EQP4035_LSS39 Reporting Limits Test Capabilities and Target Analyte List 062026- DRAFT.pdf

Michigan.gov/EGLELab Page 1 of 23 (Rev. 07/2026)

MICHIGAN DEPARTMENT OF ENVIRONMENT, GREAT LAKES, AND ENERGY

Remediation & Redevelopment Division – Laboratory Services Section

Environmental Lab Reporting Limits, Test Capabilities, and Target

Analyte List

Inorganic Metals Analysis Offerings

Reference Method: EPA 200.8 by ICP-MS

Hold Time: 180 days from collection to analysis Waters

Container: 250mL plastic bottle; 1:1 HNO3 preserved to pH<2 Water Analysis Request Form (EQP4014-01 Rev 05/2024)- Can order each metal as a total metal or a dissolved metal sample*

Analyte Reporting

Limit (ug/L) Aluminium (Al) 5 Antimony (Sb) 1 Arsenic (As) 1 Barium (Ba) 5

Beryllium (Be) 1 Cadmium (Cd) 0.2

Chromium (Cr), Total 1 Cobalt (Co) 5 Copper (Cu) 1

Iron (Fe) 20 Lead (Pb) 1

Analyte Reporting

Limit (ug/L) Manganese (Mn) 5 Molybdenum (Mo) 5

Nickel (Ni) 2 Selenium (Se) 1

Silver (Ag) 0.2 Strontium (Sr) 5 Thallium (Tl) 2 Titanium (Ti) 5 Uranium (U) 1

Vanadium (V) 2 Zinc (Zn) 5

Soils/Sediments

Container: One 8oz glass jar Soil Analysis Request Form (EQP4014-03 Rev 01/2024)

Analyte Reporting Limit

(mg/kg dry) Aluminium (Al) 1 Antimony (Sb) 0.3 Arsenic (As) 0.5 Barium (Ba) 1

Beryllium (Be) 0.2 Cadmium (Cd) 0.2

Chromium (Cr), Total 2 Cobalt (Co) 0.5 Copper (Cu) 1

Lead (Pb) 1

Analyte Reporting Limit

(mg/kg dry) Manganese (Mn) 1 Molybdenum (Mo) 1

Nickel (Ni) 1 Selenium (Se) 0.2

Silver (Ag) 0.1 Strontium (Sr) 1 Thallium (Tl) 0.5 Titanium (Ti) 1 Uranium (U) 0.5

Vanadium (V) 1 Zinc (Zn) 1

Michigan.gov/EGLELab Page 2 of 23 (Rev. 07/2026)

Environmental Lab Reporting Limits, Test Capabilities, and Target

Analyte List

Inorganic Metals Analysis Offerings (Continued)

Reference Method: EQL-0310-189-IML 2009 by ICP-MS

Hold Time: 180 days from collection to analysis

PM10 and HiVol Filters

Container: 5 x 11-1/2" envelope provided by EGLE Air Quality Division Filter analysis requests are provided by EGLE AQD staff as determined by designation on chain of custody forms at time of receipt.

PM10

Reporting

Limit (ug/L)**

HiVol Reporting

Limit (ug/L)**

Arsenic (As) 1 1 Barium (Ba) 10 50

Beryllium (Be) 1 1 Cadmium (Cd) 1 1 Chromium (Cr) 10 10

Cobalt (Co) 1 1 Copper (Cu) 5 10

Analyte

PM10

Reporting

Limit (ug/L)**

HiVol Reporting

Limit (ug/L)**

Iron (Fe) 150 120 Lead (Pb) 2 5

Manganese (Mn) 5 5 Molybdenum (Mo) 2 2

Nickel (Ni) 10 5 Vanadium (V) 1 1

Zinc (Zn) 50 30

**Reporting limits are listed in the initial units of ug/L. Final units are calculated to ng/m3 based upon each sample's individual air volume noted on the chain of custody.

Reference Method: EPA 200.7 by ICP-OES

Hold Time: 180 days from collection to analysis Waters

Container: 250mL plastic bottle; 1:1 HNO3 preserved to pH<2

Reporting Limit

(ug/L) Boron (B) 20

Calcium (Ca) 1000 Lithium (Li) 10

Analyte Reporting Limit

(ug/L) Magnesium (Mg) 500

Potassium (K) 200 Sodium (Na) 1000

Michigan.gov/EGLELab Page 3 of 23 (Rev. 07/2026)

Environmental Lab Reporting Limits, Test Capabilities, and Target

Analyte List

Inorganic Metals Analysis Offerings (Continued)

Reference Method: EPA 200.7 by ICP-OES (Continued)

Hold Time: 180 days from collection to analysis

Soils/Sediments

Soil Analysis Request Form (EQP4014-03 Rev 01/2024)

(mg/kg dry) Calcium (Ca) 50

Iron (Fe) 5 Lithium (Li) 10

Analyte Reporting Limit

(mg/kg dry) Magnesium (Mg) 100

Potassium (K) 100 Sodium (Na) 100

Reference Method: USGS I-1230-85 by Colormetric Detection via Spectrophotometer

Waters

Hold Time: 24 hours from collection to analysis

Container: 125mL plastic bottle; no preservation; field filtered upon collection

Water Analysis Request Form (EQP4014-01 Rev 05/2024)- Diss Cr6+

Analyte Reporting Limit (ug/L) Hexavalent Dissolved Chromium 5

Reference Method: EPA SW-846 7473

Hold Time: 28 days from collection to analysis

Waters

Container: 250mL plastic bottle; 1:1 HNO3 preserved to pH<2

Mercury (Hg) 0.2

Michigan.gov/EGLELab Page 4 of 23 (Rev. 07/2026)

Environmental Lab Reporting Limits, Test Capabilities, and Target

Analyte List

Inorganic Metals Analysis Offerings (Continued)

Reference Method: EPA SW-846 7473 (Continued)

Hold Time: 28 days from collection to analysis

Soils/Sediments

Analyte Reporting Limit (mg/kg)

Mercury (Hg) 0.05

Reference Method: EPA 1631E by CVAFS

Waters

Hold Time: 90 days from collection to analysis

Container: 125mL clear glass with PTFE-lined cap

Water Analysis Request Form (EQP4014-01 Rev 05/2024)- Low Level Mercury

Analyte Reporting Limit (ng/L) Mercury (Hg)- Low Level 0.5

*Dissolved metals samples must be filtered through a 0.45 micron filter in the field at the time of collection or as soon as practical.

Reference Method: EPA 200.8 and EPA SW-846 7473

Metals Packages

Container: Follow same guidelines listed above for waters and soils Choose package selection on either the water or soil analysis request form

Package Name Metals Included

OpMemo2 Sb, As, Ba, Be, Cd, Cr, Cu, Co, Fe, Pb, Mn, Hg, Mo, Ni, Se, Ag, Tl, V, Zn Michigan10 As, Ba, Cd, Cr, Cu, Pb, Hg, Se, Ag, Zn

Michigan.gov/EGLELab Page 5 of 23 (Rev. 07/2026)

Environmental Lab Reporting Limits, Test Capabilities, and Target

Analyte List

Additional Inorganic Analysis Offerings

Waters

Water Analysis Request Form (EQP4014-01 Rev 05/2024)

Limit (mg/L)

Reference Method Container and Preservation

Hold Time

Total Alkalinity 25 EPA 310.2 by Automated

Colorimetric Detection 125mL plastic bottle;

receive on ice days Alkalinity, Bicarbonate/Carbonate

SM2320B by Phenolphthalein Titration

125mL plastic bottle days

Ammonia 0.01 EPA 350.1 by Automated

Colorimetric Detection

250mL plastic bottle;

1:1 H2SO4 preserved to pH<2; receive on ice days

Chloride 4.0 SM4500Cl-E by Automated

Colorimetric Detection 125mL plastic bottle;

receive on ice days

Chlorophyll 0.001 EPA 445.0 by Fluorometric

Detection 250mL amber plastic;

1% MgCO3 preserved hours

Chemical Oxygen Demand (COD)

5.0 EPA 410.4 by Colorimetric

Detection

250mL plastic bottle;

1:1 H2SO4 preserved to pH<2; receive on ice days

Conductance, Specific umhos/cm EPA 120.1 by Automated ECM

Module 125mL plastic bottle;

receive on ice days

Cyanide, Available 0.002 ASTM D6888-16 by Automated

Amperometric Detection

125mL plastic; 10N NaOH preserved to pH<12; receive on ice days

Cyanide, Total 0.005 ASTM D7284-13 by Automated

Amperometric Detection and Manual Micro Distillation

125mL plastic; 10N NaOH preserved to pH<12; receive on ice days

Nitrate 0.010 Calculation (Nitrate+Nitrite minus Nitrite) See parent bottles hours

Nitrate + Nitrite 0.010 Systea Easy (1- Reagent) 250mL plastic bottle;

1:1 H2SO4 preserved to pH<2; receive on ice days

Nitrite 0.010 Systea Easy (1- Reagent) 125mL plastic bottle;

receive on ice hours

Michigan.gov/EGLELab Page 6 of 23 (Rev. 07/2026)

Environmental Lab Reporting Limits, Test Capabilities, and Target

Additional Inorganic Analysis Offerings (Continued)

Waters (Continued)

Limit (mg/L)

Reference Method Container and Preservation

Hold Time

Nitrogen, Kjeldahl 0.20 EPA 351.2 by Automated

Colorimetric Detection

250mL plastic bottle;

1:1 H2SO4 preserved to pH<2; receive on ice 28 days

Ortho-Phosphate and Dissolved Ortho-phosphate*** 0.010

EPA 365.1 by Automated Colorimetric Detection

125mL plastic bottle;

receive on ice hours pH pH units EPA 350.1 by Automated Electrometric Detection

125mL plastic bottle;

receive on ice minutes

Phosphorous, Total 0.010 EPA 365.1 by Automated

Colorimetric Detection

250mL plastic bottle;

1:1 H2SO4 preserved to pH<2; receive on ice 28 days

Suspended Solids

(SS)

SM2540D by Gravimetric

Determination of Non- Filterable Solids

500mL plastic bottle;

receive on ice

7 days

Total Dissolved Solids

(TDS)

SM2540C by Gravimetric

Determination of Total Filterable Solids

500mL plastic bottle;

receive on ice

7 days

Sulfate 5 ASTM D516-16 by Automated

Turbidimetric Detection 125mL plastic bottle;

receive on ice 28 days

Total Organic Carbon (TOC) & Dissolved

Organic Carbon

(DOC)***

0.5 SM5310C by Heated

Persulfate Oxidation and NDIR Determination

40mL glass vial pre-preserved with H3PO4;

receive on ice 28 days

Turbidity 1.0 NTU EPA 180.1 by Nephelometric

Detection via Manual Turbidimeter

500mL plastic bottle;

receive on ice hours

***Dissolved orthophospate samples must be filtered through a 0.45-micron filter in the field immediately after collection. Dissolved organic carbon samples must be filtered through a 0.45-micron filter in the field and then preserved within 48 hours of collection.

Michigan.gov/EGLELab Page 7 of 23 (Rev. 07/2026)

Environmental Lab Reporting Limits, Test Capabilities, and Target

Additional Inorganic Analysis Offerings (Continued)

Soils

Limit (mg/kg dry)

Reference Method Container and Preservation

Hold Time

Cyanide, Available 0.10 ASTM D6888-16 by Automated

Amperometric Detection One 8oz glass jar with

PTFE-lined cap days

Cyanide, Total 0.005 ASTM D7284-13 by Automated

Amperometric Detection and Manual Micro Distillation

One 8oz glass jar with PTFE-lined cap days

Total Solids 0.1% SM2540G by Gravimetric

Determination

One 8oz glass jar with PTFE-lined cap or capped syringe for VOC analysis only

N/A

Semi-Volatile Organics Analysis Offerings

Reference Method: EPA SW-846 8081B by GC-ECD

Hold Time:

o Water: 7 days o Soil: 14 days

Container:

o Water: Two 1000mL amber glass bottles completely filled; receive on ice o Soil: One 8oz glass jar; receive on ice

Analysis Request Forms o Water: EQP4014-01 Rev 05/2024 o Soil: EQP4014-03 Rev 01/2024 o Test Request: Pesticides & PCBs or Pesticides Only or Toxaphene and

Chlordane can be requested separately.

Pesticides in Waters and Soils

Michigan.gov/EGLELab Page 8 of 23 (Rev. 07/2026)

Environmental Lab Reporting Limits, Test Capabilities, and Target

Semi-Volatile Organics Analysis Offerings (Continued)

Pesticides in Waters and Soils (Continued)

Water Reporting

Limit (ug/L)

Soil Reporting

Limit (ug/kg) a-BHC 0.02 10 b-BHC 0.02 20 g-BHC (Lindane) 0.02 20 d-BHC 0.02 20

Heptachlor 0.01 20 Aldrin 0.01 20

Heptachlor epoxide 0.01 20 g-Chlordane 0.01 20 Endosulfan I 0.02 20 a-Chlordane 0.01 20

4,4’-DDE 0.02 20

Dieldrin 0.02 20 Endrin 0.02 20

Analyte

Water Reporting

Limit (ug/L)

Soil Reporting

Limit (ug/kg)

Endosulfan II 0.03 20

4,4’-DDD 0.02 20

2,4’-DDT 0.01 20

Endrin aldehyde 0.02 20 Endosulfan sulfate 0.05 20

4,4’-DDT 0.02 20

Endrin ketone 0.02 20

Hexabromobenzene 0.02 100 Methoxychlor 0.05 50

Mirex 0.02 50

PBB (BP-6) 0.05 250

Technical Chlordane 0.05 30 Toxaphene 0.1 170

Reference Method: EPA 608.3 by GC-ECD

Hold Time: 7 days o Pesticides: 7 days o PCBs: 1 year

Container: Two 1000mL amber glass bottles completely filled; receive on ice Wastewater Analysis Request Form (EQP4014-02 Rev 05/2024) o Test Request: Pesticides & PCBs or Pesticides Only or PCBs only or Toxaphene can be requested separately.

Pesticides and PCBs in Wastewater

Michigan.gov/EGLELab Page 9 of 23 (Rev. 07/2026)

Environmental Lab Reporting Limits, Test Capabilities, and Target

Pesticides and PCBs in Wastewater (Continued)

(ug/L) a-BHC 0.01 b-BHC 0.01 g-BHC (Lindane) 0.01 d-BHC 0.01

Heptachlor 0.01 Aldrin 0.01

Heptachlor epoxide 0.01 g-Chlordane 0.01 Endosulfan I 0.01 a-Chlordane 0.01

4,4’-DDE 0.01

Dieldrin 0.01 Endrin 0.01

4,4’-DDD 0.01

4,4’-DDT 0.01

Hexabromobenzene 0.01 Hexachlorobenzene 0.01

Hexachlorobutadiene 0.01

Analyte Reporting Limit

(ug/L) Hexachlorocyclopentadiene 0.01

Methoxychlor 0.05 Mirex 0.01

PBB (BP-6) 0.05

Pentachlorobenzene 0.01

Pentachloronitrobenzene 0.01 Toxaphene 0.1

1,2,3,4-Tetrachlorobenzene 0.01 1,2,4,5- Tetrachlorobenzene 0.01

Aroclor 1016 0.1 Aroclor 1221 0.1 Aroclor 1232 0.1 Aroclor 1242 0.1 Aroclor 1248 0.1 Aroclor 1254 0.1 Aroclor 1260 0.1 Aroclor 1262 0.1 Aroclor 1268 0.1

Reference Method: EPA SW-846 8082A by GC-ECD

Hold Time:

o Water: 1 year o Soil: 14 days

Container:

o Water: Two 1000mL amber glass bottles completely filled; receive on ice o Soil: One 8oz glass jar; receive on ice

Analysis Request Forms o Water: EQP4014-01 Rev 05/2024 o Soil: EQP4014-03 Rev 01/2024 o Test Request: Pesticides & PCBs or PCBs Only

Michigan.gov/EGLELab Page 10 of 23 (Rev. 07/2026)

Environmental Lab Reporting Limits, Test Capabilities, and Target

PCBs in Waters and Soils

Reporting

Limit (ug/L)

Soil Reporting

Limit (ug/kg)

Aroclor 1016 0.1 100 Aroclor 1221 0.1 100 Aroclor 1232 0.1 100 Aroclor 1242 0.1 100 Aroclor 1248 0.1 100

Analyte

Water Reporting

Limit (ug/L)

Soil Reporting

Limit (ug/kg)

Aroclor 1254 0.1 100 Aroclor 1260 0.1 100 Aroclor 1262 0.1 100 Aroclor 1268 0.1 100

Reference Method: EPA SW-846 8270E by GC-MS

Hold Time:

o Water: 7 days o Soil: 14 days

Container:

o Water: Two 1000mL amber glass bottles completely filled; receive on ice o Soil: One 8oz glass jar; receive on ice

Analysis Request Forms o Water: EQP4014-01 Rev 05/2024 o Test Request: BNAs or BNs only or PNAs only or Acids only ****

Base/Neutral/Acid (BNA) in Waters and Soils

Reporting

Limit (ug/L)

Soil Reporting

Limit (ug/kg)

1,2,4-Trichlorobenzene 2 200 2,4,5-Trichlorophenol 5 330 2,4,6-Trichlorophenol 4 330 2,4-Dichlorophenol 10 330 2,4-Dimethylphenol 5 330 2,4-Dinitrophenol 25 1700

Analyte

Water Reporting

Limit (ug/L)

Soil Reporting

Limit (ug/kg)

2,4-Dinitrotoluene 5 250 2,6-Dinitrotoluene 5 250

2-Chloroaniline 5 N/A 2-Chloronaphthalene 2 200

2-Chlorophenol 10 330 2-Methylnaphthalene 5 250

Michigan.gov/EGLELab Page 11 of 23 (Rev. 07/2026)

Remediation & Redevelopment Division – Laboratory Services Section

Environmental Lab Reporting Limits, Test Capabilities, and Target

Base/Neutral/Acid (BNA) in Waters and Soils (Continued)

RL

(ug/L)

Soil RL (ug/kg)

2-Methyl-4,6-dinitrophenol 20 1700 2-Methylphenol (o-Cresol) 10 330

2-Nitroaniline 20 500 2-Nitrophenol 5 330

3 & 4-Methylphenol 20 660 3-Nitroaniline 20 500

4-Bromophenyl phenyl ether 2 200 4-Chloro-3-methyl-phenol 5 200

4-Chloroaniline 10 N/A 4-Chlorodiphenylether 1 100

4-Nitroaniline 20 500 4-Nitrophenol 25 1700 Acenaphthene 1 100

Acenaphthylene 1 100 Aniline 4 N/A

Anthracene 1 100 Azobenzene 2 200

Benz[a]anthracene 1 100 Benzo[a]pyrene 1 200

Benzo[b]fluoranthene 1 200 Benzo[g,h,i]perylene 1 200 Benzo[k]fluoranthene 1 200

Benzyl Alcohol 50 2500 Bis(2-chloroethoxy)methane 2 200

Bis(2-chloroethyl)ether 1 100 Bis(2-chloroisopropyl)ether 1 100 Bis(2-ethylhexyl)phthalate 5 250

Butyl benzyl phthalate 5 250

Analyte Water

RL

(ug/L)

Soil RL (ug/kg)

Carbazole 5 250 Chrysene 1 100

Dibenz[a,h]anthracene 2 200 Dibenzofuran 4 250

Diethylphthalate 5 250 Dimethyl phthalate 5 250 Di-n-butyl phthalate 5 250 Di-n-octyl phthalate 5 250

Fluoranthene 1 100 Fluorene 1 100

Hexachlorobenzene 1 200 Hexachlorobutadiene 1 100

Hexachlorocyclopentadiene 10 1000 Hexachloroethane 1 100

Indeno(1,2,3-c,d)pyrene 2 200 Isophorone 1 100

N,N-dimethylaniline 5 N/A Naphthalene 1 100 Nitrobenzene 2 200

N-methylaniline 1 N/A N-Nitrosodimethylamine 5 250

N-Nitrosodi-n-propylamine 2 200 N-Nitrosodiphenylamine 2 200

Pentachlorophenol 20 1700 Phenanthrene 1 100

Phenol 5 330 Pyrene 1 100

Tetramethylurea 1 N/A

**** Base Neutrals (BNs only) Polynuclear Aromatics (PNAs only) Phenols (Acids only)

Note: PNAs are a subset of BNs

Michigan.gov/EGLELab Page 12 of 23 (Rev. 07/2026)

Environmental Lab Reporting Limits, Test Capabilities, and Target

Analyte List

Semi-Volatile Organics Analysis Offerings (Continued)

Reference Method: EPA 625 by GC-MS

Hold Time:

o Water: 7 days

Container:

o Water: Two 1000mL amber glass bottles completely filled; receive on ice

Wastewater Analysis Request Form (EQP4014-02 Rev 05/2024) o Test Request: BNAs

Base/Neutral/Acid (BNA) in Wastewater

(ug/L) 1,2,4-Trichlorobenzene 2 2,4,5-Trichlorophenol 10 2,4,6-Trichlorophenol 10 2,4-Dichlorophenol 10 2,4-Dimethylphenol 10 2,4-Dinitrophenol 50 2,4-Dinitrotoluene 5 2,6-Dinitrotoluene 5

2-Chloronaphthalene 2 2-Chlorophenol 10

2-Methyl-4,6-dinitrophenol 50 2-Methylnaphthalene 5

2-Methylphenol (o-Cresol) 10 2-Nitroaniline 20 2-Nitrophenol 10

3 & 4-Methylphenol 20 3-Nitroaniline 20

4-Bromophenyl phenyl ether 2 4-Chloro-3-methyl-phenol 10

4-Chlorodiphenylether 1 4-Nitroaniline 20 4-Nitrophenol 50 Acenaphthene 1

Acenaphthylene 1

Analyte Reporting Limit

(ug/L) Anthracene 1 Azobenzene 2

Benz[a]anthracene 1 Benzo[a]pyrene 2

Benzo[b]fluoranthene 2 Benzo[g,h,i]perylene 2 Benzo[k]fluoranthene 2

Bis(2-chloroethoxy)methane 2 Bis(2-chloroethyl)ether 1

Bis(2-chloroisopropyl)ether 1 Bis(2-ethylhexyl)phthalate 5

Butyl benzyl phthalate 5 Carbazole 10 Chrysene 1

Dibenz[a,h]anthracene 2 Dibenzofuran 5

Diethylphthalate 5 Dimethyl phthalate 5 Di-n-butyl phthalate 5 Di-n-octyl phthalate 5

Fluoranthene 1 Fluorene 1

Hexachlorobenzene 2 Hexachlorobutadiene 2

Michigan.gov/EGLELab Page 13 of 23 (Rev. 07/2026)

Environmental Lab Reporting Limits, Test Capabilities, and Target

Base/Neutral/Acid (BNA) in Wastewater (Continued)

(ug/L) Hexachlorocyclopentadiene 10

Hexachloroethane 1 Indeno(1,2,3-c,d)pyrene 2

Isophorone 1 Naphthalene 1 Nitrobenzene 2

N-Nitrosodimethylamine 5

Analyte Reporting Limit

(ug/L) N-Nitrosodi-n-propylamine 2 N-Nitrosodiphenylamine 2

Pentachlorophenol 50 Phenanthrene 1

Phenol 10 Pyrene 1

Reference Method: EPA SW-846 8015C by GC-FID

Hold Time:

o Water: 7 days o Soil: 14 days

Container:

o Water: Two 1000mL amber glass bottles completely filled; receive on ice o Soil: One 8oz glass jar; receive on ice

Analysis Request Forms o Water: EQP4014-01 Rev 05/2024 o Test Request: DRO / ORO

Diesel Range Organics (DRO) and Oil Range Organics (ORO)

Reporting Limit (ug/L)

Soil Reporting

Limit (ug/kg) Diesel Range Organics (C10-C20) 200 25000

Oil Range Organics (C20-C34) 500 100000

Michigan.gov/EGLELab Page 14 of 23 (Rev. 07/2026)

Environmental Lab Reporting Limits, Test Capabilities, and Target

Analyte List

Semi-Volatile Organics Analysis Offerings (Continued)

Reference Method: EPA SW-846 8327 Revision 0 by Isotope Dilution and LC/MS/MS

Hold Time:

o Water: 14 days o Soil: 28 days

Container:

o Water: Three 15mL plastic vials per sample acceptable fill volume of 4-6mL;

adhere only 1 label per vial; receive on ice o Soil: One 8oz HDPE wide-mouth jar; completely filled; receive on ice

Analysis Request Forms o PFAS for Ground, Surface, and Waste Water: EQP4014-05 Rev 08/2024 o PFAS for Soils: EQP4014-09 Rev 08/2024 o Test Request: PFAS- Method 8327

Per- and Polyfluoroalkyl Substances (PFAS) by EPA Method 8327

RL

(ng/L)

Soil

RL

(ng/kg) Perfluoro-1-butanesulfonic acid

(PFBS)

2 10

Perfluoro-1-pentanesulfonic acid (PFPeS)

2 10

Perfluoro-1-hexanesulfonic acid (PFHxS)

2 10

Perfluoro-1-heptanesulfonic acid (PFHpS)

2 10

Perfluro-1-octanesulfonic acid

(PFOS)

2 10

Perfluoro-1-nonanesulfonic acid

(PFNS)

2 10

Perfluoro-1-decanesulfonic acid

(PFDS)

2 10

1H,1H,2H,2H-perfluorohexanesulfonic acid

(4:2FTS)

2 10

Analyte Water

RL

(ng/L)

Soil

RL

(ng/kg) 1H,1H,2H,2H-perfluorooctanesulfonic acid

(6:2FTS)

2 10

1H,1H,2H,2H-perfluorodecanesulfonic acid

(8:2FTS)

2 10

Perfluoro-n-butanoic acid (PFBA) 4 10 Perfluoro-n-pentanoic acid

(PFPeA) 2 10

Perfluoro-n-hexanoic acid (PFHxA)

2 10

Perfluoro-n-heptanoic acid (PFHpA)

2 10

Perfluoro-n-octanoic acid (PFOA) 2 10 Perfluoro-n-nonanoic acid

(PFNA)

2 10

Michigan.gov/EGLELab Page 15 of 23 (Rev. 07/2026)

Environmental Lab Reporting Limits, Test Capabilities, and Target

Per- and Polyfluoroalkyl Substances (PFAS) by EPA Method 8327 (Continued)

RL

(ng/L)

Soil

RL

(ng/kg) Perfluoro-n-decanoic acid

(PFDA)

2 10

Perfluoro-n-undecanoic acid (PFUnDA)

2 10

Perfluoro-n-dodecanoic acid (PFDoDA)

2 10

Perfluoro-n-tridecanoic acid (PFTrDA)

4 10

Perfluoro-n-tetradecanoic acid (PFTeDA)

4 10

Perfluoro-1-butanesulfonamide

(PFBSA)

2 10

Perfluoro-1-hexanesulfonamide (PFHxSA)

2 10

Perfluoro-1-octanesulfonamide

(PFOSA)

2 10

N-methylperfluoro-1-octanesulfonamidoacetic acid

(NMeFOSAA) 2 10

N-ethylperfluoro-1-octanesulfonamidoacetic acid

(NEtFOSAA) 2 10

Analyte Water

RL

(ng/L)

Soil

RL

(ng/kg) Perfluoro-2-propoxypropanoic acid (HFPO-DA) 4 10

Perfluoro-4-methoxybutanoic acid (ADONA)

2 10

9-Chlorohexadecafluoro-3-oxanone-1-sulfonic acid (9Cl-

PF3ONS)

2 10

11-Chloroeicosafluoro-3-oxaundecane-1-sulfonic acid

(11Cl-PF3OUdS) 2 10

Perfluoro-4-ethylcyclohexanesulfonate

(PFECHS)

2 10

1H,1H,2H,2H,3H,3H-perfluoro-n-hexanoicacid (3:3FTCA)

4 10

1H,1H,2H,2H,3H,3H-perfluoro-n-octanoicacid (5:3FTCA)

2 10

1H,1H,2H,2H,3H,3H-perfluoro-n-decanoicacid (7:3FTCA)

2 10

Reference Method: EPA 1633 by LC/MS/MS o Water: 28 days

Container:

o Water: Two 250mL HDPE plastic bottles per sample; receive on ice

Analysis Request Forms o PFAS for Ground, Surface, and Waste Water: EQP4014-05 Rev 08/2024 o Test Request: PFAS- Method 1633

Michigan.gov/EGLELab Page 16 of 23 (Rev. 07/2026)

Environmental Lab Reporting Limits, Test Capabilities, and Target

Per- and Polyfluoroalkyl Substances (PFAS) by EPA Method 1633

RL

(ng/L) Perfluoropropanoic acid (PFPrA) 2 Perfluorobutanoic acid (PFBA) 2

Perfluoro-3-methoxypropanoic acid

(PFMPA)

2H,2H,3H,3H-perfluorohexanoic acid

(3:3FTCA)

Perfluoropropanesulfonic acid (PFPrS) 2 Perfluoropentanoic acid (PFPeA) 2 Perfluoro-4-methoxybutanoic acid

(PFMBA)

1H,1H,2H,2H-perfluorohexanesulfonic acid (4:2FTS)

Nonafluoro-3,6-dioxaheptanoic acid

(NFDHA)

Perfluorohexanoic acid (PFHxA) 2 Perfluorobutanesulfonic acid (PFBS) 2

Hexafluoropropylene oxide dimer acid

(HFPO-DA)

2H,2H,3H,3H-perfluorooctanoic acid

(5:3FTCA)

Perfluoro(2-ethyoxyethane)sulfonic acid

(PFEESA)

Perfluoroheptanoic acid (PFHpA) 2 Perfluoro-1-butanesulfonamide (PFBSA) 2

4,8-Dioxa-3H-perfluorononanoic acid

(ADONA)

Perfluoropentanesulfonic acid (PFPeS) 2 1H,1H,2H,2H-perfluorooctanesulfonic acid (6:2FTS)

Perfluorooctanoic acid (PFOA) 2 Perfluorohexanesulfonic acid (PFHxS) 2 2H,2H,3H,3H-perfluorodecanoicacid

(7:3FTCA)

Analyte

RL

(ng/L) Perfluorononanoic acid (PFNA) 2

1H,1H,2H,2H-perfluorodecanesulfonic acid (8:2FTS)

Perfluoro-4-ethylcyclohexanesulfonic acid

(PFECHS)

Perfluoroheptanesulfonic acid (PFHpS) 2 N-methylperfluorooctane sulfonamidoacetic acid (NMeFOSAA)

Perfluorodecanoic acid (PFDA) 2 N-ethyl perfluorooctane sulfonamidoacetic acid (NEtFOSAA)

Perflurooctanesulfonic acid (PFOS) 2 Perfluoro-1-hexanesulfonamide

(PFHxSA)

Perfluoroundecanoic acid (PFUnA) 2 9-Chlorohexadecafluoro-3-oxanone-1-sulfonic acid (9Cl-PF3ONS)

Perfluorononanesulfonic acid (PFNS) 2 Perfluorododecanoic acid (PFDoA) 2

Perfluorodecanesulfonic acid (PFDS) 2 Perfluorotridecanoic acid (PFTrDA) 2

11-Chloroeicosafluoro-3-oxaundecane-1-sulfonic acid (11Cl-PF3OUdS)

Perfluoro-1-octanesulfonamide (PFOSA) 2 Perfluorotetradecanoic acid (PFTeDA) 2

Perfluorododecanesulfonic acid (PFDoS) 2 N-methyl perfluorooctane sulfonamidoethanol (NMeFOSE)

N-methyl perfluorooctane sulfonamide (NMeFOSA)

N-ethyl perfluorooctane sulfonamidoethanol (NEtFOSE)

N-ethyl perfluorooctane sulfonamide (NEtFOSA)

Michigan.gov/EGLELab Page 17 of 23 (Rev. 07/2026)

Environmental Lab Reporting Limits, Test Capabilities, and Target

Volatile Organics Analysis Offerings

Reference Method: EPA SW-846 8260B by GC-MS o Water: 14 days o Soil: 14 days

Container:

o Water: Three 40mL glass vials with PTFE septum; 1:1 HCl preserved to pH<2; receive on ice o Soil: 40mL tared glass vial; 10g of sample in MeOH with PTFE septum;

receive on ice Analysis Request Forms o Water: EQP4014-01 Rev 05/2024 o Test Request: Volatiles- Full List or BTEX/MTBE/TMB or Chlorinated only****

Volatile Organic Compounds (VOCs) in Waters and Soils

RL

(ug/L)

Soil

RL

(ug/kg) 1,1,1,2-Tetrachloroethane 1 50

1,1,1-Trichloroethane 1 50 1,1,2,2-Tetrachloroethane 1 50

1,1,2-Trichloroethane 1 50 1,1,2-Trichlorotrifluoroethane 1 50

1,1-Dichloroethane 1 50 1,1-Dichloroethylene 1 50

1,2,3-Trichlorobenzene 5 250 1,2,3-Trichloropropane 1 50 1,2,3-Trimethylbenzene 1 50 1,2,4-Trichlorobenzene 5 250 1,2,4-Trimethylbenzene 1 50

1,2-Dibromo-3-chloropropane 5 250 1,2-Dibromoethane 1 50

1,2-Dichlorobenzene 1 50 1,2-Dichloroethane 1 50

1,2-Dichloropropane 1 50

Analyte Water

RL

(ug/L)

Soil

RL

(ug/kg) 1,3,5-Trimethylbenzene 1 50

1,3-Dichlorobenzene 1 50 1,4-Dichlorobenzene 1 50

2,2,4-Trimethylpentane 5 250 2-Butanone (MEK) 5 250

2-Methylnaphthalene 5 250 2-Propanone (acetone) 20 1000

4-Methyl-2-pentanone (MIBK) 5 250 Acrylonitrile 5 250

Benzene 1 50 Bromochloromethane 1 50

Bromodichloromethane 1 50 Bromoform 1 50

Bromomethane 5 200 Carbon disulfide 1 50

Carbon tetrachloride 1 50 Chlorobenzene 1 50

Michigan.gov/EGLELab Page 18 of 23 (Rev. 07/2026)

Environmental Lab Reporting Limits, Test Capabilities, and Target

Volatile Organics Analysis Offerings (Continued)

Volatile Organic Compounds (VOCs) in Waters and Soils (Continued)

RL

(ug/L)

Soil

RL

(ug/kg) Chloroethane 5 250 Chloroform 1 50

Chloromethane 5 250 cis-1,2-Dichloroethylene 1 50 cis-1,3-Dichloropropylene 1 50 Cyclohexane 5 250

Dibromochloromethane 1 50 Dibromomethane 1 50

Dichlorodifluoromethane 5 250 Diethyl ether 5 200

Diisopropyl Ether 5 250 Ethylbenzene 1 50

Ethyltertiarybutylether 5 250 Hexachloroethane 5 250

Hexane 1 50 Isopropylbenzene 1 50 m & p - Xylene 2 100 Methylcyclopentane 1 50 Methylene chloride 5 100

Analyte Water

RL

(ug/L)

Soil

RL

(ug/kg) Methyltertiarybutylether 1 50

Naphthalene 5 250 n-Butylbenzene 1 50 n-Heptane 1 50 n-Propylbenzene 1 50 o-Xylene 1 50 Pentane 5 5 sec-Butylbenzene 1 50 Styrene 1 50 tert-Butylbenzene 1 50 tertiary Butyl Alcohol 50 2500 tertiaryAmylmethylether 5 250 Tetrachloroethylene 1 50

Tetrahydrofuran 5 250 Toluene 1 50 trans-1,2-Dichloroethylene 1 50 trans-1,3-Dichloropropylene 1 50

Trichloroethylene 1 50 Trichlorofluoromethane 1 50

Vinyl chloride 1 50

Reference Method: EPA 624 by GC-MS

Hold Time:

o Water: 14 days

Container:

o Water: Three 40mL glass vials with PTFE septum; 1:1 HCl preserved to pH<2; receive on ice Wastewater Analysis Request Form (EQP4014-02 Rev 05/2024) o Test Request: Volatiles- Full List

Michigan.gov/EGLELab Page 19 of 23 (Rev. 07/2026)

Environmental Lab Reporting Limits, Test Capabilities, and Target

Volatile Organic Compounds (VOCs) in Wastewater

(ug/L) 1,1,1,2-Tetrachloroethane 1

1,1,1-Trichloroethane 1 1,1,2,2-Tetrachloroethane 1

1,1,2-Trichloroethane 1 1,1-Dichloroethane 1

1,1-Dichloroethylene 1 1,2,3-Trichlorobenzene 5 1,2,3-Trichloropropane 1 1,2,3-Trimethylbenzene 1 1,2,4-Trichlorobenzene 5 1,2,4-Trimethylbenzene 1

1,2-Dibromo-3-chloropropane

1,2-Dibromoethane 1 1,2-Dichlorobenzene 1 1,2-Dichloroethane 1

1,2-Dichloropropane 1 1,3,5-Trimethylbenzene 1

1,3-Dichlorobenzene 1 1,4-Dichlorobenzene 1 2-Butanone (MEK) 5

2-Hexanone 5 2-Methylnaphthalene 5

2-Propanone (acetone) 20 Acrylonitrile 5

Benzene 1 Bromobenzene 1

Bromochloromethane 1 Bromodichloromethane 1

Bromoform 1 Bromomethane 5

Analyte Reporting Limit

(ug/L) Carbon disulfide 1

Carbon tetrachloride 1 Chlorobenzene 1 Chloroethane 5 Chloroform 1

Chloromethane 5 cis-1,2-Dichloroethylene 1 cis-1,3-Dichloropropylene 1 Cyclohexane 5

Dibromochloromethane 1 Dibromomethane 1

Dichlorodifluoromethane 5 Diethyl ether 5 Ethylbenzene 1

Hexachloroethane 5 Isopropylbenzene 1 m & p - Xylene 2 Methylene chloride 5

Methyltertiarybutylether 1 Naphthalene 5 n-Butylbenzene 1 n-Propylbenzene 1 o-Xylene 1 p-Isopropyl toulene 1 sec-Butylbenzene 1

Styrene 1 tert-Butylbenzene 1

Tetrachloroethylene 1 Tetrahydrofuran 5

Toluene 1 trans-1,2-Dichloroethylene 1

Michigan.gov/EGLELab Page 20 of 23 (Rev. 07/2026)

Environmental Lab Reporting Limits, Test Capabilities, and Target

Volatile Organic Compounds (VOCs) in Wastewater (Continued)

(ug/L) trans-1,3-Dichloropropylene 1 trans-1,4-Dichloro-2-butene 5

Trichloroethylene 1

Analyte Reporting Limit

(ug/L) Trichlorofluoromethane 1

Vinyl chloride 1

**** BTEX/MTBE/TMB only Chlorinated Volatiles only

Reference Method: Modified EPA SW-846 8260B SIM by GC-MS o Water: 14 days

Container:

o Water: Two 40mL glass vials with PTFE septum; 1:1 HCl preserved to pH<2;

receive on ice Analysis Request Forms o Water: EQP4014-01 Rev 05/2024 o Test Request: 1,4-Dioxane

1,4- Dioxane in Water

1,4- Dioxane 0.2

Reference Method: EPA SW-846 8260B by GC-MS o Water and Soil: 14 days

Container:

o Water: Two 40mL glass vials with PTFE septum; 1:1 HCl preserved to pH<2;

receive on ice o Soil: 40mL tared glass vial; 10g of sample in MeOH with PTFE septum;

receive on ice Analysis Request Forms o Water: EQP4014-01 Rev 05/2024 or Soil: EQP4014-03 Rev 01/2024 o Test Request: GRO

Michigan.gov/EGLELab Page 21 of 23 (Rev. 07/2026)

Environmental Lab Reporting Limits, Test Capabilities, and Target

Gasoline Range Organics (GRO)

Water Reporting Limit

(ug/L) Soil Reporting Limit

(ug/kg) Gasoline Range Organics (C6-C10) 100 5000

Reference Method: EPA TO-14 by GC-FID o Water: 14 days o Air: 30 days

Container:

o Water: Two 40mL glass vials with red rubber septum; 1:1 HCl preserved to pH<2; receive on ice o Air: 1L Amber Bottlevac or 6L Suma Canister

Analysis Request Forms o Water: EQP4014-01 Rev 05/2024 o Air: EQP4014-04 Rev 01/2024 o Test Request:

Water: VOA-Methane Air: Methane, Ethane, Ethene

Methane, Ethane, and Ethene

Water Reporting Limit

(mg/L) Air Reporting Limit

(ppmv) Methane 0.010 20 Ethane 0.10 20

Ethene/Ethylene 0.010 20

Reference Method: EPA TO-15 2nd Edition by GC-MS

Hold Time: 30 days Container: 1L Amber Bottlevac or 6L Suma Canister Air Analysis Request Form: EQP4014-04 Rev 01/2024 o Test Request: Bottlevac or Canister

Michigan.gov/EGLELab Page 22 of 23 (Rev. 07/2026)

Environmental Lab Reporting Limits, Test Capabilities, and Target

Volatile Organic Compounds (VOCs) in Air

Air RL (ug/m3)

1,1,1-Trichloroethane 1.6 1,1,2,2-Tetrachloroethane 2.0

1,1,2-Trichloroethane 1.6 1,1,2-Trichlorotrifluoroethane 2.2

1,1-Dichloroethane 1.2 1,1-Dichloroethylene 1.2

1,2,3-Trichlorobenzene 7.2 1,2,3-Trichloropropane 1.8 1,2,3-Trimethylbenzene 1.4 1,2,4-Trichlorobenzene 3.6 1,2,4-Trimethylbenzene 1.4

1,2-Dibromo-3-chloropropane 2.8 1,2-Dibromoethane 2.2

1,2-Dichlorobenzene 1.8 1,2-Dichloroethane 1.2

1,2-Dichloropropane 1.3 1,3,5-Trimethylbenzene 1.4

1,3-Butadiene 0.64 1,3-Dichlorobenzene 1.8 1,4-Dichlorobenzene 1.8

2,2,4-Trimethylpentane 1.4 2-Butanone (MEK) 14

2-Methylnaphthalene 28 4-Methyl-2-pentanone (MIBK) 4.0

Acetone 58 Acetonitrile 1.6 Acrylonitrile 1.1

Benzene 0.93 Bromobenzene 1.9

Bromodichloromethane 2.0 Bromoform 3.0

Analyte Air RL (ug/m3)

Bromomethane 1.1 Carbon disulfide 0.91

Carbon tetrachloride 1.8 Chlorobenzene 1.3 Chloroethane 0.77 Chloroform 1.4

Chloromethane 0.60 cis-1,2-Dichloroethylene 1.2 cis-1,3-Dichloropropylene 1.3 Cyclohexane 1.0

Dibromochloromethane 2.5 Dichlorodifluoromethane 1.4

Diethyl ether 2.9 Diisopropyl Ether 1.2

Ethanol 46 Ethylbenzene 1.3

Ethyltertiarybutylether 1.2 Hexachloroethane 2.8

Hexane 3.4 Isopropyl Alcohol 60 Isopropylbenzene 1.4 m & p - Xylene 1.3 Methylcyclopentane 1.0 Methylene chloride 1.0

Methyltertiarybutylether 1.8 Naphthalene 25 n-Butylbenzene 5.3 n-Heptane 1.2 n-Propylbenzene 1.4 o-Xylene 1.3 Pentane 2.9 sec-Butylbenzene 1.6

Michigan.gov/EGLELab Page 23 of 23 (Rev. 07/2026)

Environmental Lab Reporting Limits, Test Capabilities, and Target

Volatile Organic Compounds (VOCs) in Air (Continued)

Air RL (ug/m3)

Styrene 1.2 tert-Butylbenzene 5.3 tertiary Butyl Alcohol 74 tertiaryAmylmethylether 1.2

Tetrachloroethylene 2.0 Tetrahydrofuran 0.86

Analyte Air RL (ug/m3)

Toluene 1.1 trans-1,2-Dichloroethylene 1.2 trans-1,3-Dichloropropylene 1.3 Trichloroethylene 1.6

Trichlorofluoromethane 1.6 Vinyl chloride 0.74

Reference Method: EPA SW-846 8260B by GC-MS

Reference Method: EPA TO-15 2nd Edition by GC-MS