B08_Attachment_5_-_Hercules_Asbestos_and_Lead_Sample_Plan___Results__2020b.pdf

ATTACHMENT 5

Hercules Asbestos and Lead Sample Plan & Results, 2020

ASBESTOS TEM LABORATORIES, INC.

Lead Paint Analysis Report

Page 1 of

3431 Ettie St.

Oakland, CA 94608

Laboratory Job #

ATEM SOP-AA-01

(EPA 3050B/EPA 7420)

(510) 704-8930

FAX (510) 704-8429

371198

Attachment 5

Page 3 of 14 Hercules Asbestos and Lead Sample Plan & Results, 2020

ASBESTOS TEM LABORATORIES, INC California DPH

ELAP ID #1866

3431 Ettie St. Oakland, CA 94608

Page 2 of

(510) 704-8930 (510) 704-8429 www.asbestostemlabs.com With Offices in Reno (775) 359-3377

Michael Gorman Maritime Technical Service 560 West Cutting Blvd Richmond, CA 94804

LABORATORY JOB # 371198

National Parks Service - M/V Hercules 13Atomic Absorption Spectroscopy analytical results for paint sample(s).

Job Site:

Job No.:

RE:

Enclosed please find results for the atomic absorption spectroscopy (AA) metals analysis of one or more paint samples. Sample preparation and analysis procedures were performed according to ATEM SOP-AA-01

(EPA 3050B / EPA 7420).

Prior to analysis, samples are checked for damage and disruption of the chain-of-custody seal. Samples are then logged-in, each given a unique laboratory number, and a hard copy containing all pertinent information is generated. This, and all other relevant paper work are kept with each sample throughout the analytical procedures to assure proper analysis.

A portion of each sample is weighed out such that an aliquot of ~0.2 grams is obtained. The weighed sample material is then placed into a digestion vessel, transferred to a fume hood, heated at ~95 Deg. C, refluxed with nitric acid to solubilize the contained metals, and treated with hydrogen peroxide to oxidize any organic binder present in the sample material. High purity water is added to make a 50 ml volume for each sample.

AA analysis is performed on a microprocessor controlled Perkin Elmer AAnalyst 300 atomic absorption spectrophotometer, operating in the flame mode. Samples are diluted as needed to allow reading of concentrations in the calibration range. QC analyses are prepared and performed along with each sample batch to ensure accurate analytical determinations. Data is compiled into a standard report format and subjected to a thorough quality assurance check before the information is released to the client.

Sincerely Yours, Laboratory Manager

ASBESTOS TEM LABORATORIES, INC.

Note: Results for routine quality control samples run in parallel to the samples reported here were within acceptable limits.

Additional Note: Wherever possible, Asbestos TEM Laboratories highly recommends the submission of field blanks with each sample set. It is recommended to analyze field blanks collected in parallel to all samples collected in the field as a check against media contamination from the manufacturer or in the field. Sample results are not corrected for contamination based on the field blank(s) or other analytical blank(s).

Disclaimer - These results relate only to the samples tested as received and must not be reproduced, except in full, with the approval of the laboratory. Incorrect or illegible information supplied by the customer may adversely affect the validity of test results. This report must not be used to claim product endorsement by AIHA or any other agency of the U.S. Government.

Nov/04/2020

Attachment 5

Page 4 of 14 Hercules Asbestos and Lead Sample Plan & Results, 2020 http://www.asbestostemlabs.com

Jie ZhangJo Ann Huerto

Analytical results posted above relate only to the material(s) tested. µg - micrograms 1% = 10,000 ppm 1ppm = 1 mg/Kg The sample has not been blank corrected.

LEAD PAINT ANALYSIS REPORT

Contact:

Address: Job Site / No.

Analyst

Samples Submitted:

Samples Analyzed:

LOCATION / DESCRIPTION

ASBESTOS TEM LABORATORIES, INC. 3431 Ettie St., Oakland, CA 94608 (510) 704-8930 www.asbestostemlabs.com With Offices in Reno (775) 359-3377

Lab ID #

Lab ID #

Lab ID #

Lab ID #

Lab ID #

Lab ID #

Lab ID #

Lab ID #

Lab ID #

Lab ID #

Lab QC Reviewer

ATOMIC ABSORPTION SPECTROSCOPY

Page: of

METALSAMPLE ID

National Parks Service - M/V Hercules

Oct-30-20

Michael Gorman

Nov-04-20

SAMPLE

RESULT

REPORTING

LIMIT

Sampling Date Analysis Date Analyzed Weight (g)

Sampling Date Analysis Date Analyzed Weight (g)

Sampling Date Analysis Date Analyzed Weight (g)

Sampling Date Analysis Date Analyzed Weight (g)

Sampling Date Analysis Date Analyzed Weight (g)

Sampling Date Analysis Date Analyzed Weight (g)

Sampling Date Analysis Date Analyzed Weight (g)

Sampling Date Analysis Date Analyzed Weight (g)

Sampling Date Analysis Date Analyzed Weight (g)

Sampling Date Analysis Date Analyzed Weight (g)

Report No.:

Date Submitted:

Date Reported:

371198

96-07048-001

Paint Chips 95000 46

Oct-23-20 Nov-04-20 0.2193 mg/kg mg/kg

9.500 % 0.005 %

Pb

96-07048-002

Paint Chips 14000 38

Oct-23-20 Nov-04-20 0.2609 mg/kg mg/kg

1.400 % 0.004 %

Pb

96-07048-003

Paint Chips 210000 45

Oct-23-20 Nov-04-20 0.2242 mg/kg mg/kg

21.000 % 0.005 %

Pb

96-07048-004

Paint Chips 200000 41

Oct-23-20 Nov-04-20 0.2434 mg/kg mg/kg

20.000 % 0.004 %

Pb

96-07048-005

Paint Chips 4100 42

Oct-23-20 Nov-04-20 0.2392 mg/kg mg/kg

0.410 % 0.004 %

Pb

96-07048-006

Paint Chips 180000 45

Oct-23-20 Nov-04-20 0.2223 mg/kg mg/kg

18.000 % 0.005 %

Pb

96-07048-007

Paint Chips 270 43

Oct-23-20 Nov-04-20 0.2344 mg/kg mg/kg

0.027 % 0.004 %

Pb

96-07048-008

Paint Chips 2700 46

Oct-23-20 Nov-04-20 0.2168 mg/kg mg/kg

0.270 % 0.005 %

Pb

96-07048-009

Paint Chips 290000 37

Oct-23-20 Nov-04-20 0.2679 mg/kg mg/kg

29.000 % 0.004 %

Pb

96-07048-010

Paint Chips 220000 41

Oct-23-20 Nov-04-20 0.2463 mg/kg mg/kg

22.000 % 0.004 %

Pb

560 West Cutting Blvd

Richmond, CA 94804

Maritime Technical Service

ATEM SOP-AA-01 (EPA 3050B / EPA 7000B) 3 4

Attachment 5

Page 5 of 14 Hercules Asbestos and Lead Sample Plan & Results, 2020

Jie ZhangJo Ann Huerto

Analytical results posted above relate only to the material(s) tested. µg - micrograms 1% = 10,000 ppm 1ppm = 1 mg/Kg The sample has not been blank corrected.

LEAD PAINT ANALYSIS REPORT

Contact:

Address: Job Site / No.

Analyst

Samples Submitted:

Samples Analyzed:

LOCATION / DESCRIPTION

ASBESTOS TEM LABORATORIES, INC. 3431 Ettie St., Oakland, CA 94608 (510) 704-8930 www.asbestostemlabs.com With Offices in Reno (775) 359-3377

Lab ID #

Lab ID #

Lab ID #

Lab ID #

Lab ID #

Lab ID #

Lab ID #

Lab ID #

Lab ID #

Lab ID #

Lab QC Reviewer

ATOMIC ABSORPTION SPECTROSCOPY

Page: of

METALSAMPLE ID

National Parks Service - M/V Hercules

Oct-30-20

Michael Gorman

Nov-04-20

SAMPLE

RESULT

REPORTING

LIMIT

Sampling Date Analysis Date Analyzed Weight (g)

Sampling Date Analysis Date Analyzed Weight (g)

Sampling Date Analysis Date Analyzed Weight (g)

Sampling Date Analysis Date Analyzed Weight (g)

Sampling Date Analysis Date Analyzed Weight (g)

Sampling Date Analysis Date Analyzed Weight (g)

Sampling Date Analysis Date Analyzed Weight (g)

Sampling Date Analysis Date Analyzed Weight (g)

Sampling Date Analysis Date Analyzed Weight (g)

Sampling Date Analysis Date Analyzed Weight (g)

Report No.:

Date Submitted:

Date Reported:

371198

96-07048-011

Paint Chips 400000 47

Oct-23-20 Nov-04-20 0.2134 mg/kg mg/kg

40.000 % 0.005 %

Pb

96-07048-012

Paint Chips 310000 50

Oct-23-20 Nov-04-20 0.2015 mg/kg mg/kg

31.000 % 0.005 %

Pb

96-07048-013

Paint Chips 220000 40

Oct-23-20 Nov-04-20 0.2525 mg/kg mg/kg

22.000 % 0.004 %

Pb

560 West Cutting Blvd

Richmond, CA 94804

Maritime Technical Service

ATEM SOP-AA-01 (EPA 3050B / EPA 7000B) 4 4

Attachment 5

Page 6 of 14 Hercules Asbestos and Lead Sample Plan & Results, 2020

Page 7 of 14 Hercules Asbestos and Lead Sample Plan & Results, 2020

Page 8 of 14 Hercules Asbestos and Lead Sample Plan & Results, 2020

ASBESTOS TEM LABORATORIES, INC.

Analytical Report

EPA Interim Method Polarized Light Microscopy

Laboratory Job #

3431 Ettie St.

Oakland, CA 94608

(510) 704-8930

FAX (510) 704-8429

1350 FREEPORT BLVD. UNIT 104, SPARKS, NV 89431

Ph. (775) 359-3377

With Branch Offices Located At:

www.asbestostemlabs.com

371199

Attachment 5

Page 9 of 14 Hercules Asbestos and Lead Sample Plan & Results, 2020

ASBESTOS TEM LABORATORIES, INC

Enclosed please find the bulk material analytical results for one or more samples submitted for asbestos analysis.

The analyses were performed in accordance with EPA Method 600/R-93/116 or 600/M4-82-020 for the determination of asbestos in bulk building materials by polarized light microscopy (PLM). Please note that while PLM analysis is commonly performed on non-friable and fine grained materials such as floor tiles and dust, the EPA method recognizes that PLM is subject to limitations. In these situations, accurate results may only be obtainable through the use of more sophisticated and accurate techniques such as transmission electron microscopy (TEM) or X-ray diffraction (XRD).

Prior to analysis, samples are logged-in and all data pertinent to the sample recorded. The samples are checked for damage or disruption of any chain-of-custody seals. A unique laboratory ID number is assigned to each sample.

A hard copy log-in sheet containing all pertinent information concerning the sample is generated. This and all other relevant paper work are kept with the sample throughout the analytical procedures to assure proper analysis.

Each sample is opened in a class 100 HEPA negative air hood. A representative sampling of the material is selected and placed onto a glass microscope slide containing a drop of refractive index oil. The glass slide is placed under a polarizing light microscope where standard mineralogical techniques are used to analyze and quantify the various materials present, including asbestos. The data is then compiled into a standard report format and reviewed by the authorized signatory before being released to the client.

Sincerely Yours, Lab Manager

ASBESTOS TEM LABORATORIES, INC.

Michael Gorman

LABORATORY JOB # 371199

National Parks Servie - M/V Hercules 16Polarized light microscopy analytical results for bulk sample(s).

Job Site:

Job No.:

RE:

Nov-04-20

Maritime Technical Service 560 West Cutting Blvd Richmond, CA 94804

CA DPH ELAP

Lab No. 1866

NVLAP Lab Code: 101891-0 Oakland, CA

. .. 3431 Ettie St. Oakland, CA 94608 (510) 704-8930 FAX (510) 704-8429 With Offices in Reno, NV (775) 359-3377www.asbestostemlabs.com

Disclaimer - These results relate only to the samples tested as received and must not be reproduced, except in full, with the approval of the laboratory. Incorrect or illegible information supplied by the customer may adversely affect the validity of test results. This report must not be used to claim product endorsement by NVLAP or any other agency of the U.S. Government.

Note: Test samples will be stored for three months after data of receipt, after which they will be properly disposed unless client makes other arrangements with the laboratory.

Attachment 5

Page 10 of 14 Hercules Asbestos and Lead Sample Plan & Results, 2020

ANALYTICAL REPORT

Contact:

Address:

Job Site / No.

% TYPE

Analyst

POLARIZED LIGHT MICROSCOPY

Samples Indicated:

Reg. Samples Analyzed:

ASBESTOS

OTHER DATA

SAMPLE ID FIELD

LAB

Lab ID #

Lab ID #

Lab ID #

Lab ID #

Lab ID #

Lab ID #

Lab ID #

Lab ID #

Lab ID #

Lab ID #

Date Submitted:

Date Reported:

National Parks Servie - M/V Hercules

Oct-30-20 Nov-04-20

Michael Gorman Report No.

96-07049-001

01 None Detected None Detected 99-100% Opq, Paint

Paint Chips

Paint Chips-Off-White/BrownOct-23-20 0930 Nov-02-20

96-07049-002

02 None Detected None Detected 99-100% Opq, Paint

Paint Chips

Paint Chips-Off-White/BrownOct-23-20 0930 Nov-02-20

96-07049-003

03 None Detected None Detected 99-100% Qtz, Opq, Calc

Cement/Plaster

Cement/Plaster-GreyOct-23-20 0930 Nov-02-20

96-07049-004

04 None Detected None Detected 99-100% Opq, Paint

Paint Chips

Paint Chips-Off-White/BrownOct-23-20 0930 Nov-02-20

96-07049-005

05 None Detected None Detected 99-100% Opq, Paint

Paint Chips

Paint Chips-Off-White/BrownOct-23-20 0930 Nov-02-20

96-07049-006

06 None Detected None Detected 99-100% Opq, Paint

Paint Chips

Paint Chips-Off-White/BrownOct-23-20 0930 Nov-02-20

96-07049-007

07 None Detected None Detected 99-100% Opq, Paint

Paint Chips

Paint Chips-Off-White/BrownOct-23-20 0930 Nov-02-20

96-07049-008

08 None Detected None Detected 99-100% Opq, Paint

Paint Chips

Paint Chips-Off-White/BrownOct-23-20 0930 Nov-02-20

96-07049-009

09 None Detected None Detected 99-100% Opq, Paint

Paint Chips

Paint Chips-Off-White/BrownOct-23-20 0930 Nov-02-20

96-07049-010

10 None Detected None Detected 99-100% Opq, Paint

Paint Chips

Paint Chips-Off-White/BrownOct-23-20 0930 Nov-02-20

Detection Limit of Method is Estimated to be 1% Asbestos Using a Visual Area Estimation Technique

560 West Cutting Blvd Richmond, CA 94804

DESCRIPTION

1 ofPage:

ASBESTOS TEM LABORATORIES, INC. 3431 Ettie St., Oakland, CA 94608 (510) 704-8930

EPA Method 600/R-93/116 or 600/M4-82-020

Maritime Technical Service Split Layers Analyzed: 0

1) Non-Asbestos Fibers

2) Matrix Materials

3) Date/Time Collected

4) Date Analyzed

1) 2)

3) 4) 1) 2)

3) 4) 1) 2)

3) 4) 1) 2)

3) 4) 1) 2)

3) 4) 1) 2)

3) 4) 1) 2)

3) 4) 1) 2)

3) 4) 1) 2)

3) 4) 1) 2)

3) 4)

With Offices in Reno, NV (775) 359-3377www.asbestostemlabs.com

371199

Attachment 5

Page 11 of 14 Hercules Asbestos and Lead Sample Plan & Results, 2020

ANALYTICAL REPORT

Contact:

Address:

Job Site / No.

% TYPE

Analyst

POLARIZED LIGHT MICROSCOPY

Samples Indicated:

Reg. Samples Analyzed:

ASBESTOS

OTHER DATA

SAMPLE ID FIELD

LAB

Lab ID #

Lab ID #

Lab ID #

Lab ID #

Lab ID #

Lab ID #

Lab ID #

Lab ID #

Lab ID #

Lab ID #

Date Submitted:

Date Reported:

National Parks Servie - M/V Hercules

Oct-30-20 Nov-04-20

Michael Gorman Report No.

96-07049-011

11 None Detected None Detected 99-100% Qtz, Calc, Opq

Cement/Plaster

Cement/Plaster-GreyOct-23-20 0930 Nov-02-20

96-07049-012

12 None Detected None Detected 99-100% Opq, Paint

Paint Chips

Paint Chips-Off-White/BrownOct-23-20 0930 Nov-02-20

96-07049-013

13 None Detected None Detected 99-100% Opq, Paint

Paint Chips

Paint Chips-Off-White/BrownOct-23-20 Nov-02-20

96-07049-014

14 None Detected None Detected 99-100% Opq, Paint

Paint Chips

Paint Chips-Off-White/BrownOct-23-20 Nov-02-20

96-07049-015

15 None Detected None Detected 99-100% Opq, Paint

Paint Chips

Paint Chips-Off-White/BrownOct-23-20 0930 Nov-02-20

96-07049-016

16 None Detected None Detected 99-100% Opq, Qtz, Calc

Cement/Plaster

Cement/Plaster-GreyOct-23-20 0930 Nov-02-20

Detection Limit of Method is Estimated to be 1% Asbestos Using a Visual Area Estimation Technique

560 West Cutting Blvd Richmond, CA 94804

DESCRIPTION

2 ofPage:

ASBESTOS TEM LABORATORIES, INC. 3431 Ettie St., Oakland, CA 94608 (510) 704-8930

EPA Method 600/R-93/116 or 600/M4-82-020

Maritime Technical Service Split Layers Analyzed: 0

1) Non-Asbestos Fibers

2) Matrix Materials

3) Date/Time Collected

4) Date Analyzed

1) 2)

3) 4) 1) 2)

3) 4) 1) 2)

3) 4) 1) 2)

3) 4) 1) 2)

3) 4) 1) 2)

3) 4) 1) 2)

3) 4) 1) 2)

3) 4) 1) 2)

3) 4) 1) 2)

3) 4)

With Offices in Reno, NV (775) 359-3377www.asbestostemlabs.com

371199

Attachment 5

Page 12 of 14 Hercules Asbestos and Lead Sample Plan & Results, 2020

Page 13 of 14 Hercules Asbestos and Lead Sample Plan & Results, 2020

Page 14 of 14 Hercules Asbestos and Lead Sample Plan & Results, 2020

FUEL OIL TANKSENGINE ROOM FUEL OIL TANKS FR

FOC'SLE / CREW BERTHING

SHIP SERVICE SPACE

AFT PEAK

BHD

BHD

BHDBHD

BHD

BHD

51 45 41 36

SWASH SWASH

POTABLE

WATER TK

SWASH

STUFFING

BOX

INT.

BEARING

CHAIN

LKR

CLBOILER

Maritime Technical Services, LLC.

114 Tamal Vista, San Rafael CA. 94901

510-499-2995

WWW.MARITIMETECHSERVICES.COM

A

1 2 3 4 5 6 7 8 9

B

C

D

E

F

A

B

C

D

E

F

11.18.2020AHP

N/A- -

N/ANATIONAL PARK SERVICE

4 5

10 11

HERCULES

SAMPLE PLAN

BOTTOM/BILGE DECK

SAMPLE LOCATIONS

1. Aft Eng Room STBD bulkhead (White paint)

2. Aft Eng Room STBD bilge (Red paint)

3. Aft Eng Room PORT bilge (Cement ballast)

4. Eng Room PORT fwd bulkhead (White paint)

5. Eng Room PORT fwd bulkhead (Red paint)

6. Eng Room STBD Engine Base (Orange paint)

8. Boiler Room (Silver paint)

9. Boiler Room fwd Bulkhead PORT (White paint)

10. Ship Svc Space STBD Bulkhead (Silver paint)

11. Bilge under Feed water Tank (Cement Ballast)

12. Bilge frame under Feed water Tank (Red paint)

13. Collision bulkhead PORT (Silver paint)

Attachment 5

Page 1 of 14 Hercules Asbestos and Lead Sample Plan & Results, 2020

AutoCAD SHX Text Customer

AutoCAD SHX Text Rules

AutoCAD SHX Text Paint

AutoCAD SHX Text Design:

AutoCAD SHX Text Approval:

AutoCAD SHX Text Order no.

AutoCAD SHX Text Drawing no.

AutoCAD SHX Text Page

AutoCAD SHX Text Of

AutoCAD SHX Text USCG, ABS, DNV, etc..

AutoCAD SHX Text Revision:

AutoCAD SHX Text Scale:

AutoCAD SHX Text Description:

AutoCAD SHX Text Date:

AutoCAD SHX Text Date:

FUEL OIL TANKSFUEL OIL TANKS FUEL OIL TANKS FR

BALLAST

FEED WTR

LAZARETTE

BALLAST / FEED WTR

BHD 60

FOC'SLE / CREW BERTHING

SHIP SERVICE SPACE

MAIN ENGINE

MACHINE SHOPAFT PEAK

POTABLE WATER

TANK

CHAIN

LKR

9' DRAFT

WHEELHOUSE

CREW

BERTHING

WINDLASS

ENGINE

CHAIN

LKR

BHD

BHD

BHD BHD

BHD

51 45 41 36

30 25

20 15 10

Maritime Technical Services, LLC.

114 Tamal Vista, San Rafael CA. 94901

510-499-2995

WWW.MARITIMETECHSERVICES.COM

A

1 2 3 4 5 6 7 8 9

B

C

D

E

F

A

B

C

D

E

F

11.18.2020AHP

N/A- -

N/ANATIONAL PARK SERVICE

HERCULES

SAMPLE PLAN

PROFILE

SAMPLE LOCATIONS

7. Workshop overhead (White paint)

14. Crew Berthing overhead (White paint)

15. Crew Berthing STBD bulkhead (White paint)

Attachment 5

Page 2 of 14 Hercules Asbestos and Lead Sample Plan & Results, 2020

AutoCAD SHX Text Customer

AutoCAD SHX Text Rules

AutoCAD SHX Text Paint

AutoCAD SHX Text Design:

AutoCAD SHX Text Approval:

AutoCAD SHX Text Order no.

AutoCAD SHX Text Drawing no.

AutoCAD SHX Text Page

AutoCAD SHX Text Of

AutoCAD SHX Text USCG, ABS, DNV, etc..

AutoCAD SHX Text Revision:

AutoCAD SHX Text Scale:

AutoCAD SHX Text Description:

AutoCAD SHX Text Date:

AutoCAD SHX Text Date: