 (63 - 120) Dibromofluoromethane 105 (68 - 121)

NOTE(S):NOTE(S):______________________________________________________________________________________________________________________________________________________________________________ Results and reporting limits have been adjusted for dry weight.

J Estimated result. Result is less than RL.

B Method blank contamination. The associated method blank contains the target analyte at a reportable level.

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METHOD BLANK REPORTMETHOD BLANK REPORT

GC/MS VolatilesGC/MS Volatiles

Client Lot #...:Client Lot #...: C9K060597 Work Order #...:Work Order #...: LPEA71AA Matrix.........:Matrix.........: SOLID MB Lot-Sample #:MB Lot-Sample #: C9K130000-045

Prep Date......:Prep Date......: 11/13/09 Analysis Time..:Analysis Time..: 05:44 Analysis Date..:Analysis Date..: 11/13/09 Prep Batch #...:Prep Batch #...: 9317045 Dilution Factor:Dilution Factor: 1

REPORTING

PARAMETER_________________________ RESULT_______________ LIMIT_________ UNITS__________ METHOD_________________ AcetoneAcetone 9.5 J9.5 J 2020 ug/kgug/kg SW846 8260BSW846 8260B Benzene ND 5.0 ug/kg SW846 8260B Bromodichloromethane ND 5.0 ug/kg SW846 8260B Bromoform ND 5.0 ug/kg SW846 8260B Bromomethane ND 5.0 ug/kg SW846 8260B 2-Butanone ND 5.0 ug/kg SW846 8260B Carbon disulfide ND 5.0 ug/kg SW846 8260B Carbon tetrachloride ND 5.0 ug/kg SW846 8260B Chlorobenzene ND 5.0 ug/kg SW846 8260B Chloroethane ND 5.0 ug/kg SW846 8260B Chloroform ND 5.0 ug/kg SW846 8260B Chloromethane ND 5.0 ug/kg SW846 8260B Cyclohexane ND 5.0 ug/kg SW846 8260B Dibromochloromethane ND 5.0 ug/kg SW846 8260B 1,2-Dibromo-3-chloro- ND 5.0 ug/kg SW846 8260B propane

1,2-Dibromoethane ND 5.0 ug/kg SW846 8260B 1,3-Dichlorobenzene ND 5.0 ug/kg SW846 8260B 1,4-Dichlorobenzene ND 5.0 ug/kg SW846 8260B 1,2-Dichlorobenzene ND 5.0 ug/kg SW846 8260B Dichlorodifluoromethane ND 5.0 ug/kg SW846 8260B 1,1-Dichloroethane ND 5.0 ug/kg SW846 8260B 1,2-Dichloroethane ND 5.0 ug/kg SW846 8260B 1,1-Dichloroethene ND 5.0 ug/kg SW846 8260B cis-1,2-Dichloroethene ND 5.0 ug/kg SW846 8260B trans-1,2-Dichloroethene ND 5.0 ug/kg SW846 8260B 1,2-Dichloropropane ND 5.0 ug/kg SW846 8260B cis-1,3-Dichloropropene ND 5.0 ug/kg SW846 8260B trans-1,3-Dichloropropene ND 5.0 ug/kg SW846 8260B Ethylbenzene ND 5.0 ug/kg SW846 8260B 2-Hexanone ND 5.0 ug/kg SW846 8260B Isopropylbenzene ND 5.0 ug/kg SW846 8260B Methyl acetate ND 5.0 ug/kg SW846 8260B Methylene chlorideMethylene chloride 3.4 J3.4 J 5.05.0 ug/kgug/kg SW846 8260BSW846 8260B Methylcyclohexane ND 5.0 ug/kg SW846 8260B 4-Methyl-2-pentanone ND 5.0 ug/kg SW846 8260B Methyl tert-butyl ether ND 5.0 ug/kg SW846 8260B Styrene ND 5.0 ug/kg SW846 8260B 1,1,2,2-Tetrachloroethane ND 5.0 ug/kg SW846 8260B 1,2,4-Trichloro-1,2,4-Trichloro- 1.5 J1.5 J 5.05.0 ug/kgug/kg SW846 8260BSW846 8260B benzenebenzene

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Client Lot #...:Client Lot #...: C9K060597 Work Order #...:Work Order #...: LPEA71AA Matrix.........:Matrix.........: SOLID

REPORTING

PARAMETER_________________________ RESULT_______________ LIMIT_________ UNITS__________ METHOD_________________ Tetrachloroethene ND 5.0 ug/kg SW846 8260B 1,1,1-Trichloroethane ND 5.0 ug/kg SW846 8260B 1,1,2-Trichloroethane ND 5.0 ug/kg SW846 8260B Trichloroethene ND 5.0 ug/kg SW846 8260B Trichlorofluoromethane ND 5.0 ug/kg SW846 8260B 1,1,2-Trichloro- ND 5.0 ug/kg SW846 8260B 1,2,2-trifluoroethane

Toluene ND 5.0 ug/kg SW846 8260B Vinyl chloride ND 5.0 ug/kg SW846 8260B Xylenes (total) ND 15 ug/kg SW846 8260B

PERCENT RECOVERY

SURROGATE_________________________ RECOVERY________ LIMITS__________

1,2-Dichloroethane-d4 113 (52 - 124) Toluene-d8 101 (72 - 127) 4-Bromofluorobenzene 93 (63 - 120) Dibromofluoromethane 101 (68 - 121)

NOTE(S):NOTE(S):______________________________________________________________________________________________________________________________________________________________________________________ Calculations are performed before rounding to avoid round-off errors in calculated results.

J Estimated result. Result is less than RL.

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LABORATORY CONTROL SAMPLE EVALUATION REPORTLABORATORY CONTROL SAMPLE EVALUATION REPORT

Client Lot #...:Client Lot #...: C9K060597 Work Order #...:Work Order #...: LPEA71AC Matrix.........:Matrix.........: SOLID LCS Lot-Sample#:LCS Lot-Sample#: C9K130000-045 Prep Date......:Prep Date......: 11/13/09 Analysis Date..:Analysis Date..: 11/13/09 Prep Batch #...:Prep Batch #...: 9317045 Analysis Time..:Analysis Time..: 06:55 Dilution Factor:Dilution Factor: 1

PERCENT RECOVERY

PARAMETER________________________ RECOVERY________ LIMITS__________ METHOD_________________ BenzeneBenzene 9595 (77 - 120)(77 - 120) SW846 8260BSW846 8260B ChlorobenzeneChlorobenzene 9696 (79 - 120)(79 - 120) SW846 8260BSW846 8260B 1,1-Dichloroethene1,1-Dichloroethene 7676 (59 - 129)(59 - 129) SW846 8260BSW846 8260B TrichloroetheneTrichloroethene 9898 (76 - 119)(76 - 119) SW846 8260BSW846 8260B TolueneToluene 9999 (78 - 124)(78 - 124) SW846 8260BSW846 8260B

PERCENT RECOVERY

SURROGATE_________________________ RECOVERY________ LIMITS__________

1,2-Dichloroethane-d4 104 (52 - 124) Toluene-d8 102 (72 - 127) 4-Bromofluorobenzene 93 (63 - 120) Dibromofluoromethane 101 (68 - 121)

NOTE(S):NOTE(S):__________________________________________________________________________________________________________________________________________________________________________ Calculations are performed before rounding to avoid round-off errors in calculated results.

Bold print denotes control parameters

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MATRIX SPIKE SAMPLE EVALUATION REPORTMATRIX SPIKE SAMPLE EVALUATION REPORT

Client Lot #...:Client Lot #...: C9K060597 Work Order #...:Work Order #...: LN2F61D6-MS Matrix.........:Matrix.........: SOLID MS Lot-Sample #:MS Lot-Sample #: C9K060574-001 LN2F61D7-MSD Date Sampled...:Date Sampled...: 11/04/09 Date Received..:Date Received..: 11/06/09 MS Run #.......:MS Run #.......: 9317032 Prep Date......:Prep Date......: 11/13/09 Analysis Date..:Analysis Date..: 11/13/09 Prep Batch #...:Prep Batch #...: 9317045 Analysis Time..:Analysis Time..: 07:19 Dilution Factor:Dilution Factor: 1 % Moisture.....:% Moisture.....: 46

PERCENT RECOVERY RPD

PARAMETER_________________________ RECOVERY_________ LIMITS__________ RPD____ LIMITS_________ METHOD_________________ BenzeneBenzene 9999 (77 - 120)(77 - 120) SW846 8260BSW846 8260B

101101 (77 - 120)(77 - 120) 2.22.2 (0-20)(0-20) SW846 8260BSW846 8260B

ChlorobenzeneChlorobenzene 101101 (79 - 120)(79 - 120) SW846 8260BSW846 8260B

101101 (79 - 120)(79 - 120) 0.590.59 (0-20)(0-20) SW846 8260BSW846 8260B

1,1-Dichloroethene1,1-Dichloroethene 7979 (59 - 129)(59 - 129) SW846 8260BSW846 8260B

7676 (59 - 129)(59 - 129) 4.24.2 (0-25)(0-25) SW846 8260BSW846 8260B

TrichloroetheneTrichloroethene 103103 (76 - 119)(76 - 119) SW846 8260BSW846 8260B

103103 (76 - 119)(76 - 119) 0.550.55 (0-21)(0-21) SW846 8260BSW846 8260B

TolueneToluene 105105 (78 - 124)(78 - 124) SW846 8260BSW846 8260B

106106 (78 - 124)(78 - 124) 0.710.71 (0-21)(0-21) SW846 8260BSW846 8260B

PERCENT RECOVERY

SURROGATE_________________________ RECOVERY________ LIMITS__________

1,2-Dichloroethane-d4 104 (52 - 124)

103 (52 - 124) Toluene-d8 98 (72 - 127)

98 (72 - 127) 4-Bromofluorobenzene 91 (63 - 120)

89 (63 - 120) Dibromofluoromethane 94 (68 - 121)

96 (68 - 121)

NOTE(S):NOTE(S):______________________________________________________________________________________________________________________________________________________________________________________ Calculations are performed before rounding to avoid round-off errors in calculated results.

Bold print denotes control parameters

Results and reporting limits have been adjusted for dry weight.

C9K060597 17 of 72

GC/MS SemivolatilesGC/MS Semivolatiles

Lot-Sample #...:Lot-Sample #...: C9K060597-001 Work Order #...:Work Order #...: LN2ME1AD Matrix.........:Matrix.........: SOLID Date Sampled...:Date Sampled...: 11/03/09 Date Received..:Date Received..: 11/06/09 MS Run #.......:MS Run #.......: 9314317 Prep Date......:Prep Date......: 11/10/09 Analysis Date..:Analysis Date..: 11/11/09 Prep Batch #...:Prep Batch #...: 9314572 Analysis Time..:Analysis Time..: 09:53 Dilution Factor:Dilution Factor: 3.75 % Moisture.....:% Moisture.....: 26 Method.........:Method.........: SW846 8270C

REPORTING

PARAMETER______________________________ RESULT_______________ LIMIT_________ UNITS_________ MDL_______________ AcenaphtheneAcenaphthene 26 J26 J 3434 ug/kgug/kg 5.45.4 AcenaphthyleneAcenaphthylene 11 J11 J 3434 ug/kgug/kg 6.76.7 AcetophenoneAcetophenone 24 J24 J 170170 ug/kgug/kg 7.77.7 AnthraceneAnthracene 120120 3434 ug/kgug/kg 5.95.9 Atrazine ND 170 ug/kg 8.0 Benzo(a)anthraceneBenzo(a)anthracene 14001400 3434 ug/kgug/kg 5.45.4 Benzo(a)pyreneBenzo(a)pyrene 470470 3434 ug/kgug/kg 9.49.4 Benzo(b)fluorantheneBenzo(b)fluoranthene 610610 3434 ug/kgug/kg 6.86.8 Benzo(ghi)peryleneBenzo(ghi)perylene 6161 3434 ug/kgug/kg 2.52.5 Benzo(k)fluoranthene ND 34 ug/kg 7.0 BenzaldehydeBenzaldehyde 140 J140 J 170170 ug/kgug/kg 4.44.4 1,1'-Biphenyl1,1'-Biphenyl 90 J90 J 170170 ug/kgug/kg 7.77.7 bis(2-Chloroethoxy) ND 170 ug/kg 6.7 methane bis(2-Chloroethyl)- ND 34 ug/kg 2.9 ether bis(2-Ethylhexyl)bis(2-Ethylhexyl) 76 J76 J 170170 ug/kgug/kg 1414 phthalatephthalate 4-Bromophenyl phenyl ND 170 ug/kg 7.1 ether Butyl benzyl phthalateButyl benzyl phthalate 29 J29 J 170170 ug/kgug/kg 1212 Caprolactam ND 860 ug/kg 22 CarbazoleCarbazole 110110 3434 ug/kgug/kg 4.44.4 4-Chloroaniline ND 170 ug/kg 5.2 4-Chloro-3-methylphenol ND 170 ug/kg 5.0 2-Chloronaphthalene ND 34 ug/kg 4.5 2-Chlorophenol ND 170 ug/kg 5.2 4-Chlorophenyl phenyl ND 170 ug/kg 7.4 ether ChryseneChrysene 29002900 3434 ug/kgug/kg 5.95.9 Dibenz(a,h)anthraceneDibenz(a,h)anthracene 8989 3434 ug/kgug/kg 7.47.4 DibenzofuranDibenzofuran 47 J47 J 170170 ug/kgug/kg 5.75.7 3,3'-Dichlorobenzidine ND 170 ug/kg 32 2,4-Dichlorophenol ND 34 ug/kg 6.8 Diethyl phthalate ND 170 ug/kg 9.5 2,4-Dimethylphenol ND 170 ug/kg 7.1 Dimethyl phthalate ND 170 ug/kg 5.7 Di-n-butyl phthalateDi-n-butyl phthalate 44 J44 J 170170 ug/kgug/kg 9.49.4

C9K060597 18 of 72

GC/MS SemivolatilesGC/MS Semivolatiles

Lot-Sample #...:Lot-Sample #...: C9K060597-001 Work Order #...:Work Order #...: LN2ME1AD Matrix.........:Matrix.........: SOLID

REPORTING

PARAMETER______________________________ RESULT_______________ LIMIT_________ UNITS_________ MDL_______________ 4,6-Dinitro- ND 860 ug/kg 160

2-methylphenol 2,4-Dinitrophenol ND 860 ug/kg 54 2,4-Dinitrotoluene ND 170 ug/kg 7.9 2,6-Dinitrotoluene ND 170 ug/kg 8.6 Di-n-octyl phthalate ND 170 ug/kg 4.3 FluorantheneFluoranthene 940940 3434 ug/kgug/kg 2.82.8 FluoreneFluorene 100100 3434 ug/kgug/kg 5.15.1 Hexachlorobenzene ND 34 ug/kg 6.4 Hexachlorobutadiene ND 34 ug/kg 7.1 Hexachlorocyclopenta- ND 170 ug/kg 6.4 diene Hexachloroethane ND 170 ug/kg 5.7 Indeno(1,2,3-cd)pyreneIndeno(1,2,3-cd)pyrene 5151 3434 ug/kgug/kg 1.81.8 Isophorone ND 170 ug/kg 6.5 2-Methylnaphthalene2-Methylnaphthalene 210210 3434 ug/kgug/kg 6.66.6 2-Methylphenol ND 170 ug/kg 6.2 4-Methylphenol4-Methylphenol 99 J99 J 170170 ug/kgug/kg 7.47.4 NaphthaleneNaphthalene 200200 3434 ug/kgug/kg 4.94.9 2-Nitroaniline ND 860 ug/kg 10 3-Nitroaniline ND 860 ug/kg 5.5 4-Nitroaniline ND 860 ug/kg 8.2 Nitrobenzene ND 34 ug/kg 8.5 2-Nitrophenol ND 170 ug/kg 6.4 4-Nitrophenol ND 860 ug/kg 99 N-Nitrosodi-n-propyl- ND 34 ug/kg 9.3 amine N-Nitrosodiphenylamine ND 34 ug/kg 6.9 2,2'-oxybis ND 34 ug/kg 7.3

(1-Chloropropane) Pentachlorophenol ND 170 ug/kg 29 PhenanthrenePhenanthrene 10001000 3434 ug/kgug/kg 4.04.0 PhenolPhenol 6666 3434 ug/kgug/kg 6.76.7 PyrenePyrene 980980 3434 ug/kgug/kg 8.98.9 2,4,5-Trichloro- ND 170 ug/kg 4.1 phenol 2,4,6-Trichloro- ND 170 ug/kg 8.4 phenol

C9K060597 19 of 72

GC/MS SemivolatilesGC/MS Semivolatiles

Lot-Sample #...:Lot-Sample #...: C9K060597-001 Work Order #...:Work Order #...: LN2ME1AD Matrix.........:Matrix.........: SOLID

PERCENT RECOVERY

SURROGATE______________________________ RECOVERY_______________ LIMITS__________

Nitrobenzene-d5 88 (27 - 110) Terphenyl-d14 108 (21 - 130) 2-Fluorobiphenyl 96 (28 - 108) 2-Fluorophenol 95 (28 - 107) Phenol-d5 95 (30 - 112) 2,4,6-Tribromophenol 78 (21 - 116)

NOTE(S):NOTE(S):______________________________________________________________________________________________________________________________________________________________________________ Results and reporting limits have been adjusted for dry weight.

C9K060597 20 of 72

GC/MS SemivolatilesGC/MS Semivolatiles

Lot-Sample #...:Lot-Sample #...: C9K060597-002 Work Order #...:Work Order #...: LN2MG1AM Matrix.........:Matrix.........: SOLID Date Sampled...:Date Sampled...: 11/03/09 Date Received..:Date Received..: 11/06/09 MS Run #.......:MS Run #.......: 9314317 Prep Date......:Prep Date......: 11/10/09 Analysis Date..:Analysis Date..: 11/11/09 Prep Batch #...:Prep Batch #...: 9314572 Analysis Time..:Analysis Time..: 10:14 Dilution Factor:Dilution Factor: 3.48 % Moisture.....:% Moisture.....: 26 Method.........:Method.........: SW846 8270C

REPORTING

PARAMETER______________________________ RESULT_______________ LIMIT_________ UNITS_________ MDL_______________ Acenaphthene ND 32 ug/kg 5.0 Acenaphthylene ND 32 ug/kg 6.3 Acetophenone ND 160 ug/kg 7.2 AnthraceneAnthracene 7.4 J7.4 J 3232 ug/kgug/kg 5.55.5 Atrazine ND 160 ug/kg 7.4 Benzo(a)anthraceneBenzo(a)anthracene 11 J11 J 3232 ug/kgug/kg 5.05.0 Benzo(a)pyrene ND 32 ug/kg 8.8 Benzo(b)fluorantheneBenzo(b)fluoranthene 19 J19 J 3232 ug/kgug/kg 6.46.4 Benzo(ghi)perylene ND 32 ug/kg 2.3 Benzo(k)fluoranthene ND 32 ug/kg 6.5 Benzaldehyde ND 160 ug/kg 4.1 1,1'-Biphenyl1,1'-Biphenyl 29 J29 J 160160 ug/kgug/kg 7.27.2 bis(2-Chloroethoxy) ND 160 ug/kg 6.3 methane bis(2-Chloroethyl)- ND 32 ug/kg 2.8 ether bis(2-Ethylhexyl)bis(2-Ethylhexyl) 48 J48 J 160160 ug/kgug/kg 1313 phthalatephthalate 4-Bromophenyl phenyl ND 160 ug/kg 6.7 ether Butyl benzyl phthalateButyl benzyl phthalate 35 J35 J 160160 ug/kgug/kg 1111 CaprolactamCaprolactam 21 J21 J 800800 ug/kgug/kg 2121 Carbazole ND 32 ug/kg 4.1 4-Chloroaniline ND 160 ug/kg 4.9 4-Chloro-3-methylphenol ND 160 ug/kg 4.7 2-Chloronaphthalene ND 32 ug/kg 4.2 2-Chlorophenol ND 160 ug/kg 4.8 4-Chlorophenyl phenyl ND 160 ug/kg 6.9 ether ChryseneChrysene 3434 3232 ug/kgug/kg 5.55.5 Dibenz(a,h)anthracene ND 32 ug/kg 6.9 Dibenzofuran ND 160 ug/kg 5.3 3,3'-Dichlorobenzidine ND 160 ug/kg 30 2,4-Dichlorophenol ND 32 ug/kg 6.4 Diethyl phthalate ND 160 ug/kg 8.9 2,4-Dimethylphenol ND 160 ug/kg 6.6 Dimethyl phthalate ND 160 ug/kg 5.3 Di-n-butyl phthalateDi-n-butyl phthalate 39 J39 J 160160 ug/kgug/kg 8.88.8

C9K060597 21 of 72

GC/MS SemivolatilesGC/MS Semivolatiles

Lot-Sample #...:Lot-Sample #...: C9K060597-002 Work Order #...:Work Order #...: LN2MG1AM Matrix.........:Matrix.........: SOLID

REPORTING

PARAMETER______________________________ RESULT_______________ LIMIT_________ UNITS_________ MDL_______________ 4,6-Dinitro- ND 800 ug/kg 150

2-methylphenol 2,4-Dinitrophenol ND 800 ug/kg 50 2,4-Dinitrotoluene ND 160 ug/kg 7.4 2,6-Dinitrotoluene ND 160 ug/kg 8.0 Di-n-octyl phthalate ND 160 ug/kg 4.0 FluorantheneFluoranthene 3434 3232 ug/kgug/kg 2.72.7 Fluorene ND 32 ug/kg 4.7 Hexachlorobenzene ND 32 ug/kg 6.0 Hexachlorobutadiene ND 32 ug/kg 6.7 Hexachlorocyclopenta- ND 160 ug/kg 6.0 diene Hexachloroethane ND 160 ug/kg 5.3 Indeno(1,2,3-cd)pyrene ND 32 ug/kg 1.7 Isophorone ND 160 ug/kg 6.1 2-Methylnaphthalene2-Methylnaphthalene 7676 3232 ug/kgug/kg 6.26.2 2-Methylphenol ND 160 ug/kg 5.8 4-Methylphenol ND 160 ug/kg 6.9 NaphthaleneNaphthalene 5151 3232 ug/kgug/kg 4.64.6 2-Nitroaniline ND 800 ug/kg 9.6 3-Nitroaniline ND 800 ug/kg 5.1 4-Nitroaniline ND 800 ug/kg 7.7 Nitrobenzene ND 32 ug/kg 7.9 2-Nitrophenol ND 160 ug/kg 6.0 4-Nitrophenol ND 800 ug/kg 93 N-Nitrosodi-n-propyl- ND 32 ug/kg 8.7 amine N-Nitrosodiphenylamine ND 32 ug/kg 6.4 2,2'-oxybis ND 32 ug/kg 6.9

(1-Chloropropane) Pentachlorophenol ND 160 ug/kg 27 PhenanthrenePhenanthrene 8282 3232 ug/kgug/kg 3.83.8 Phenol ND 32 ug/kg 6.2 PyrenePyrene 3434 3232 ug/kgug/kg 8.38.3 2,4,5-Trichloro- ND 160 ug/kg 3.9 phenol 2,4,6-Trichloro- ND 160 ug/kg 7.8 phenol

C9K060597 22 of 72

GC/MS SemivolatilesGC/MS Semivolatiles

Lot-Sample #...:Lot-Sample #...: C9K060597-002 Work Order #...:Work Order #...: LN2MG1AM Matrix.........:Matrix.........: SOLID

PERCENT RECOVERY

SURROGATE______________________________ RECOVERY_______________ LIMITS__________

Nitrobenzene-d5 82 (27 - 110) Terphenyl-d14 100 (21 - 130) 2-Fluorobiphenyl 83 (28 - 108) 2-Fluorophenol 85 (28 - 107) Phenol-d5 86 (30 - 112) 2,4,6-Tribromophenol 58 (21 - 116)

NOTE(S):NOTE(S):______________________________________________________________________________________________________________________________________________________________________________ Results and reporting limits have been adjusted for dry weight.

C9K060597 23 of 72

GC/MS SemivolatilesGC/MS Semivolatiles

Lot-Sample #...:Lot-Sample #...: C9K060597-003 Work Order #...:Work Order #...: LN2MK1AM Matrix.........:Matrix.........: SOLID Date Sampled...:Date Sampled...: 11/03/09 Date Received..:Date Received..: 11/06/09 MS Run #.......:MS Run #.......: 9314317 Prep Date......:Prep Date......: 11/10/09 Analysis Date..:Analysis Date..: 11/11/09 Prep Batch #...:Prep Batch #...: 9314572 Analysis Time..:Analysis Time..: 11:19 Dilution Factor:Dilution Factor: 3.75 % Moisture.....:% Moisture.....: 24 Method.........:Method.........: SW846 8270C

REPORTING

PARAMETER______________________________ RESULT_______________ LIMIT_________ UNITS_________ MDL_______________ AcenaphtheneAcenaphthene 140140 3333 ug/kgug/kg 5.35.3 AcenaphthyleneAcenaphthylene 23 J23 J 3333 ug/kgug/kg 6.66.6 AcetophenoneAcetophenone 14 J14 J 160160 ug/kgug/kg 7.67.6 AnthraceneAnthracene 140140 3333 ug/kgug/kg 5.85.8 Atrazine ND 160 ug/kg 7.8 Benzo(a)anthraceneBenzo(a)anthracene 350350 3333 ug/kgug/kg 5.35.3 Benzo(a)pyreneBenzo(a)pyrene 300300 3333 ug/kgug/kg 9.29.2 Benzo(b)fluorantheneBenzo(b)fluoranthene 460460 3333 ug/kgug/kg 6.76.7 Benzo(ghi)peryleneBenzo(ghi)perylene 190190 3333 ug/kgug/kg 2.42.4 Benzo(k)fluoranthene ND 33 ug/kg 6.9 Benzaldehyde ND 160 ug/kg 4.3 1,1'-Biphenyl1,1'-Biphenyl 38 J38 J 160160 ug/kgug/kg 7.57.5 bis(2-Chloroethoxy) ND 160 ug/kg 6.6 methane bis(2-Chloroethyl)- ND 33 ug/kg 2.9 ether bis(2-Ethylhexyl)bis(2-Ethylhexyl) 63 J63 J 160160 ug/kgug/kg 1414 phthalatephthalate 4-Bromophenyl phenyl ND 160 ug/kg 7.0 ether Butyl benzyl phthalateButyl benzyl phthalate 12 J12 J 160160 ug/kgug/kg 1212 Caprolactam ND 840 ug/kg 22 CarbazoleCarbazole 3434 3333 ug/kgug/kg 4.34.3 4-Chloroaniline ND 160 ug/kg 5.1 4-Chloro-3-methylphenol ND 160 ug/kg 4.9 2-Chloronaphthalene ND 33 ug/kg 4.5 2-Chlorophenol ND 160 ug/kg 5.1 4-Chlorophenyl phenyl ND 160 ug/kg 7.3 ether ChryseneChrysene 410410 3333 ug/kgug/kg 5.85.8 Dibenz(a,h)anthraceneDibenz(a,h)anthracene 6161 3333 ug/kgug/kg 7.37.3 DibenzofuranDibenzofuran 8.7 J8.7 J 160160 ug/kgug/kg 5.65.6 3,3'-Dichlorobenzidine ND 160 ug/kg 31 2,4-Dichlorophenol ND 33 ug/kg 6.7 Diethyl phthalate ND 160 ug/kg 9.3 2,4-Dimethylphenol ND 160 ug/kg 6.9 Dimethyl phthalate ND 160 ug/kg 5.6 Di-n-butyl phthalateDi-n-butyl phthalate 40 J40 J 160160 ug/kgug/kg 9.29.2

C9K060597 24 of 72

GC/MS SemivolatilesGC/MS Semivolatiles

Lot-Sample #...:Lot-Sample #...: C9K060597-003 Work Order #...:Work Order #...: LN2MK1AM Matrix.........:Matrix.........: SOLID

REPORTING

PARAMETER______________________________ RESULT_______________ LIMIT_________ UNITS_________ MDL_______________ 4,6-Dinitro- ND 840 ug/kg 160

2-methylphenol 2,4-Dinitrophenol ND 840 ug/kg 53 2,4-Dinitrotoluene ND 160 ug/kg 7.7 2,6-Dinitrotoluene ND 160 ug/kg 8.4 Di-n-octyl phthalateDi-n-octyl phthalate 68 J68 J 160160 ug/kgug/kg 4.24.2 FluorantheneFluoranthene 810810 3333 ug/kgug/kg 2.82.8 FluoreneFluorene 110110 3333 ug/kgug/kg 5.05.0 Hexachlorobenzene ND 33 ug/kg 6.2 Hexachlorobutadiene ND 33 ug/kg 7.0 Hexachlorocyclopenta- ND 160 ug/kg 6.3 diene Hexachloroethane ND 160 ug/kg 5.6 Indeno(1,2,3-cd)pyreneIndeno(1,2,3-cd)pyrene 160160 3333 ug/kgug/kg 1.81.8 Isophorone ND 160 ug/kg 6.4 2-Methylnaphthalene2-Methylnaphthalene 9696 3333 ug/kgug/kg 6.56.5 2-Methylphenol ND 160 ug/kg 6.1 4-Methylphenol ND 160 ug/kg 7.2 NaphthaleneNaphthalene 7373 3333 ug/kgug/kg 4.84.8 2-Nitroaniline ND 840 ug/kg 10 3-Nitroaniline ND 840 ug/kg 5.4 4-Nitroaniline ND 840 ug/kg 8.1 Nitrobenzene ND 33 ug/kg 8.3 2-Nitrophenol ND 160 ug/kg 6.3 4-Nitrophenol ND 840 ug/kg 97 N-Nitrosodi-n-propyl- ND 33 ug/kg 9.2 amine N-Nitrosodiphenylamine ND 33 ug/kg 6.8 2,2'-oxybis ND 33 ug/kg 7.2

(1-Chloropropane) Pentachlorophenol ND 160 ug/kg 29 PhenanthrenePhenanthrene 670670 3333 ug/kgug/kg 3.93.9 Phenol ND 33 ug/kg 6.6 PyrenePyrene 660660 3333 ug/kgug/kg 8.88.8 2,4,5-Trichloro- ND 160 ug/kg 4.1 phenol 2,4,6-Trichloro- ND 160 ug/kg 8.2 phenol

C9K060597 25 of 72

GC/MS SemivolatilesGC/MS Semivolatiles

Lot-Sample #...:Lot-Sample #...: C9K060597-003 Work Order #...:Work Order #...: LN2MK1AM Matrix.........:Matrix.........: SOLID

PERCENT RECOVERY

SURROGATE______________________________ RECOVERY_______________ LIMITS__________

Nitrobenzene-d5 93 (27 - 110) Terphenyl-d14 99 (21 - 130) 2-Fluorobiphenyl 99 (28 - 108) 2-Fluorophenol 94 (28 - 107) Phenol-d5 94 (30 - 112) 2,4,6-Tribromophenol 58 (21 - 116)

NOTE(S):NOTE(S):______________________________________________________________________________________________________________________________________________________________________________ Results and reporting limits have been adjusted for dry weight.

C9K060597 26 of 72

GC/MS SemivolatilesGC/MS Semivolatiles

Client Lot #...:Client Lot #...: C9K060597 Work Order #...:Work Order #...: LN7TF1AA Matrix.........:Matrix.........: SOLID MB Lot-Sample #:MB Lot-Sample #: C9K100000-572

Prep Date......:Prep Date......: 11/10/09 Analysis Time..:Analysis Time..: 09:10 Analysis Date..:Analysis Date..: 11/11/09 Prep Batch #...:Prep Batch #...: 9314572 Dilution Factor:Dilution Factor: 0.5

REPORTING

PARAMETER_________________________ RESULT_______________ LIMIT_________ UNITS__________ METHOD_________________ Acenaphthene ND 3.4 ug/kg SW846 8270C Acenaphthylene ND 3.4 ug/kg SW846 8270C Acetophenone ND 16 ug/kg SW846 8270C Anthracene ND 3.4 ug/kg SW846 8270C Atrazine ND 16 ug/kg SW846 8270C Benzo(a)anthracene ND 3.4 ug/kg SW846 8270C Benzo(a)pyrene ND 3.4 ug/kg SW846 8270C Benzo(b)fluoranthene ND 3.4 ug/kg SW846 8270C Benzo(ghi)perylene ND 3.4 ug/kg SW846 8270C Benzo(k)fluoranthene ND 3.4 ug/kg SW846 8270C Benzaldehyde ND 16 ug/kg SW846 8270C 1,1'-Biphenyl ND 16 ug/kg SW846 8270C bis(2-Chloroethoxy) ND 16 ug/kg SW846 8270C methane bis(2-Chloroethyl)- ND 3.4 ug/kg SW846 8270C ether bis(2-Ethylhexyl) ND 16 ug/kg SW846 8270C phthalate

4-Bromophenyl phenyl ND 16 ug/kg SW846 8270C ether

Butyl benzyl phthalate ND 16 ug/kg SW846 8270C Caprolactam ND 85 ug/kg SW846 8270C Carbazole ND 3.4 ug/kg SW846 8270C 4-Chloroaniline ND 16 ug/kg SW846 8270C 4-Chloro-3-methylphenol ND 16 ug/kg SW846 8270C 2-Chloronaphthalene ND 3.4 ug/kg SW846 8270C 2-Chlorophenol ND 16 ug/kg SW846 8270C 4-Chlorophenyl phenyl ND 16 ug/kg SW846 8270C ether

Chrysene ND 3.4 ug/kg SW846 8270C Dibenz(a,h)anthracene ND 3.4 ug/kg SW846 8270C Dibenzofuran ND 16 ug/kg SW846 8270C 3,3'-Dichlorobenzidine ND 16 ug/kg SW846 8270C 2,4-Dichlorophenol ND 3.4 ug/kg SW846 8270C Diethyl phthalate ND 16 ug/kg SW846 8270C 2,4-Dimethylphenol ND 16 ug/kg SW846 8270C Dimethyl phthalate ND 16 ug/kg SW846 8270C Di-n-butyl phthalate ND 16 ug/kg SW846 8270C 4,6-Dinitro- ND 85 ug/kg SW846 8270C 2-methylphenol

2,4-Dinitrophenol ND 85 ug/kg SW846 8270C

C9K060597 27 of 72

Client Lot #...:Client Lot #...: C9K060597 Work Order #...:Work Order #...: LN7TF1AA Matrix.........:Matrix.........: SOLID

REPORTING

PARAMETER_________________________ RESULT_______________ LIMIT_________ UNITS__________ METHOD_________________ 2,4-Dinitrotoluene ND 16 ug/kg SW846 8270C 2,6-Dinitrotoluene ND 16 ug/kg SW846 8270C Di-n-octyl phthalate ND 16 ug/kg SW846 8270C Fluoranthene ND 3.4 ug/kg SW846 8270C Fluorene ND 3.4 ug/kg SW846 8270C Hexachlorobenzene ND 3.4 ug/kg SW846 8270C Hexachlorobutadiene ND 3.4 ug/kg SW846 8270C Hexachlorocyclopenta- ND 16 ug/kg SW846 8270C diene

Hexachloroethane ND 16 ug/kg SW846 8270C Indeno(1,2,3-cd)pyrene ND 3.4 ug/kg SW846 8270C Isophorone ND 16 ug/kg SW846 8270C 2-Methylnaphthalene ND 3.4 ug/kg SW846 8270C 2-Methylphenol ND 16 ug/kg SW846 8270C 4-Methylphenol ND 16 ug/kg SW846 8270C Naphthalene ND 3.4 ug/kg SW846 8270C 2-Nitroaniline ND 85 ug/kg SW846 8270C 3-Nitroaniline ND 85 ug/kg SW846 8270C 4-Nitroaniline ND 85 ug/kg SW846 8270C Nitrobenzene ND 3.4 ug/kg SW846 8270C 2-Nitrophenol ND 16 ug/kg SW846 8270C 4-Nitrophenol ND 85 ug/kg SW846 8270C N-Nitrosodi-n-propyl- ND 3.4 ug/kg SW846 8270C amine

N-Nitrosodiphenylamine ND 3.4 ug/kg SW846 8270C 2,2'-oxybis ND 3.4 ug/kg SW846 8270C (1-Chloropropane)

Pentachlorophenol ND 16 ug/kg SW846 8270C Phenanthrene ND 3.4 ug/kg SW846 8270C Phenol ND 3.4 ug/kg SW846 8270C Pyrene ND 3.4 ug/kg SW846 8270C 2,4,5-Trichloro- ND 16 ug/kg SW846 8270C phenol

2,4,6-Trichloro- ND 16 ug/kg SW846 8270C phenol

PERCENT RECOVERY

SURROGATE_________________________ RECOVERY________ LIMITS__________

Nitrobenzene-d5 66 (27 - 110) Terphenyl-d14 94 (21 - 130) 2-Fluorobiphenyl 73 (28 - 108) 2-Fluorophenol 68 (28 - 107) Phenol-d5 73 (30 - 112) 2,4,6-Tribromophenol 46 (21 - 116)

C9K060597 28 of 72

Client Lot #...:Client Lot #...: C9K060597 Work Order #...:Work Order #...: LN7TF1AA Matrix.........:Matrix.........: SOLID

NOTE(S):NOTE(S):______________________________________________________________________________________________________________________________________________________________________________________ Calculations are performed before rounding to avoid round-off errors in calculated results.

C9K060597 29 of 72

Client Lot #...:Client Lot #...: C9K060597 Work Order #...:Work Order #...: LN7TF1AC Matrix.........:Matrix.........: SOLID LCS Lot-Sample#:LCS Lot-Sample#: C9K100000-572 Prep Date......:Prep Date......: 11/10/09 Analysis Date..:Analysis Date..: 11/12/09 Prep Batch #...:Prep Batch #...: 9314572 Analysis Time..:Analysis Time..: 09:35 Dilution Factor:Dilution Factor: 0.5

PERCENT RECOVERY

PARAMETER________________________ RECOVERY________ LIMITS__________ METHOD_________________ AcenaphtheneAcenaphthene 7373 (42 - 104)(42 - 104) SW846 8270CSW846 8270C 1,4-Dichlorobenzene1,4-Dichlorobenzene 7474 (41 - 101)(41 - 101) SW846 8270CSW846 8270C 1,2,4-Trichloro-1,2,4-Trichloro- 7373 (41 - 105)(41 - 105) SW846 8270CSW846 8270C benzenebenzene

4-Bromophenyl phenyl4-Bromophenyl phenyl 7474 (43 - 111)(43 - 111) SW846 8270CSW846 8270C etherether

Butyl benzyl phthalateButyl benzyl phthalate 7979 (40 - 117)(40 - 117) SW846 8270CSW846 8270C 4-Chloro-3-methylphenol4-Chloro-3-methylphenol 6363 (43 - 110)(43 - 110) SW846 8270CSW846 8270C 2-Chlorophenol2-Chlorophenol 7070 (40 - 105)(40 - 105) SW846 8270CSW846 8270C 2,4-Dinitrotoluene2,4-Dinitrotoluene 8484 (48 - 118)(48 - 118) SW846 8270CSW846 8270C HexachloroethaneHexachloroethane 7575 (40 - 102)(40 - 102) SW846 8270CSW846 8270C 4-Methylphenol4-Methylphenol 7070 (43 - 107)(43 - 107) SW846 8270CSW846 8270C NaphthaleneNaphthalene 7474 (42 - 104)(42 - 104) SW846 8270CSW846 8270C 4-Nitrophenol4-Nitrophenol 8787 (27 - 131)(27 - 131) SW846 8270CSW846 8270C N-Nitrosodi-n-propyl-N-Nitrosodi-n-propyl- 7575 (42 - 108)(42 - 108) SW846 8270CSW846 8270C amineamine

PentachlorophenolPentachlorophenol 8585 (18 - 125)(18 - 125) SW846 8270CSW846 8270C PhenolPhenol 6767 (39 - 105)(39 - 105) SW846 8270CSW846 8270C PyrenePyrene 7676 (39 - 113)(39 - 113) SW846 8270CSW846 8270C

PERCENT RECOVERY

SURROGATE_________________________ RECOVERY________ LIMITS__________

Nitrobenzene-d5 78 (27 - 110) Terphenyl-d14 82 (21 - 130) 2-Fluorobiphenyl 78 (28 - 108) 2-Fluorophenol 80 (28 - 107) Phenol-d5 77 (30 - 112) 2,4,6-Tribromophenol 79 (21 - 116)

NOTE(S):NOTE(S):__________________________________________________________________________________________________________________________________________________________________________ Calculations are performed before rounding to avoid round-off errors in calculated results.

C9K060597 30 of 72

Client Lot #...:Client Lot #...: C9K060597 Work Order #...:Work Order #...: LN2MG1CA-MS Matrix.........:Matrix.........: SOLID MS Lot-Sample #:MS Lot-Sample #: C9K060597-002 LN2MG1CC-MSD Date Sampled...:Date Sampled...: 11/03/09 Date Received..:Date Received..: 11/06/09 MS Run #.......:MS Run #.......: 9314317 Prep Date......:Prep Date......: 11/10/09 Analysis Date..:Analysis Date..: 11/11/09 Prep Batch #...:Prep Batch #...: 9314572 Analysis Time..:Analysis Time..: 10:36 Dilution Factor:Dilution Factor: 3.48 % Moisture.....:% Moisture.....: 26

PERCENT RECOVERY RPD

PARAMETER_________________________ RECOVERY_________ LIMITS__________ RPD____ LIMITS_________ METHOD_________________ AcenaphtheneAcenaphthene 8080 (42 - 104)(42 - 104) SW846 8270CSW846 8270C

8282 (42 - 104)(42 - 104) 3.13.1 (0-34)(0-34) SW846 8270CSW846 8270C

1,4-Dichlorobenzene1,4-Dichlorobenzene 6666 (41 - 101)(41 - 101) SW846 8270CSW846 8270C

7070 (41 - 101)(41 - 101) 5.95.9 (0-32)(0-32) SW846 8270CSW846 8270C

1,2,4-Trichloro-1,2,4-Trichloro- 6969 (41 - 105)(41 - 105) SW846 8270CSW846 8270C benzene

7575 (41 - 105)(41 - 105) 7.27.2 (0-36)(0-36) SW846 8270CSW846 8270C

4-Bromophenyl phenyl4-Bromophenyl phenyl 7878 (43 - 111)(43 - 111) SW846 8270CSW846 8270C ether

8585 (43 - 111)(43 - 111) 8.78.7 (0-20)(0-20) SW846 8270CSW846 8270C

Butyl benzyl phthalateButyl benzyl phthalate 8686 (40 - 117)(40 - 117) SW846 8270CSW846 8270C

9494 (40 - 117)(40 - 117) 8.68.6 (0-34)(0-34) SW846 8270CSW846 8270C

4-Chloro-3-methylphenol4-Chloro-3-methylphenol 7777 (43 - 110)(43 - 110) SW846 8270CSW846 8270C

8383 (43 - 110)(43 - 110) 7.67.6 (0-31)(0-31) SW846 8270CSW846 8270C

2-Chlorophenol2-Chlorophenol 7474 (40 - 105)(40 - 105) SW846 8270CSW846 8270C

7676 (40 - 105)(40 - 105) 3.33.3 (0-37)(0-37) SW846 8270CSW846 8270C

2,4-Dinitrotoluene2,4-Dinitrotoluene 8484 (48 - 118)(48 - 118) SW846 8270CSW846 8270C

8585 (48 - 118)(48 - 118) 1.41.4 (0-33)(0-33) SW846 8270CSW846 8270C

HexachloroethaneHexachloroethane 6767 (40 - 102)(40 - 102) SW846 8270CSW846 8270C

6565 (40 - 102)(40 - 102) 2.42.4 (0-34)(0-34) SW846 8270CSW846 8270C

4-Methylphenol4-Methylphenol 7777 (43 - 107)(43 - 107) SW846 8270CSW846 8270C

8383 (43 - 107)(43 - 107) 8.18.1 (0-36)(0-36) SW846 8270CSW846 8270C

NaphthaleneNaphthalene 8181 (42 - 104)(42 - 104) SW846 8270CSW846 8270C

8888 (42 - 104)(42 - 104) 7.27.2 (0-25)(0-25) SW846 8270CSW846 8270C

4-Nitrophenol4-Nitrophenol 6161 (27 - 131)(27 - 131) SW846 8270CSW846 8270C

6767 (27 - 131)(27 - 131) 9.49.4 (0-33)(0-33) SW846 8270CSW846 8270C

N-Nitrosodi-n-propyl-N-Nitrosodi-n-propyl- 7575 (42 - 108)(42 - 108) SW846 8270CSW846 8270C amine

8181 (42 - 108)(42 - 108) 7.17.1 (0-32)(0-32) SW846 8270CSW846 8270C

PentachlorophenolPentachlorophenol 16 a16 a (18 - 125)(18 - 125) SW846 8270CSW846 8270C 17 a17 a (18 - 125)(18 - 125) 8.78.7 (0-34)(0-34) SW846 8270CSW846 8270C

PhenolPhenol 7070 (39 - 105)(39 - 105) SW846 8270CSW846 8270C

7676 (39 - 105)(39 - 105) 7.57.5 (0-40)(0-40) SW846 8270CSW846 8270C

PyrenePyrene 8383 (39 - 113)(39 - 113) SW846 8270CSW846 8270C

8989 (39 - 113)(39 - 113) 6.76.7 (0-28)(0-28) SW846 8270CSW846 8270C

C9K060597 31 of 72

Client Lot #...:Client Lot #...: C9K060597 Work Order #...:Work Order #...: LN2MG1CA-MS Matrix.........:Matrix.........: SOLID MS Lot-Sample #:MS Lot-Sample #: C9K060597-002 LN2MG1CC-MSD

PERCENT RECOVERY

SURROGATE_________________________ RECOVERY________ LIMITS__________

Nitrobenzene-d5 77 (27 - 110)

81 (27 - 110) Terphenyl-d14 93 (21 - 130)

96 (21 - 130) 2-Fluorobiphenyl 84 (28 - 108)

86 (28 - 108) 2-Fluorophenol 79 (28 - 107)

80 (28 - 107) Phenol-d5 82 (30 - 112)

86 (30 - 112) 2,4,6-Tribromophenol 70 (21 - 116)

72 (21 - 116)

NOTE(S):NOTE(S):______________________________________________________________________________________________________________________________________________________________________________________ Calculations are performed before rounding to avoid round-off errors in calculated results.

Bold print denotes control parameters

Results and reporting limits have been adjusted for dry weight.

a Spiked analyte recovery is outside stated control limits.

C9K060597 32 of 72

GC SemivolatilesGC Semivolatiles

Lot-Sample #...:Lot-Sample #...: C9K060597-001 Work Order #...:Work Order #...: LN2ME1A6 Matrix.........:Matrix.........: SOLID Date Sampled...:Date Sampled...: 11/03/09 Date Received..:Date Received..: 11/06/09 MS Run #.......:MS Run #.......: 9314318 Prep Date......:Prep Date......: 11/10/09 Analysis Date..:Analysis Date..: 11/19/09 Prep Batch #...:Prep Batch #...: 9314573 Analysis Time..:Analysis Time..: 18:46 Dilution Factor:Dilution Factor: 0.75 % Moisture.....:% Moisture.....: 26 Method.........:Method.........: SW846 8081B

REPORTING

PARAMETER______________________________ RESULT_______________ LIMIT_________ UNITS_________ MDL_______________ alpha-BHC ND 1.7 ug/kg 0.27 beta-BHCbeta-BHC 0.81 J0.81 J 1.71.7 ug/kgug/kg 0.440.44 delta-BHC ND 1.7 ug/kg 0.26 gamma-BHC (Lindane) ND 1.7 ug/kg 0.29 Heptachlor ND 1.7 ug/kg 0.37 Aldrin ND 1.7 ug/kg 0.30 Heptachlor epoxide ND 1.7 ug/kg 0.33 Endosulfan IEndosulfan I 0.87 J,PG0.87 J,PG 1.71.7 ug/kgug/kg 0.320.32 Dieldrin ND 1.7 ug/kg 0.28 4,4'-DDE ND 1.7 ug/kg 0.25 Endrin ND 1.7 ug/kg 0.33 Endrin ketone ND 1.7 ug/kg 0.26 Endrin aldehyde ND 1.7 ug/kg 0.33 Endosulfan II ND 1.7 ug/kg 0.30 4,4'-DDD ND 1.7 ug/kg 0.22 Endosulfan sulfate ND 1.7 ug/kg 0.18 4,4'-DDT ND 1.7 ug/kg 0.25 Methoxychlor ND 3.3 ug/kg 0.35 alpha-Chlordane ND 1.7 ug/kg 0.33 gamma-Chlordane ND 1.7 ug/kg 0.33 Toxaphene ND 67 ug/kg 11

PERCENT RECOVERY

SURROGATE______________________________ RECOVERY_______________ LIMITS__________

Tetrachloro-m-xylene 70 (45 - 130) Decachlorobiphenyl 100 (45 - 130)

NOTE(S):NOTE(S):______________________________________________________________________________________________________________________________________________________________________________ Results and reporting limits have been adjusted for dry weight.

J Estimated result. Result is less than RL.

PG The percent difference between the original and confirmation analyses is greater than 40%.

C9K060597 33 of 72

GC SemivolatilesGC Semivolatiles

Lot-Sample #...:Lot-Sample #...: C9K060597-002 Work Order #...:Work Order #...: LN2MG1AH Matrix.........:Matrix.........: SOLID Date Sampled...:Date Sampled...: 11/03/09 Date Received..:Date Received..: 11/06/09 MS Run #.......:MS Run #.......: 9314318 Prep Date......:Prep Date......: 11/10/09 Analysis Date..:Analysis Date..: 11/19/09 Prep Batch #...:Prep Batch #...: 9314573 Analysis Time..:Analysis Time..: 19:15 Dilution Factor:Dilution Factor: 0.7 % Moisture.....:% Moisture.....: 26 Method.........:Method.........: SW846 8081B

REPORTING

PARAMETER______________________________ RESULT_______________ LIMIT_________ UNITS_________ MDL_______________ alpha-BHC ND 1.6 ug/kg 0.26 beta-BHC ND 1.6 ug/kg 0.41 delta-BHC ND 1.6 ug/kg 0.24 gamma-BHC (Lindane) ND 1.6 ug/kg 0.28 Heptachlor ND 1.6 ug/kg 0.35 Aldrin ND 1.6 ug/kg 0.28 Heptachlor epoxide ND 1.6 ug/kg 0.31 Endosulfan IEndosulfan I 0.32 J,PG0.32 J,PG 1.61.6 ug/kgug/kg 0.300.30 Dieldrin ND 1.6 ug/kg 0.26 4,4'-DDE4,4'-DDE 0.59 J0.59 J 1.61.6 ug/kgug/kg 0.240.24 Endrin ND 1.6 ug/kg 0.31 Endrin ketone ND 1.6 ug/kg 0.25 Endrin aldehyde ND 1.6 ug/kg 0.31 Endosulfan II ND 1.6 ug/kg 0.28 4,4'-DDD ND 1.6 ug/kg 0.21 Endosulfan sulfate ND 1.6 ug/kg 0.16 4,4'-DDT ND 1.6 ug/kg 0.24 Methoxychlor ND 3.1 ug/kg 0.33 alpha-Chlordane ND 1.6 ug/kg 0.31 gamma-Chlordane ND 1.6 ug/kg 0.31 Toxaphene ND 63 ug/kg 11

PERCENT RECOVERY

SURROGATE______________________________ RECOVERY_______________ LIMITS__________

Tetrachloro-m-xylene 54 (45 - 130) Decachlorobiphenyl 77 (45 - 130)

NOTE(S):NOTE(S):______________________________________________________________________________________________________________________________________________________________________________ Results and reporting limits have been adjusted for dry weight.

J Estimated result. Result is less than RL.

C9K060597 34 of 72

GC SemivolatilesGC Semivolatiles

Lot-Sample #...:Lot-Sample #...: C9K060597-003 Work Order #...:Work Order #...: LN2MK1AH Matrix.........:Matrix.........: SOLID Date Sampled...:Date Sampled...: 11/03/09 Date Received..:Date Received..: 11/06/09 MS Run #.......:MS Run #.......: 9314318 Prep Date......:Prep Date......: 11/10/09 Analysis Date..:Analysis Date..: 11/19/09 Prep Batch #...:Prep Batch #...: 9314573 Analysis Time..:Analysis Time..: 20:40 Dilution Factor:Dilution Factor: 0.75 % Moisture.....:% Moisture.....: 24 Method.........:Method.........: SW846 8081B

REPORTING

PARAMETER______________________________ RESULT_______________ LIMIT_________ UNITS_________ MDL_______________ alpha-BHC ND 1.7 ug/kg 0.27 beta-BHC ND 1.7 ug/kg 0.43 delta-BHC ND 1.7 ug/kg 0.25 gamma-BHC (Lindane) ND 1.7 ug/kg 0.29 Heptachlor ND 1.7 ug/kg 0.37 Aldrin ND 1.7 ug/kg 0.29 Heptachlor epoxide ND 1.7 ug/kg 0.32 Endosulfan IEndosulfan I 0.55…

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