J34786-1 UDS Level 2 Report Final Report.pdf

ANALYTICAL REPORT

TestAmerica Laboratories, Inc.

TestAmerica Pittsburgh 301 Alpha Drive RIDC Park Pittsburgh, PA 15238 Tel: (412)963-7058

TestAmerica Job ID: 180-34786-1 Client Project/Site: Paint Chips

For:

911th Airlift Wing 1100 Herman Ave--B-333 Pittsburgh IAP/ARS Coraopolis, Pennsylvania 15108-4421

Attn: Adrian Mood

Authorized for release by:

7/17/2014 3:00:12 PM

Veronica Bortot, Senior Project Manager (412)963-2435 veronica.bortot@testamericainc.com

This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature.

Results relate only to the items tested and the sample(s) as received by the laboratory.

https://secure.testamericainc.com/TotalAccess/login.aspx http://www.testamericainc.com/AskTheExpert/Expert_index.htm http://www.testamericainc.com mailto:veronica.bortot@testamericainc.com

Table of Contents

Client: 911th Airlift Wing Project/Site: Paint Chips

TestAmerica Job ID: 180-34786-1

TestAmerica Pittsburgh

7/17/2014

Cover Page

Table of Contents

Case Narrative

Definitions/Glossary

Certification Summary

Sample Summary

Method Summary

Lab Chronicle

Client Sample Results

QC Sample Results

QC Association Summary

Chain of Custody

Receipt Checklists

Case Narrative Client: 911th Airlift Wing TestAmerica Job ID: 180-34786-1

Project/Site: Paint Chips

Job ID: 180-34786-1

Laboratory: TestAmerica Pittsburgh

Narrative

Job Narrative

180-34786-1

Comments

No additional comments.

Receipt

The samples were received on 7/11/2014 3:50 PM; the samples arrived in good condition, properly preserved and, where required, on ice.

The temperature of the cooler at receipt was 3.9º C.

Except:

The COC lists one sample and two containers. It was very noticeable that there were two different samples, plus the bags were labeled sample 1 and sample 2. The PM was notified, and was told by the client that there would be two samples.

Metals

No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.

TestAmerica Pittsburgh Page 3 of 13 7/17/2014

Definitions/Glossary TestAmerica Job ID: 180-34786-1Client: 911th Airlift Wing

Project/Site: Paint Chips

Glossary

These commonly used abbreviations may or may not be present in this report.

¤ Listed under the "D" column to designate that the result is reported on a dry weight basis

Abbreviation

%R Percent Recovery

CFL Contains Free Liquid

CNF Contains no Free Liquid

DER Duplicate error ratio (normalized absolute difference)

Dil Fac Dilution Factor

DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample

DLC Decision level concentration

MDA Minimum detectable activity

EDL Estimated Detection Limit

MDC Minimum detectable concentration

MDL Method Detection Limit

ML Minimum Level (Dioxin)

NC Not Calculated

ND Not detected at the reporting limit (or MDL or EDL if shown)

PQL Practical Quantitation Limit

QC Quality Control

RER Relative error ratio

RL Reporting Limit or Requested Limit (Radiochemistry)

RPD Relative Percent Difference, a measure of the relative difference between two points

TEF Toxicity Equivalent Factor (Dioxin)

TEQ Toxicity Equivalent Quotient (Dioxin)

TestAmerica Pittsburgh

Page 4 of 13 7/17/2014

Certification Summary

Project/Site: Paint Chips

Laboratory: TestAmerica Pittsburgh All certifications held by this laboratory are listed. Not all certifications are applicable to this report.

Authority Program EPA Region Certification ID Expiration Date

Arkansas DEQ 88-06906State Program 06-27-15

California NELAP 9 4224CA 03-31-14 *

Connecticut State Program 1 PH-0688 09-30-14

Florida NELAP 4 E871008 06-30-15

Illinois NELAP 5 002602 06-30-15

Kansas NELAP 7 E-10350 01-31-15

Louisiana NELAP 6 04041 06-30-15

New Hampshire NELAP 1 203011 04-04-15

New Jersey NELAP 2 PA005 06-30-15

New York NELAP 2 11182 03-31-15

North Carolina (WW/SW) State Program 4 434 12-31-14

Pennsylvania NELAP 3 02-00416 04-30-15

South Carolina State Program 4 89014 04-30-14 *

Texas NELAP 6 T104704528 03-31-15

US Fish & Wildlife Federal LE94312A-1 11-30-14

USDA Federal P330-10-00139 05-23-16

Utah NELAP 8 STLP 05-31-15

Virginia NELAP 3 460189 09-14-14

West Virginia DEP State Program 3 142 01-31-15

Wisconsin State Program 5 998027800 08-31-14

TestAmerica Pittsburgh

* Certification renewal pending - certification considered valid.

Page 5 of 13 7/17/2014

Sample Summary

Project/Site: Paint Chips

Lab Sample ID Client Sample ID ReceivedCollectedMatrix

180-34786-1 PAINT CHIPS SAMPLE 1 Solid 07/11/14 14:30 07/11/14 15:50

180-34786-2 PAINT CHIPS SAMPLE 2 Solid 07/11/14 14:30 07/11/14 15:50

TestAmerica Pittsburgh

Page 6 of 13 7/17/2014

Method Summary

Project/Site: Paint Chips

Method Method Description LaboratoryProtocol

SW8466010C Metals (ICP) TAL PIT

Protocol References:

SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.

Laboratory References:

TAL PIT = TestAmerica Pittsburgh, 301 Alpha Drive, RIDC Park, Pittsburgh, PA 15238, TEL (412)963-7058

TestAmerica Pittsburgh

Page 7 of 13 7/17/2014

Lab Chronicle

Project/Site: Paint Chips

Client Sample ID: PAINT CHIPS SAMPLE 1 Lab Sample ID: 180-34786-1 Matrix: SolidDate Collected: 07/11/14 14:30

Date Received: 07/11/14 15:50

Prep 3050B RJR07/15/14 06:30 TAL PIT111434

Type

Batch

Method

Batch

Prep Type LabAnalystRun

Prepared or Analyzed

Initial

Amount Amount

Final Batch

NumberFactor

Dil

Total/NA 00000.99 g 100 mL

Analysis 6010C 1 111692 07/16/14 12:38 RJG TAL PITTotal/NA 00000.99 g 100 mL

CInstrument ID:

Client Sample ID: PAINT CHIPS SAMPLE 2 Lab Sample ID: 180-34786-2 Matrix: SolidDate Collected: 07/11/14 14:30

Date Received: 07/11/14 15:50

Prep 3050B RJR07/15/14 06:30 TAL PIT111434

Type

Batch

Method

Batch

Prep Type LabAnalystRun

Prepared or Analyzed

Initial

Amount Amount

Final Batch

NumberFactor

Dil

Total/NA 00001.04 g 100 mL

Analysis 6010C 1 111692 07/16/14 12:44 RJG TAL PITTotal/NA 00001.04 g 100 mL

CInstrument ID:

Laboratory References:

TAL PIT = TestAmerica Pittsburgh, 301 Alpha Drive, RIDC Park, Pittsburgh, PA 15238, TEL (412)963-7058

Analyst References:

Lab: TAL PIT

Batch Type: Prep

RJR = Ron Rosenbaum

Batch Type: Analysis

RJG = Rob Good

TestAmerica Pittsburgh

Page 8 of 13 7/17/2014

Client Sample Results

Project/Site: Paint Chips

Lab Sample ID: 180-34786-1Client Sample ID: PAINT CHIPS SAMPLE 1 Matrix: SolidDate Collected: 07/11/14 14:30

Date Received: 07/11/14 15:50

Method: 6010C - Metals (ICP)

RL MDL

Lead 120 1.0 0.10 mg/Kg 07/15/14 06:30 07/16/14 12:38 1

Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier

Lab Sample ID: 180-34786-2Client Sample ID: PAINT CHIPS SAMPLE 2 Matrix: SolidDate Collected: 07/11/14 14:30

Date Received: 07/11/14 15:50

Method: 6010C - Metals (ICP)

RL MDL

Lead 190 0.96 0.098 mg/Kg 07/15/14 06:30 07/16/14 12:44 1

Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier

TestAmerica Pittsburgh

Page 9 of 13 7/17/2014

QC Sample Results

Project/Site: Paint Chips

Method: 6010C - Metals (ICP)

Client Sample ID: Method BlankLab Sample ID: MB 180-111434/1-A

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 111692 Prep Batch: 111434

RL MDL

Lead ND 1.0 0.10 mg/Kg 07/15/14 06:30 07/16/14 11:27 1

MB MB

Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier

Client Sample ID: Lab Control SampleLab Sample ID: LCS 180-111434/2-A

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 111692 Prep Batch: 111434

Lead 50.0 45.3 mg/Kg 91 80 - 120

Analyte

LCS LCS

DUnitResult Qualifier %Rec

Spike

Added

%Rec.

Limits

TestAmerica Pittsburgh

Page 10 of 13 7/17/2014

QC Association Summary

Project/Site: Paint Chips

Metals

Prep Batch: 111434

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Solid 3050B180-34786-1 PAINT CHIPS SAMPLE 1 Total/NA

Solid 3050B180-34786-2 PAINT CHIPS SAMPLE 2 Total/NA

Solid 3050BLCS 180-111434/2-A Lab Control Sample Total/NA

Solid 3050BMB 180-111434/1-A Method Blank Total/NA

Analysis Batch: 111692

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Solid 6010C 111434180-34786-1 PAINT CHIPS SAMPLE 1 Total/NA

Solid 6010C 111434180-34786-2 PAINT CHIPS SAMPLE 2 Total/NA

Solid 6010C 111434LCS 180-111434/2-A Lab Control Sample Total/NA

Solid 6010C 111434MB 180-111434/1-A Method Blank Total/NA

TestAmerica Pittsburgh

Page 11 of 13 7/17/2014

Page 12 of 137/17/2014

Login Sample Receipt Checklist

Client: 911th Airlift Wing Job Number: 180-34786-1

Login Number: 34786

Question Answer Comment

Creator: Watson, Debbie

List Source: TestAmerica Pittsburgh

List Number: 1

TrueRadioactivity wasn't checked or is </= background as measured by a survey meter.

TrueThe cooler's custody seal, if present, is intact.

TrueSample custody seals, if present, are intact.

TrueThe cooler or samples do not appear to have been compromised or tampered with.

TrueSamples were received on ice.

TrueCooler Temperature is acceptable.

TrueCooler Temperature is recorded.

TrueCOC is present.

TrueCOC is filled out in ink and legible.

TrueCOC is filled out with all pertinent information.

TrueIs the Field Sampler's name present on COC?

TrueThere are no discrepancies between the containers received and the COC.

TrueSamples are received within Holding Time.

TrueSample containers have legible labels.

TrueContainers are not broken or leaking.

TrueSample collection date/times are provided.

TrueAppropriate sample containers are used.

TrueSample bottles are completely filled.

TrueSample Preservation Verified.

TrueThere is sufficient vol. for all requested analyses, incl. any requested

MS/MSDs

TrueContainers requiring zero headspace have no headspace or bubble is

<6mm (1/4").

TrueMultiphasic samples are not present.

TrueSamples do not require splitting or compositing.

N/AResidual Chlorine Checked.

TestAmerica Pittsburgh Page 13 of 13 7/17/2014