Attachment_4.pdf

PRE-DEMOLITION SURVEY REPORT

FOR

HAZARDOUS MATERIALS

AT

CRAB ORCHARD NWR

6987 HEAD QUARTERS RD.

MARION, IL 62959

CLIENT:

UNITED STATES DEPT. OF THE INTERIOR

U.S. FISH & WILDLIFE SERVICES

5275 LEESBURG PIKE

FALLS CHURCH, VA 22041

FWS 140F0622Q0015

INSPECTION DATES:

FEBRUARY 15-16, 2022

PRIME CONTRACTOR:

CASTLE HILL ASSOCIATES, LLC

1197 FARNSWORTH RD. – UNIT E

WATERVILLE, OH 43566

567-952-0212

PRE-DEMOLTION SURVEY FOR HAZARDOUS MATERIALS

CRAB ORCHARD NWR – MARION, IL

FEBRUARY 2022

TABLE OF CONTENTS

1. HAZMAT INSPECTION SUMMARY

A. ASBESTOS CONTAINING MATERIALS

B. LEAD-BASED PAINT

C. UNIVERSAL WASTES

2. ASBESTOS SAMPLING DATA, INVENTORY BY BUILDING, AND

PHOTOS

• INSPECTION SUMMARY

• LISTING OF INSPECTED BUILDINGS

• BUILDINGS WITH NO ASBESTOS CONTAINING MATERIALS

• INVENTORY OF ASBESTOS MATERIALS BY BUILDING

• ASBESTOS BULK SAMPLING DATA

• ASBESTOS CONTAINING MATERIAL PHOTOS

3. LEAD PAINT SAMPLING DATA

• LEAD-BASED PAINT COMPONENTS INVENTORY

4. UNIVERSAL WASTES & HAZMAT

• UNIVERSAL WASTE & HAZMAT MATERIAL INVENTORY

APPENDICES

Appendix A – Asbestos Sample Location Drawings

Appendix B – Lead Paint XRF Testing Data

Appendix C – Asbestos Laboratory Report

Appendix D – Inspector Certifications

Appendix E – Laboratory Certifications

HAZMAT INSPECTION SUMMARY

PROJECT SUMMARY

On February 15-16, 2022, Castle Hill Associates performed hazardous materials (HazMat) inspections prior to planned demolition of the following buildings at Crab Orchard NWR in Marion, IL:

AREA

FACILITIES # OR

DESCRIPTION

BLDG. NUMBER BUILDING USE SF

2D 10068288

BLDG 1-10, 1-10A, 1-10B

(GD)

VACANT STORAGE 186

2D 10068290 BLDG 1-9 (GD) VACANT STORAGE 565

2D 10068291 BLDG 1-6 (GD) VACANT PRODUCTION BLDG. 11,808

2D 10068301 BLDG 1-11 (GD) VACANT PRODUCTION BLDG. 2,001

2D 10068303 BLDG 1-4 (GD) VACANT PRODUCTION 2,088

2D 10068304 BLDG 1-8 (GD) VACANT PRODUCTION BLDG. 8,453

2D

SMALL MIXING HOUSES &

MISC BUILDINGS

16 SMALL MIXING HOUSES SMALL METAL MIXING HOUSES 12,000

2D STEAMLINES PIPE RACKS

OVERHEAD PIPE RACKS & ON

GROUND

2,240 LF

I Area, Area 9

10068263 BLDG I-1-25 VACANT GD LAB BUILDING 7,072

7 10013435 BLDG IN-3-2 (GD) STORAGE WAREHOUSE BLDG 10,250

7 10013436 BLDG IN-3-3 (GD) STORAGE WAREHOUSE BLDG 10,250

7 10013448 BLDG IN-6-2 (GD) STORAGE WAREHOUSE BLDG 10,250

7 10013439 BLDG IN-4-1 (GD) STORAGE WAREHOUSE BLDG 10,250

7 10013420

BLDG IN-1-1

(EMA/SHERIFF)

STORAGE WAREHOUSE BLDG 10,250

7 10013421 BLDG IN-1-2 (HAB HUM) STORAGE WAREHOUSE BLDG 10,250

7 10013443 BLDG IN-4-6 (OLIN) STORAGE WAREHOUSE BLDG 10,250

7 10013445 BLDG IN-5-4 (IDNR) STORAGE WAREHOUSE BLDG 10,250

7 10013449 BLDG IN-6-5 (USFWS) STORAGE WAREHOUSE BLDG 10,250

7 10013444 BLDG IN-5-1 (USFW) STORAGE WAREHOUSE BLDG 10,250

7 10013447

AREA-7, BLDG IN-6-1

(USFW)

STORAGE WAREHOUSE BLDG 10,250

7 10013427 BLDG IN-2-1 (VACANT) STORAGE WAREHOUSE BLDG 10,250

7 10013597 QUONSET VACANT QUONSET 940

A-3-2 10013416 BLDG A-3-2

OLD CRAB ORCHARD VISITOR

CENTER

3,455

S Area 10013406 BLDG 1-2 (IL DNR) EQUIP VEHICLE STORAGE 4,107

The work was conducted in accordance with the SOW issued by the USFWS on February 15-16, 2022.

The SOW specified the following materials be inspected, tested, and quantified in the buildings:

1. Asbestos-Containing Materials (ACM)

2. Lead in Paint (XRF)

3. ORM’s (Universal Wastes/Hazardous Components)

INSPECTOR INFORMATION

Asbestos Inspector: Brett Brumbaugh Certification: Asbestos Inspector, State of Illinois License #: 100-09972 Expiration: 05/15/22

Lead Inspector: Eric Columbo Certification: Lead Risk Assessor, State of Illinois License #: 007571 Expiration: 01/31/23

HazMat Inspector: Brett L. Brumbaugh, REPA, CESCO Certifications: Registered Environmental Property Assessor – REPA #5866

Certified Environmental Safety and Compliance Officer – CESCO #123337

PROJECT SCOPE OF WORK

The scope of this project was intended to perform all work necessary for and incidental to the inspection of structures prior to building renovations, demolition and/or deconstruction to determine the presence of asbestos, lead, and hazardous materials. This scope included sampling, testing and an assessment for Asbestos Containing Material (ACM), Lead Based Paint (LBP), and hazardous material survey prior to the demolition of building(s) and/or to perform repairs or maintenance to building(s) that are occupied.

Buildings listed as scheduled for demolition included destructive testing to determine presence of asbestos. Buildings that are not scheduled for demolition tested all materials that were accessible.

Material that was not accessible was assumed to be an asbestos contaminated material. The areas inspected included all interior areas, exteriors, roofs, interstitial spaces, wall spaces, and mechanical systems.

The surveys were performed in accordance with all applicable regulations of the State of Illinois, Occupational Safety and Health Administration (OSHA) and the United States Environmental Protection Agency (EPA).

Asbestos bulk sampling was conducted in accordance with the US EPA established guidelines document, "Guidance for Controlling Asbestos-Containing Materials in Buildings" (USEPA 560/5-85-024, 1985) and USEPA 40 CFR Part 763.86 "Asbestos-Containing Materials in Schools, Final Rule" (AHERA). Each bulk sample was analyzed for asbestos content by Polarized Light Microscopy (PLM) Method EPA - 600/R-93-116 Visual Area Estimation.

The Lead XRF surveys tested all interior and exterior building components in the buildings with an XRF handheld analyzer to identify the components which have lead-based paint (LBP).

The ORM/Universal Waste Survey was conducted by a visual inspection and inventory of the interior and exterior of the building for other hazardous components, including but not limited to: universal wastes such as fluorescent light tubes/bulbs, mercury-vapor light bulbs, polychlorinated biphenyl (PCB) containing items such as light ballasts, electrical transformers, batteries for exit and emergency lights, spent lead acid or Ni/Cd batteries, mercury- containing thermostats, smoke detectors, ozone depleting potential (ODP) and global warming potential (GWP) refrigerants, and fire extinguishers.

Explosives testing and residual explosive dust testing was not including in this scope of work and was conducted as part of a separate contract.

INSPECTION SUMMARY & FINDINGS

ASBESTOS CONTAINING MATERIALS (ACM)

Asbestos Sampling Overview A total of 157 asbestos bulk samples (185 sample layers) were collected from the buildings as part of this project. Sampling was not conducted for the exterior Galbestos® siding at the direction of the USFWS since this material has been previously tested and known to contain asbestos. All bulk sampling of suspected asbestos was based upon the appearance, texture, and location of the material in accordance with US EPA NESHAP regulations. All bulk samples were analyzed utilizing current EPA methods for PLM (Polarized Light Microscopy) by Eurofins/EMLab/P&K Laboratory in Marlton, NJ. The laboratory is accredited by the NIST, NVLAP program (National Institute of Standards and Technology, National Voluntary Laboratory Accreditation Program) and also an American Industrial Hygiene Association (AIHA) accredited laboratory.

BUILDINGS WITH NO ASBESTOS MATERIALS IDENTIFIED

As a result of the inspections and testing, the following buildings did not contain any asbestos containing materials:

AREA BLDG. NUMBER BUILDING USE

2D Pipe Racks Overhead Pipe Racks & Pipe on Ground

2D D-1-9 (W. of D-1-6) Metal Storage Building

2D D-1-17 Vacant Storage

2D D-1-26 Mix House

2D D-1-43 E. Mixer

2D D-1-45 Mix House

2D D-1-47 Mix House

2D D-1-56 Mix House

2D D-1-57 Mix House

2D D-1-68 Mix House

2D D-1-92 Metal Storage Bldg. E. of D-1-8

2D D-1-93 Metal Storage Bldg. E. of D-1-6

A-3-2 Former Visitor Center Vacant – Used for Storage

7 Quonset Hut Vacant Storage

BUILDINGS WITH ASBESTOS CONTAINING MATERIALS

AREA 2D

D-1-4 VACANT PRODUCTION BUILDING

ASBESTOS CONTAINING

MATERIALS

LOCATIONS QUANTITY

EPA ASBESTOS

CATEGORY

Window glazing E. windows 4 windows

64 lf Category 2 non-friable

Wiring inside original metal conduit w/white paint

Throughout building ~600 lf Category 2 non-friable

Gaskets in 4’ fluorescent light fixture glass enclosures

Throughout building 38 fixtures

380 lf Category 2 non-friable

D-1-6 VACANT PRODUCTION BUILDING

LOCATIONS QUANTITY

EPA ASBESTOS

CATEGORY

Transite cement siding Building lower exterior walls, E. & W. walkway walls, and Gable ends

4,970 sf + debris on ground

Category 2 non-friable

12” tan floor tile (negative mastic) N. restrooms 220 sf Category 1 non-friable

Window glazing E. windows and S.E.

breezeway windows

34 windows 340 lf

Category 2 non-friable

Window frame caulk E. windows and S.E.

breezeway windows

34 windows 340 lf

Category 2 non-friable

Wiring inside original metal conduit w/white paint

Throughout building ~1,300 lf Category 2 non-friable

Gaskets in 4’ fluorescent light fixture glass enclosures

Throughout building 59 fixtures

590 lf Category 2 non-friable

Gaskets on metal blast doors E. & W. blast doors in middle mixing chambers

6 doors 144 lf

D-1-8 VACANT PRODUCTION BUILDING

LOCATIONS QUANTITY

EPA ASBESTOS

CATEGORY

Transite cement siding Building lower exterior walls and Gable ends

2,860 sf + debris on ground

Category 2 non-friable

9” tan floor tile (negative mastic) Office area 860 sf Category 1 non-friable

12” white floor tile and black mastic Office storage room 120 sf Category 1 non-friable

Window glazing Windows in S.W. breezeway 2 windows

22 lf Category 2 non-friable

Wiring inside original metal conduit w/white paint

Throughout building ~1,300 lf Category 2 non-friable

Gaskets in 4’ fluorescent light fixture glass enclosures

Throughout building 40 fixtures

400 lf Category 2 non-friable

Gaskets in round incandescent light fixtures with glass enclosures

E. & W. exterior walkways 9 fixtures Category 2 non-friable

BUILDINGS WITH ASBESTOS CONTAINING MATERIALS (Cont.)

D-1-10 VACANT STORAGE

LOCATIONS QUANTITY

EPA ASBESTOS

CATEGORY

Gaskets in 4’ fluorescent light fixture glass enclosures

Throughout building 2 fixtures

20 lf

D-1-10A MIX HOUSE

LOCATIONS QUANTITY

EPA ASBESTOS

CATEGORY

Exterior door frame caulk Entry door 1 door

18 lf

D-1-10B MIX HOUSE

LOCATIONS QUANTITY

EPA ASBESTOS

CATEGORY

Exterior door frame caulk Entry door 1 door

18 lf Category 2 non-friable

Transite cement interior wall and ceiling panels

Interior walls & ceiling 560 sf Category 2 non-friable

D-1-11 VACANT PRODUCTION BUILDING

LOCATIONS QUANTITY

EPA ASBESTOS

CATEGORY

Wiring inside original metal conduit w/white paint

Throughout building ~700 lf Category 2 non-friable

D-1-29 MIX HOUSE

LOCATIONS QUANTITY

EPA ASBESTOS

CATEGORY

Gaskets in 4’ fluorescent light fixture glass enclosures

Throughout building 2 fixtures

D-1-47 MIX HOUSE

LOCATIONS QUANTITY

EPA ASBESTOS

CATEGORY

Gaskets in 4’ fluorescent light fixture glass enclosures

Throughout building 2 fixtures

D-1-44 MIX HOUSE

LOCATIONS QUANTITY

EPA ASBESTOS

CATEGORY

Gaskets in round incandescent light

Building interior 3 fixtures Category 2 non-friable

D-1-48 MIX HOUSE

LOCATIONS QUANTITY

EPA ASBESTOS

CATEGORY

Gaskets in 4’ fluorescent light fixture glass enclosures

Throughout building 2 fixtures

D-1-49 MIX HOUSE

LOCATIONS QUANTITY

EPA ASBESTOS

CATEGORY

Gaskets in 4’ fluorescent light fixture glass enclosures

Throughout building 2 fixtures

D-1-58 MIX HOUSE

LOCATIONS QUANTITY

EPA ASBESTOS

CATEGORY

Gaskets in round incandescent light

Building interior 2 fixtures Category 2 non-friable

S AREA

S-1-2 EQUIPMENT STORAGE BUILDING

LOCATIONS QUANTITY

EPA ASBESTOS

CATEGORY

Galbestos corrugated metal siding and roofing

Exterior walls, roof, window trim, and corner trim

8,740 sf + debris on ground

Category 2 non-friable

Exterior window frame caulking Exterior windows 12 windows

336 sf Category 2 non-friable

Transite cement energy panels (2 layers of transite with interior insul.)

Middle storage room walls and ceiling

1,015 sf Category 2 non-friable

Mag block pipe insulation S. equipment storage room 10 lf RACM

I AREA-AREA 9

I-1-25 VACANT PRODUCTION BUILDING

LOCATIONS QUANTITY

EPA ASBESTOS

CATEGORY

Transite roofing shingles Roof 4,080 sf

+ debris on ground Category 2 non-friable

12” tan floor tile (negative mastic) 1st floor N.E. storage room 256 sf Category 1 non-friable

12” white floor tile (negative mastic) 2nd floor break room and restrooms incl. hallway

1,716 sf Category 1 non-friable

Transite cement energy panels (2 layers of transite with interior insul.)

2nd floor ceilings 2,178 sf Category 2 non-friable

Tar roof seam crack sealant 2nd floor S. concrete roof 64 sf Category 1 non-friable

AREA 7

IN-1-1 STORAGE WAREHOUSE BUILDING

LOCATIONS QUANTITY

EPA ASBESTOS

CATEGORY

Galbestos corrugated metal siding and roofing

Exterior walls, roof, window trim, and corner trim

22,076 sf Category 2 non-friable

Galbestos paper debris on ground Building perimeter on concrete and in soil/vegetation

Surrounding all sides of building

Category 2 non-friable

Exterior window frame caulking Exterior windows 18 windows

288 Lf

IN-1-2 STORAGE WAREHOUSE BUILDING

LOCATIONS QUANTITY

EPA ASBESTOS

CATEGORY

Galbestos corrugated metal siding and roofing

Exterior walls, roof, window trim, and corner trim

22,076 sf Category 2 non-friable

Galbestos paper debris on ground Building perimeter on concrete and in soil/vegetation

Surrounding all sides of building

Category 2 non-friable

Exterior window frame caulking Exterior windows 18 windows

IN-2-1 STORAGE WAREHOUSE BUILDING

LOCATIONS QUANTITY

EPA ASBESTOS

CATEGORY

Galbestos corrugated metal siding and roofing

Exterior walls, roof, window trim, and corner trim

22,076 sf Category 2 non-friable

Galbestos paper debris on ground Building perimeter on concrete and in soil/vegetation

Surrounding all sides of building

Category 2 non-friable

Exterior window frame caulking Exterior windows 18 windows

IN-3-2 STORAGE WAREHOUSE BUILDING

LOCATIONS QUANTITY

EPA ASBESTOS

CATEGORY

Galbestos corrugated metal siding and roofing

Exterior walls, roof, window trim, and corner trim

22,076 sf Category 2 non-friable

Galbestos paper debris on ground Building perimeter on concrete and in soil/vegetation

Surrounding all sides of building

Category 2 non-friable

Exterior window frame caulking Exterior windows 18 windows

IN-3-3 STORAGE WAREHOUSE BUILDING

LOCATIONS QUANTITY

EPA ASBESTOS

CATEGORY

Galbestos corrugated metal siding and roofing

Exterior walls, roof, window trim, and corner trim

22,076 sf Category 2 non-friable

Galbestos paper debris on ground Building perimeter on concrete and in soil/vegetation

Surrounding all sides of building

Category 2 non-friable

Exterior window frame caulking Exterior windows 18 windows

IN-4-1 STORAGE WAREHOUSE BUILDING

LOCATIONS QUANTITY

EPA ASBESTOS

CATEGORY

Galbestos corrugated metal siding and roofing

Exterior walls, roof, window trim, and corner trim

22,076 sf Category 2 non-friable

Galbestos paper debris on ground Building perimeter on concrete and in soil/vegetation

Surrounding all sides of building

Category 2 non-friable

Exterior window frame caulking Exterior windows 18 windows

IN-4-6 STORAGE WAREHOUSE BUILDING

LOCATIONS QUANTITY

EPA ASBESTOS

CATEGORY

Galbestos corrugated metal siding and roofing

Exterior walls, roof, window trim, and corner trim

22,076 sf Category 2 non-friable

Galbestos paper debris on ground Building perimeter on concrete and in soil/vegetation

Surrounding all sides of building

Category 2 non-friable

Exterior window frame caulking Exterior windows 18 windows

IN-5-4 STORAGE WAREHOUSE BUILDING

LOCATIONS QUANTITY

EPA ASBESTOS

CATEGORY

Galbestos corrugated metal siding and roofing

Exterior walls, roof, window trim, and corner trim

22,076 sf Category 2 non-friable

Galbestos paper debris on ground Building perimeter on concrete and in soil/vegetation

Surrounding all sides of building

Category 2 non-friable

Exterior window frame caulking Exterior windows 18 windows

IN-6-1 STORAGE WAREHOUSE BUILDING

LOCATIONS QUANTITY

EPA ASBESTOS

CATEGORY

Galbestos corrugated metal siding and roofing

Exterior walls, roof, window trim, and corner trim

22,076 sf Category 2 non-friable

Galbestos paper debris on ground Building perimeter on concrete and in soil/vegetation

Surrounding all sides of building

Category 2 non-friable

Exterior window frame caulking Exterior windows 18 windows

IN-6-2 STORAGE WAREHOUSE BUILDING

LOCATIONS QUANTITY

EPA ASBESTOS

CATEGORY

Galbestos corrugated metal siding and roofing

Exterior walls, roof, window trim, and corner trim

22,076 sf Category 2 non-friable

Galbestos paper debris on ground Building perimeter on concrete and in soil/vegetation

Surrounding all sides of building

Category 2 non-friable

Exterior window frame caulking Exterior windows 18 windows

IN-6-5 STORAGE WAREHOUSE BUILDING

LOCATIONS QUANTITY

EPA ASBESTOS

CATEGORY

Galbestos corrugated metal siding and roofing

Exterior walls, roof, window trim, and corner trim

22,076 sf Category 2 non-friable

Galbestos paper debris on ground Building perimeter on concrete and in soil/vegetation

Surrounding all sides of building

Category 2 non-friable

Exterior window frame caulking Exterior windows 18 windows

LEAD PAINT

RESULTS OF LEAD XRF TESTING OF PAINT

As a result of the XRF testing of all major building components, the following components have been identified as having lead-based paint or coatings:

D-1-6

• Interior wood ceilings in hallways

• Exterior wood soffits

D-1-8

• Exterior wood entry doors

• Exterior wood soffits

D-1-10

• Exterior wood entry doors

Pipe Rack/Bridge between D-1-10 and D-1-11

• Metal supports

I AREA / AREA 9

I-1-25

• Interior wood passage doors

S-1-2

• Wood overhead garage doors

• Yellow floor striping on concrete

IN-1-1

IN-1-2

IN-2-1

AREA 7 (cont.)

IN-3-2

IN-3-3

IN-4-1

IN-4-6

IN-5-1

IN-5-4

IN-6-1

IN-6-2

IN-6-5

RECOMMENDATIONS FOR LEAD PAINTED COMPONENTS

The lead painted components identified in the buildings are not required to be removed prior to demolition. The Occupational Safety & Health Administration (OSHA) regulates workers exposure to lead paint concentrations in any amount, therefore, in order to satisfy OSHA requirements, worker protection and monitoring may be required for work activities that disturb paints that contain lead in any amount. In accordance with the OSHA Construction Standard for

Lead (29 CFR 1926.62), it is the contractors’ responsibility to protect their workers when an employee may be occupationally exposed to lead.

UNIVERSAL WASTE/HAZMAT SURVEY

INSPECTION OVERVIEW

The ORM/Universal Waste Survey was conducted by a visual inspection and inventory of the interior and exterior of the building for other hazardous components, including but not limited to: universal wastes such as fluorescent light tubes/bulbs, mercury-vapor light bulbs, polychlorinated biphenyl (PCB) containing items such as light ballasts, electrical transformers, batteries for exit and emergency lights, spent lead acid or Ni/Cd batteries, mercury- containing thermostats, smoke detectors, ozone depleting potential (ODP) and global warming potential (GWP) refrigerants, and fire extinguishers. Per the PWS, no testing was conducted for these materials, just a visual inventory.

ORM/HAZMAT FINDINGS

As a result of this inspection, the following ORM/HazMat Components were identified in the buildings:

HazMat Material Building Components Quantity

Mercury Fluorescent Tubes Light fixtures 74 tubes

PCB light fixture ballasts Light fixtures 37 each

Hg/Sodium high pressure light bulbs Exterior light fixtures 1 each

HazMat Material Building Components Quantity

Mercury Fluorescent Tubes Light fixtures 122 tubes

PCB light fixture ballasts Light fixtures 61 each

Mercury Fluorescent Tubes Light fixtures 148 tubes

PCB light fixture ballasts Light fixtures 74 each

Mercury Fluorescent Tubes Light fixtures 4 tubes

PCB light fixture ballasts Light fixtures 2 each

D-1-10B MIX HOUSE

Mercury Fluorescent Tubes Light fixtures 2 tubes

PCB light fixture ballasts Light fixtures 1 each

D-1-17 VACANT STORAGE BUILDING

Mercury Fluorescent Tubes Light fixtures 10 tubes

PCB light fixture ballasts Light fixtures 5 each

Mercury Fluorescent Tubes Light fixtures 6 tubes

PCB light fixture ballasts Light fixtures 3 each

D-1-43 MIX HOUSE

Hg/Sodium high pressure light bulbs Exterior light fixtures 4 each

D-1-57 MIX HOUSE

D-1-58 MIX HOUSE

D-1-68 MIX HOUSE

AREA A-3-2

A-3-2 VACANT VISITOR CENTER

HazMat Material Building Components Quantity

Mercury Fluorescent Tubes Light fixtures 58 tubes

Mercury CFL Bulbs Round light fixtures 45 each

PCB light fixture ballasts Light fixtures 29 each

Fire extinguisher chemicals Fire Extinguishers 2 each

Batteries Exit light fixtures 6 each

I AREA / AREA 9

Mercury Fluorescent Tubes Light fixtures 58 tubes

Mercury Thermostats Thermostats 4 each

PCB light fixture ballasts Light fixtures 29 each

HazMat Material Building Components Quantity

Mercury Fluorescent Tubes Light fixtures 14 tubes

PCB light fixture ballasts Light fixtures 7 each

IN-1-1 STORAGE WAREHOUSE BUILDING

HazMat Material Building Components Quantity

IN-1-2 STORAGE WAREHOUSE BUILDING

Mercury CFL Fluorescent bulbs Light fixtures 30 bulbs

IN-2-1 STORAGE WAREHOUSE/OFFICE BUILDING

Mercury Fluorescent Tubes Light fixtures 110 tubes

Mercury CFL Bulbs Round light fixtures 8 each

Mercury thermostats Thermostats 1 each

PCB light fixture ballasts Light fixtures 55 each

Fire extinguisher chemicals Fire Extinguishers 2 each

Batteries Exit light fixtures 10 each

CFC refrigerants A/C compressor 1 each

IN-3-2 STORAGE WAREHOUSE BUILDING

Mercury Fluorescent Tubes Light fixtures 12 tubes

PCB light fixture ballasts Light fixtures 6 each

IN-3-3 STORAGE WAREHOUSE BUILDING

IN-4-6 STORAGE WAREHOUSE BUILDING

IN-6-1 STORAGE WAREHOUSE BUILDING

Mercury Fluorescent Tubes Light fixtures 18 tubes

PCB light fixture ballasts Light fixtures 9 each

IN-6-2 STORAGE WAREHOUSE BUILDING

IN-6-5 STORAGE WAREHOUSE BUILDING

HAZMAT RECOMMENDATIONS

The identified Universal Wastes and HazMat materials identified in the buildings are required to be removed prior to demolition. All items must be handled, transported, and disposed/recycled in an EPA approved facility by persons with proper training in the handling of Universal Wastes and Hazardous Materials as defined by OSHA and the US EPA.

ASBESTOS BULK SAMPLING DATA

ASBESTOS BULK SAMPLE DESCRIPTIONS & RESULTS

PLM by EPA Method 600/R-93/116

Location: Crab Orchard NWR - Marion, IL Sampling Date: February 15, 2022 Inspector: Brett Brumbaugh Analysis Date: February 22, 2022 Laboratory: Eurofins/EMLab/P&K Laboratory – Marlton, NJ Accreditation: NVLAP Asbestos Bulk Accredited Laboratory # 200844-0 Analytical Method: EPA 600/R-93/116

BLDG.

SAMPLE

MATERIAL DESCRIPTION SAMPLE LOCATION LABORATORY RESULT

D-1-6 1 Transite siding E. wall by N.E. corner of bldg. 12% Chrysotile Asbestos

D-1-6 2 Black tar paper under transite E. wall by N.E. corner of bldg. No Asbestos Detected

D-1-6 3 Black tar paper under transite W. wall in middle of bldg. No Asbestos Detected

D-1-6 4a Black roofing shingle E. Side of building No Asbestos Detected

D-1-6 4b Silver paint on roofing shingle E. Side of building No Asbestos Detected

D-1-6 5a Black roofing shingle W. Side of building No Asbestos Detected

D-1-6 5b Silver paint on roofing shingle W. Side of building No Asbestos Detected

D-1-6 6a 12” tan floor tile N. Men’s restroom 2% Chrysotile Asbestos

D-1-6 6b Yellow mastic “” No Asbestos Detected

D-1-6 7a 12” tan floor tile N. Women’s restroom 2% Chrysotile Asbestos

D-1-6 7b Yellow mastic “” No Asbestos Detected

D-1-6 8 Roofing tar paper W. side of building No Asbestos Detected

D-1-6 9 Roofing tar paper E. side of building No Asbestos Detected

D-1-6 10 Window glazing N.E. window wall 2% Chrysotile Asbestos

D-1-6 11 Window glazing S.E. window wall No Asbestos Detected

D-1-6 12 Blast door gasket W. side of building 35% Chrysotile Asbestos

D-1-6 13 White duct mastic on FG duct W. hallway by D-1-9 No Asbestos Detected

D-1-6 14 White duct mastic on FG duct W. hallway No Asbestos Detected

D-1-6 15 Drywall joint compound South storage area No Asbestos Detected

D-1-6 16 Drywall joint compound South storage area No Asbestos Detected

D-1-6 17 Drywall joint compound South storage area No Asbestos Detected

D-1-6 18 Mud fitting on fiberglass pipe Middle production room @ ceiling No Asbestos Detected

D-1-6 19 Mud fitting on fiberglass pipe North production room @ ceiling No Asbestos Detected

D-1-6 20 Mud fitting on fiberglass pipe South production room @ ceiling No Asbestos Detected

D-1-6 21a Black roofing shingle S.E. corner of building No Asbestos Detected

D-1-6 21b Silver paint on roofing shingle “” No Asbestos Detected

D-1-6 22a Black roofing shingle N.W. corner of building No Asbestos Detected

D-1-6 22b Silver paint on roofing shingle “” No Asbestos Detected

D-1-6 23 Tan window frame caulking Southeast breezeway windows 4% Chrysotile Asbestos

D-1-6 24 Tan window frame caulking Southeast breezeway windows 4% Chrysotile Asbestos

D-1-6 25 Window glazing Southeast breezeway windows 3% Chrysotile Asbestos

D-1-6 26 Fluor. Light fixture gasket Middle production room 45% Chrysotile Asbestos

D-1-10 27 Fluor. Light fixture gasket South production room 80% Chrysotile Asbestos

D-1-6 28 Drywall joint compound N.E. hallway No Asbestos Detected

D-1-4 29 Drywall joint compound Middle hallway area No Asbestos Detected

D-1-4 30 Drywall joint compound S.W. hallway area No Asbestos Detected

D-1-4 31 Tan window glazing E. wall windows 4% Chrysotile Asbestos

D-1-4 32 Tan window glazing E. wall windows 5% Chrysotile Asbestos

D-1-4 33 Tan window frame caulking E. wall windows No Asbestos Detected

D-1-4 34 Tan window frame caulking E. wall windows No Asbestos Detected

EPA Definition of an asbestos containing material: > 1% asbestos

Inspector: Brett Brumbaugh Analysis Date: February 22, 2022 Laboratory: Eurofins/EMLab/P&K Laboratory – Marlton, NJ

MATERIAL DESCRIPTION SAMPLE LOCATION LABORATORY RESULT

D-1-4 35 Roofing tar paper S.E. corner of building No Asbestos Detected

D-1-4 36 Roofing tar paper N.E. corner of building No Asbestos Detected

D-1-4 37 Foam roofing S.E. corner of building No Asbestos Detected

D-1-4 38 Foam roofing N.E. corner of building No Asbestos Detected

D-1-8 39 Transite siding W. wall by N.E. corner of bldg. 15% Chrysotile Asbestos

D-1-8 40 Black roofing shingle E. side of building No Asbestos Detected

D-1-8 41 Black roofing shingle W. side of building No Asbestos Detected

D-1-8 42 Roofing tar paper E. side of building No Asbestos Detected

D-1-8 43 Roofing tar paper W. side of building No Asbestos Detected

D-1-8 44 Siding tar paper E. side of building No Asbestos Detected

D-1-8 45 Siding tar paper W. side of building No Asbestos Detected

D-1-8 46 Mud fitting on fiberglass pipe Middle production room @ ceiling No Asbestos Detected

D-1-8 47 Mud fitting on fiberglass pipe North production room @ ceiling No Asbestos Detected

D-1-8 48 Mud fitting on fiberglass pipe South production room @ ceiling No Asbestos Detected

D-1-8 49 Fiberglass blast door gasket West hallway No Asbestos Detected

D-1-8 50a 9” tan floor tile Office area 4% Chrysotile Asbestos

D-1-8 50b Black mastic “” No Asbestos Detected

D-1-8 51a 9” tan floor tile Office area 4% Chrysotile Asbestos

D-1-8 51b Black mastic “” No Asbestos Detected

D-1-8 52a 12” white/beige floor tile Office storage room 4% Chrysotile Asbestos

D-1-8 52b Black mastic “” 2% Chrysotile Asbestos

D-1-8 53a 12” white/beige floor tile Office storage room 4% Chrysotile Asbestos

D-1-8 53b Black mastic “” 2% Chrysotile Asbestos

D-1-8 54a Brown cove base Office area No Asbestos Detected

D-1-8 54b Tan cove base mastic “” No Asbestos Detected

D-1-8 55a Brown cove base Office area No Asbestos Detected

D-1-8 55b Tan cove base mastic Office area No Asbestos Detected

D-1-8 56 12” ceiling tile Office area No Asbestos Detected

D-1-8 57 12” ceiling tile Office area No Asbestos Detected

D-1-8 58 Incand. light fixture gasket E. hallway 30% Chrysotile Asbestos

D-1-8 59 Window glazing S.W. breezeway 4% Chrysotile Asbestos

D-1-8 60 Window glazing S.W. breezeway 3% Chrysotile Asbestos

D-1-11 61 Drywall joint compound E. side of building No Asbestos Detected

D-1-11 62 Drywall joint compound Middle of building No Asbestos Detected

D-1-11 63 Drywall joint compound W. side of building No Asbestos Detected

D-1-11 64 Wire coating in metal conduit

S.W. hallway 60% Chrysotile Asbestos

D-1-8 65 Wire coating in metal conduit

S. side of building 60% Chrysotile Asbestos

Inspector: Brett Brumbaugh Analysis Date: February 22, 2022 Laboratory: Eurofins/EMLab/P&K Laboratory – Marlton, NJ

MATERIAL DESCRIPTION SAMPLE LOCATION LABORATORY RESULT

D-1-10A 66 Door frame caulking E. Door frame 4% Chrysotile Asbestos

D-1-10A 67 Door frame caulking W. door frame 4% Chrysotile Asbestos

D-1-10B 68 Black roofing shingle N. side of bldg. No Asbestos Detected

D-1-10B 69 Black roofing shingle S. side of bldg. No Asbestos Detected

D-1-10B 70 Roofing tar paper N. side of bldg. No Asbestos Detected

D-1-10B 71 Roofing tar paper S. side of bldg. No Asbestos Detected

D-1-10B 72 Door frame caulking N. entry door 3% Chrysotile Asbestos

D-1-10B 73 Door frame caulking S. entry door 3% Chrysotile Asbestos

D-1-10B 74 Ext. siding tar paper N. side of bldg. No Asbestos Detected

D-1-10B 75 Ext. siding tar paper S. side of bldg. No Asbestos Detected

D-1-10B 76 Transite siding E. wall interior 15% Chrysotile Asbestos

D-1-29 77 Drywall joint compound Building interior wall No Asbestos Detected

D-1-29 78 Drywall joint compound Building interior ceiling No Asbestos Detected

D-1-49 79 Door frame caulking Entry door No Asbestos Detected

D-1-49 80 Door frame caulking Entry door No Asbestos Detected

D-1-49 81 Tan wall panel seam caulking Interior wall panel No Asbestos Detected

D-1-49 82 Tan wall panel seam caulking Interior wall panel No Asbestos Detected

Vis. Ctr. 83 Ext. window caulk S. side of building No Asbestos Detected

Vis. Ctr. 84 Ext. window caulk W. side of building No Asbestos Detected

Vis. Ctr. 85 Drywall joint compound Hallway by back entry door No Asbestos Detected

Vis. Ctr. 86 Drywall joint compound Break room No Asbestos Detected

Vis. Ctr. 87 Drywall joint compound Lobby No Asbestos Detected

Vis. Ctr. 88a 12” blue floor tile Storage room No Asbestos Detected

Vis. Ctr. 88b Yellow mastic “” No Asbestos Detected

Vis. Ctr. 89a 12” blue floor tile Break room No Asbestos Detected

Vis. Ctr. 89b Yellow mastic “” No Asbestos Detected

S 1-2 90 Exterior window caulking S. side of building 8% Chrysotile Asbestos

S 1-2 91 Exterior window caulking N. side of building 8% Chrysotile Asbestos

S 1-2 92 Transite energy panel Middle storage room wall 15% Chrysotile Asbestos

S 1-2 93 Window glazing S. side of building No Asbestos Detected

S 1-2 94 Window glazing N. side of building No Asbestos Detected

S 1-2 95 Mag. block pipe insulation S. storage room 16% Chrysotile Asbestos

IN-6-1 96 Window glazing W. interior window No Asbestos Detected

IN-6-1 97 Window glazing E. interior window No Asbestos Detected

IN-5-1 98 Window glazing W. interior window No Asbestos Detected

IN-5-1 99 Window glazing E. interior window No Asbestos Detected

IN-5-1 100 Ext. window caulk N. exterior window frame 3% Chrysotile Asbestos

IN-6-1 101 Ext. window caulk N. exterior window frame 8% Chrysotile Asbestos

IN-6-1 102 Ext. window caulk E. exterior window frame 8% Chrysotile Asbestos

Inspector: Brett Brumbaugh Analysis Date: February 22, 2022 Laboratory: Eurofins/EMLab/P&K Laboratory – Marlton, NJ

MATERIAL DESCRIPTION SAMPLE LOCATION LABORATORY RESULT

IN-2-1 103 Popcorn spray-on ceiling Main office area at E. side of bldg. No Asbestos Detected

IN-2-1 104 Popcorn spray-on ceiling Main office area at E. side of bldg. No Asbestos Detected

IN-2-1 105 Popcorn spray-on ceiling Main office area at E. side of bldg. No Asbestos Detected

IN-2-1 106 Drywall joint compound Main office area at E. side of bldg. No Asbestos Detected

IN-2-1 107 Drywall joint compound Main office area at E. side of bldg. No Asbestos Detected

IN-2-1 108 Drywall joint compound Main office area restroom No Asbestos Detected

IN-2-1 109a Tan linoleum sheet flooring Main office area restroom No Asbestos Detected

IN-2-1 109b Yellow mastic Main office area restroom No Asbestos Detected

IN-2-1 110a Tan linoleum sheet flooring Main office area restroom No Asbestos Detected

IN-2-1 110b Yellow mastic Main office area restroom No Asbestos Detected

IN-2-1 111 Popcorn spray-on ceiling Main office area at E. side of bldg. No Asbestos Detected

IN-2-1 112 Popcorn spray-on ceiling Main office area at E. side of bldg. No Asbestos Detected

IN-2-1 113 Ext. window caulk N. side of building No Asbestos Detected

IN-2-1 114 Window glazing W. end of building interior No Asbestos Detected

IN-5-4 115 Exterior window caulking South side of building 5% Chrysotile Asbestos

IN-5-4 116 Window glazing W. building interior No Asbestos Detected

IN-6-5 117 Window glazing E. interior window No Asbestos Detected

D-1-9 118 Drywall joint compound Ceiling No Asbestos Detected

D-1-9 119 Drywall joint compound Ceiling No Asbestos Detected

Bunkers 120 Black asphalt coating on floor East bunker E. of D-1-43 mixer No Asbestos Detected

Bunkers 121 Black asphalt coating on floor East bunker E. of D-1-43 mixer No Asbestos Detected

Bunkers 122 Black asphalt coating on floor East bunker E. of D-1-43 mixer No Asbestos Detected

Sampling Date: February 16, 2022 Inspector: Brett Brumbaugh Analysis Date: February 22, 2022 Laboratory: Eurofins/EMLab/P&K Laboratory – Marlton, NJ

MATERIAL DESCRIPTION SAMPLE LOCATION LABORATORY RESULT

I-1-25 201 Transite roof shingle S.E. corner of roof 12% Chrysotile Asbestos

I-1-25 202 Window glazing 1st floor E. window No Asbestos Detected

I-1-25 203 Window glazing 1st floor W. window No Asbestos Detected

I-1-25 204a 12” tan floor tile 1st floor N. storage room 2% Chrysotile Asbestos

I-1-25 204b Black mastic “ No Asbestos Detected

I-1-25 205 Drywall mud 1st floor storage area No Asbestos Detected

I-1-25 206 Drywall mud 1st floor W. wall No Asbestos Detected

I-1-25 207a 12” white floor tile 2nd floor locker room 2% Chrysotile Asbestos

I-1-25 207b Black mastic “” No Asbestos Detected

I-1-25 208 Drywall mud 2nd floor locker room No Asbestos Detected

I-1-25 209a Tan cove base 2nd floor restroom No Asbestos Detected

I-1-25 209b Brown mastic “” No Asbestos Detected

I-1-25 210 Transite ceiling panel 2nd floor locker room 15% Chrysotile Asbestos

I-1-25 211 Roofing tar on seams 2nd balcony concrete roof deck 6% Chrysotile Asbestos

I-1-25 212 Tar paper on transite roof 2nd floor S.E. corner No Asbestos Detected

I-1-25 213 Tar paper on transite roof 2nd floor S.W. corner No Asbestos Detected

IN-6-2 214 Window glazing N. window No Asbestos Detected

IN-6-2 215 Window glazing S. window No Asbestos Detected

IN-6-2 216 Ext. window caulk N. side of building 6% Chrysotile Asbestos

IN-6-2 217 Tar roofing over garage door S. side of building No Asbestos Detected

IN-4-1 218 Ext. window caulk E. side of building 6% Chrysotile Asbestos

IN-4-1 219 Window glazing S. side of building No Asbestos Detected

IN-4-1 220 Window glazing W. side of building No Asbestos Detected

IN-3-2 221 Window glazing E. side of building No Asbestos Detected

IN-3-2 222 Ext. window caulk N. side of building 6% Chrysotile Asbestos

IN-3-2 223 Tar roofing over garage door N. side of building No Asbestos Detected

IN-3-3 224 Window glazing E. side of building No Asbestos Detected

IN-3-3 225 Ext. window caulk N. side of building 6% Chrysotile Asbestos

IN-5-1 226 Tar roofing over garage door S. side of building No Asbestos Detected

IN-5-1 227 Tar spacers for Galbestos W. side of building No Asbestos Detected

IN-5-1 228 Window glazing E. side of building No Asbestos Detected

IN-5-1 229 Window glazing N. side of building No Asbestos Detected

IN-4-6 230 Window glazing N. side of building No Asbestos Detected

IN-4-6 231 Window glazing E. side of building No Asbestos Detected

IN-1-1 232 Window glazing N. side of building No Asbestos Detected

IN-1-1 233 Window glazing S. side of building No Asbestos Detected

IN-1-2 234 Window glazing E. side of building No Asbestos Detected

IN-1-2 235 Window glazing N. side of building No Asbestos Detected

ASBESTOS CONTAINING MATERIAL PHOTOS

PHOTOGRAPHS OF ASBESTOS MATERIALS

Photo A-1 Window glazing

Photo A-2

Wiring inside original metal conduit w/white paint

Photo A-3

Gaskets in 4’ fluorescent light fixture glass enclosures

Photo A-4 Transite cement siding

Photo A-5 under metal siding

Photo A-6

Photo A-7 12” tan floor tile (negative mastic)

Photo A-8

Photo A-9 Window frame caulk and glazing

Photo A-10

Photo A-11

Photo A-12 Gaskets on metal blast doors

Photo A-13

Photo A-14

Photo A-15

Photo A-16 9” tan floor tile (negative

Photo A-17 12” white floor tile and black mastic

Photo A-18

Photo A-19

Photo A-20

Photo A-21

Photo A-22

Photo A-23 Exterior door frame caulk

D-1-10B VACANT MIX HOUSSE

Photo A-24 Exterior door frame caulk

Photo A-25 Transite cement interior wall panels

Photo A-26

Transite cement interior ceiling panels

Photo A-27

Photo A-28

Photo A-29

Photo A-30 Gaskets in round incandescent light fixtures with glass enclosures

Photo A-31

Photo A-32

Photo A-33 Galbestos corrugated metal siding

Photo A-34 metal siding and roofing

Photo A-35 Window frame caulk

Photo A-36 Transite cement energy panels on walls and ceiling (2 layers of transite with interior insul.)

Photo A-37 Mag block pipe insulation

Photo A-38 Transite roofing shingles

Photo A-39 12” tan floor tile (negative

Photo A-40 12” white floor tile (negative mastic)

Photo A-41 panels (2 layers of transite with interior insul.)

Photo A-42 panels (2 layers of transite with interior insul.)

Photo A-43

Tar roof seam crack sealant on 2nd floor porch/roof

AREA 7 WAREHOUSE BUILDINGS

Photo A-44

Photo A-45

Photo A-46

Photo A-47

Photo A-48

Photo A-49

Photo A-50

Photo A-51

Photo A-52

Photo A-53

Photo A-54

Photo A-55

Photo A-56 Galbestos paper debris on ground

Photo A-57

Photo A-58

Photo A-59

Photo A-60

Photo A-61

Photo A-62

Photo A-63

Photo A-64

Photo A-65 Exterior window frame caulking

Photo A-66

Photo A-67

APPENDIX A

ASBESTOS SAMPLE LOCATION DRAWINGS

APPENDIX B

LEAD PAINT XRF TESTING DATA

LEAD INSPECTION

REPORT

FACILITY:

US Fish & Wildlife Service

Crab Orchard National Wildlife Refuge Marion, IL

D-Area Demolition, Lead-Based Paint Inspection

FOR:

Project Manager: Brett Brumbaugh Castle Hill Associates 1197 Farnsworth Road Unit E Waterville, OH 43566

PROJECT NUMBER: 2201-029

DATE OF SERVICE: February 15, 2022

February 28, 2022

Brett Brumbaugh Environmental & Regulatory Affairs Manager Castle Hill Associates 1197 Farnsworth Road Unit E Waterville, OH 43566

Re: US Fish & Wildlife Service Crab Orchard National Wildlife Refuge - Marion, IL D-Area Demolition, Lead Based Paint Inspection

Dear Mr. Brumbaugh:

On February 15, 2022, Farmer Environmental Services, LLC, performed a survey for painted surfaces with suspect lead-based paint on various structures scheduled for demolition in the D-Area of Crab Orchard National Wildlife Refuge outside of Marion, IL.

The scope of sampling included sufficient testing to provide information for the demolition of the structures. The structures have been vacant for a number of years and are in various states of disrepair. Evidence of floral and faunal habitation and environmental exposure was observed. Some structures were not able to be identified by identification number and were grouped into a larger group of structures. Other structures were in such disrepair it wasn’t safe to fully or even partially inspect those structures. Fifteen structures and one grouping of structures were inspected.

A Niton XLp Analyzer (X-Ray Fluorescence) was used for testing purposes. The Farmer Environmental field rep was trained in the use of the Niton Analyzer. XRF testing is a non-destructive testing method. The analyzer provides a positive or negative reading (as well as a concentration). The criterion for lead-based paint when using an XRF Analyzer is one milligram per square centimeter (1.0 mg/cm2). A total of 126 painted surfaces were tested. The scope of testing included walls, ceilings, door components, and miscellaneous other interior and exterior painted surfaces.

Testing found the following surfaces to be above the criterion of 1.0 mg/cm2:

D-1-10 Mixhouse – Exterior Door Trim (wood) Deteriorated Condition Bridge between D-1-10 & D-1-11 – Railing (metal) Deteriorated Condition D-1-9 – Hallway Ceiling (wood) by North Bay Deteriorated Condition D-1-9 – Hallway Ceiling (wood) by South Bay Deteriorated Condition D-1-8 – Exterior Door Slab (wood), South Side Deteriorated Condition D-1-8 – Exterior Soffit (wood), South Side Deteriorated Condition

In addition to the lead-based paint identified on the previous page, testing results did show concentrations of lead at less than 1.0 mg/cm2. Painted surfaces with concentrations under the criterion referenced above are deemed lead containing paint.

Lead can still be present in paint which is not classified as “lead based”. This would occur when the paint has a lower amount of lead than the EPA regulates. If lead is present in the paint, lead dust can be released when the paint deteriorates, or is disturbed during remodeling, renovation, sanding, or some maintenance work that breaks the surfaces of the paint, as well as demolition activities. Activities that impact lead containing paint should be performed in accordance with the OSHA lead standard for the construction industry.

A table listing the XRF test locations (per building) can be found on the pages following this summary. If there are any questions, or additional information is needed, please contact us at 618-656-6988.

Respectfully Submitted, Mike Burke (prepared by) Farmer Environmental Services, LLC

XRF – Lead Based Paint Inspection Key:

Column 1: The room, room number, or best description possible for the test shot

Column 2: Direction for surfaces such as walls, etc.

Column 3: The description of the surface (Wall, Door, Door Frame, etc.)

Column 4: The substrate of the surface W = Wood M = Metal P = Plaster, CB = Concrete Block, C = Concrete, D = Drywall, etc.

Column 5: The condition of the surface: I = Intact or D = Deteriorated

Column 6: The XRF Reading

Any reading 1.0 or greater is considered to be Lead-Based Paint (LBP)

Column 7: Pos = Positive for LBP. The row will also be highlighted in yellow Neg = Negative for LBP

Column 8: Any additional notes found during testing

Project: Crab Orchard NWR - USDA

Address: Marion, IL

Technician: Brett Brumbaugh

Date: 2/16/2022

XRF Mfg.: Viken Detection

Model: Pb200i

Type: XRF Lead Paint Analyzer

Serial # 2757

Reading # Building Building Area/Room Component Substrate Paint Color Pb Conc.

mg/cm2 Result

1 I-1-25 Exterior Wall Concrete White 0.1 Negative

2 I-1-25 Exterior Window frame Metal White 0.1 Negative

3 I-1-25 Interior 1st floor Door Metal Blue -0.1 Negative

4 I-1-25 Interior 1st floor Wall Drywall Blue -0.1 Negative

5 I-1-25 Interior 1st floor Wall Block White -0.2 Negative

6 I-1-25 Interior 1st floor Door Wood Blue 1.0 Positive

7 I-1-25 Interior 1st floor Pipe Metal White 0.2 Negative

8 I-1-25 Interior 1st floor Door frame Wood Blue -0.1 Negative

9 I-1-25 Interior 1st floor Door Wood Blue 0.0 Negative

10 I-1-25 Interior 2nd floor Door frame Metal Blue 0.5 Negative

11 I-1-25 Interior 2nd floor Door Wood Blue 0.0 Negative

12 I-1-25 Interior 2nd floor Wall Block White 0.0 Negative

13 I-1-25 Interior 2nd floor Water heater Metal Blue 0.3 Negative

14 I-1-25 Interior 2nd floor Porch Wood White -0.1 Negative

15 IN-6-2 Exterior Bay door trim Wood Brown -0.4 Negative

16 IN-6-2 Exterior Siding Metal Beige 0.4 Negative

17 IN-6-2 Interior Floor striping Concrete Yellow 0.0 Negative

18 IN-6-2 Interior Floor striping Concrete Yellow 0.5 Negative

19 IN-6-2 Interior Siding Metal Black 0.3 Negative

20 IN-6-2 Interior Door trim Wood Beige -0.3 Negative

21 IN-6-2 Exterior Siding Metal Brown 0.3 Negative

22 IN-6-2 Exterior Overhead garage door Wood Beige -0.2 Negative

23 IN-4-1 Exterior Siding Metal Beige -0.2 Negative

24 IN-4-1 Exterior Trim Wood Brown -0.3 Negative

25 IN-4-1 Interior Floor striping Concrete Yellow 2.1 Positive

26 IN-4-1 Interior Column Metal White -0.1 Negative

27 IN-4-1 Interior Column Metal White -0.3 Negative

28 IN-4-1 Interior Siding Metal Black -0.2 Negative

29 IN-4-1 Interior Floor striping Concrete Yellow 0.5 Negative

30 IN-4-1 Interior Overhead garage door Wood Gray 3.9 Positive

31 IN-4-1 Interior Overhead garage door Wood Beige 3.1 Positive

32 IN-4-1 Interior Overhead garage door Wood White 14.7 Positive

33 IN-3-2 Exterior Overhead garage door Wood White 0.0 Negative

34 IN-3-2 Exterior Siding Metal Beige -0.1 Negative

35 IN-3-2 Exterior Door trim Wood Brown -0.3 Negative

36 IN-3-2 Interior Overhead garage door Wood Gray 2.6 Positive

37 IN-3-2 Interior Floor striping Concrete Yellow 0.4 Negative

38 IN-3-2 Exterior Overhead garage door Wood White -0.3 Negative

39 IN-3-2 Exterior Overhead garage door Wood Beige 3.2 Positive

40 IN-3-3 Exterior Overhead garage door Wood Beige 1.9 Positive

41 IN-3-3 Exterior Siding Metal Black -0.2 Negative

42 IN-3-3 Exterior Column Metal White 0.0 Negative

43 IN-3-3 Exterior Overhead garage door Wood Gray -0.3 Negative

44 IN-3-3 Exterior Door trim Wood White 0.5 Negative

45 IN-3-3 Interior Floor striping Concrete Yellow 3.6 Positive

46 IN-3-3 Interior Overhead garage door Wood White 3.3 Positive

47 IN-3-3 Interior Overhead garage door Wood Gray 1.3 Positive

48 IN-3-3 Interior Window frame Metal White 0.0 Negative

49 QUONSET Interior Door trim Wood Brown 0.6 Negative

Technician: Brett Brumbaugh

Date: 2/16/2022

XRF Mfg.: Viken Detection

Model: Pb200i

Type: XRF Lead Paint Analyzer

Serial # 2757

Reading # Building Building Area/Room Component Substrate Paint Color Pb Conc.

mg/cm2 Result

50 QUONSET Exterior Door Wood Brown 0.2 Negative

51 QUONSET Exterior Awning Metal Gray 0.0 Negative

52 IN-2-1 Exterior Siding Metal Tan -0.1 Negative

53 IN-2-1 Exterior Overhead garage door Wood Gray 1.0 Positive

54 IN-2-1 Exterior Window frame Metal Gray -0.3 Negative

55 IN-2-1 Interior Siding Metal Black 0.1 Negative

56 IN-1-1 Exterior Siding Metal Tan 0.0 Negative

57 IN-1-1 Exterior Window frame Metal White -0.1 Negative

58 IN-1-1 Interior Siding Metal Black 0.3 Negative

59 IN-1-2 Exterior Overhead garage door Wood Gray 4.0 Positive

60 IN-1-2 Interior Floor striping Concrete Yellow -0.2 Negative

61 IN-1-2 Interior Column Metal White 0.6 Negative

62 IN-1-2 Interior Window frame Metal White 0.1 Negative

63 IN-5-1 Exterior Window frame Metal White -0.1 Negative

64 IN-5-1 Exterior Siding Metal Tan 0.3 Negative

65 IN-5-1 Exterior Overhead garage door Wood Gray 5.8 Positive

66 IN-5-1 Exterior Window frame Metal White 0.5 Negative

67 IN-5-1 Interior Overhead garage door Wood Tan 9.0 Positive

68 IN-6-1 Exterior Door trim Wood Tan 0.2 Negative

69 IN-6-1 Exterior Siding Metal Tan 0.2 Negative

70 IN-6-1 Exterior Door trim Wood White -0.4 Negative

71 IN-6-1 Exterior Overhead garage door Wood Gray -0.6 Negative

72 IN-6-1 Exterior Siding Metal Tan -0.2 Negative

73 IN-6-1 Interior Overhead garage door Wood Beige 1.2 Positive

74 S-1-2 Exterior Overhead garage door Wood Gray 1.5 Positive

75 S-1-2 Interior Siding Metal Black -0.1 Negative

76 S-1-2 Interior Floor striping Concrete Yellow 2.9 Positive

77 S-1-2 Interior Column Metal White 0.4 Negative

78 VIS. CTR Exterior Siding Wood Brown 0.0 Negative

79 VIS. CTR Exterior Window frame Wood Brown -0.1 Negative

80 VIS. CTR Interior Wall Drywall White 0.0 Negative

81 VIS. CTR Interior Door Metal Tan -0.2 Negative

82 VIS. CTR Interior Door frame Wood Tan -0.2 Negative

83 VIS. CTR Interior Ceiling Drywall White 0.1 Negative

84 IN-4-6 Exterior Door trim Wood Brown 3.0 Positive

85 IN-4-6 Interior Overhead garage door Wood Gray 3.0 Positive

86 IN-4-6 Exterior Siding Metal Beige -0.1 Negative

87 IN-4-6 Exterior Door trim Wood Brown 5.1 Positive

88 IN-4-6 Exterior Siding Metal Beige 0.0 Negative

89 IN-4-6 Interior Overhead garage door Wood Gray 2.9 Positive

90 IN-1-1 Interior Column Wood Brown -0.2 Negative

91 IN-1-1 Interior Wall Metal Brown -0.2 Negative

92 IN-1-1 Interior Overhead garage door Wood Brown 8.1 Positive

93 IN-1-1 Interior Floor striping Concrete Yellow 6.3 Positive

94 IN-1-1 Interior Overhead garage door Wood Gray 2.2 Positive

95 IN-1-1 Interior Overhead garage door Wood Gray 4.2 Positive

96 IN-1-2 Interior Floor striping Concrete Yellow 4.0 Positive

97 IN-1-2 Interior Wall Metal Black 0.5 Negative

98 IN-1-2 Interior Floor striping Concrete Yellow 4.2 Positive

Technician: Brett Brumbaugh

Date: 2/16/2022

XRF Mfg.: Viken Detection

Model: Pb200i

Type: XRF Lead Paint Analyzer

Serial # 2757

Reading # Building Building Area/Room Component Substrate Paint Color Pb Conc.

mg/cm2 Result

99 IN-1-2 Interior Wall Metal Black -0.2 Negative

100 IN-1-2 Interior Column Metal White -0.1 Negative

101 IN-1-2 Interior Window frame Metal White -0.1 Negative

102 IN-1-2 Exterior Siding Metal Tan 0.1 Negative

103 n/a Calibration Test Block Block N/A 1.0 Positive

104 n/a Calibration Test Block Block N/A 0.9 Positive

105 n/a Calibration Test Block Block N/A 1.0 Positive

106 n/a Calibration Test Block Block N/A 0.0 Negative

107 n/a Calibration Test Block Block N/A 0.1 Negative

108 n/a Calibration Test Block Block N/A 0.1 Negative

APPENDIX C

ASBESTOS LABORATORY REPORT

Approved by:

Approved Signatory Balu Krishnan

Report for:

Mr. Brett Brumbaugh, REPA Castle Hill Associates PO Box 283 Waterville, OH 43566

Regarding: Project: CRAB ORCHARD NWR - MARION, IL; ACM NESHAP SURVEYS

EML ID: 2855469

All samples were received in acceptable condition unless noted in the Report Comments portion in the body of the report. The results relate only to the samples as received and tested. The results include an inherent uncertainty of measurement associated with estimating percentages by polarized light microscopy. Measurement uncertainty data for sample results with >1% asbestos concentration can be provided when requested.

Eurofins EMLab P&K ("the Company") shall have no liability to the client or the client's customer with respect to decisions or recommendations made, actions taken or courses of conduct implemented by either the client or the client's customer as a result of or based upon the Test Results. In no event shall the Company be liable to the client with respect to the Test Results except for the Company's own willful misconduct or gross negligence nor shall the Company be liable for incidental or consequential damages or lost profits or revenues to the fullest extent such liability may be disclaimed by law, even if the Company has been advised of the possibility of such damages, lost profits or lost revenues. In no event shall the Company's liability with respect to the Test Results exceed the amount paid to the Company by the client therefor.

Dates of Analysis:

Asbestos PLM: 02-22-2022

Service SOPs: Asbestos PLM (EPA 40CFR App E to Sub E of Part 763 & EPA METHOD 600/R-93-116, SOP EM-AS-S-1267) NVLAP Lab Code 200844-0

EMLab ID:…