ATTACH_1_STANDARDIZED_TEST_REPORTS.doc

STANDARDIZED FORMAT FOR USE IN THE

PREPARATION OF PRODUCT TEST REPORTS

GENERAL INSTRUCTIONS

February 2010

These instructions are designed for use as a guide in preparing/formatting test reports in a consistent manner. Computer generated or typed test reports are acceptable. A Standardized Test report format is provided at Figure I and includes all tests approved for all refined products. The Test Codes used in this standard report format will be incorporated into future Electronic Data Interchange (EDI) transmissions of test result data.

The ASTM Aviation Turbine Fuel Report Form found in ASTM Method D-1655 was used as a template for the expanded “generic” standard test report form for other refined products. The codes containing an alpha character indicate alternative methods used to measure a property or characteristic. A numeric change of “1” unit indicates one or more measurements, ratings or test conditions which can be reported for a particular method. All measurements are in metric units, except for the API gravity reported at 60oF.

The use of this code provides flexibility in adding or deleting test methods while not affecting the existing methods and thus eliminates the need for additional programming. For example, an ASTM method may have an equivalent ISO or other method. If the ASTM test method number is used as a reference, the ISO equivalent may be lost unless new programming is established to make it a choice. With the code, the equivalency will continue without any additional programming. Another example is adding a new test method for Freezing Point. There are currently 3 methods (300A-C) for measuring the characteristic of freezing point. The new method would be assigned the code “300D” and would be available immediately as an alternative method for determination of freezing point while retaining the old methods without having to renumber the whole list and change associated database programming.

Each test report should be tailored to include only those rows of information that are applicable to the specific product being tested and the methods used to evaluate each property. Select only those methods authorized by the product specification unless otherwise stated in the contract. The code used should be limited to the actual test method used for a particular analysis. If an analysis is performed which is not cited by the specification, report the result, units and method used at the bottom of the report. If a test code does not appear for a specification or contract approved method, contact the Defense Energy Support Center (DLA ENERGY) at commercial (703) 767-8360.

DETAILED INSTRUCTIONS FOR THE STANDARD TEST REPORT FORMAT (FIGURE 1)

Item 1: This date is the tank approval date, which is usually the date the testing is completed or the report date.

Item 2B: The City should match the “Shipped From” city on the DD 250-series document.

Item 6A: Record the basic slate of crudes from which this product is derived.

Item 6B: Annotate the refining processes used in the production of this product (e.g., Atmospheric Distillation; Hydrogenation, Hydrocracking, etc)

Item 8: Report the quantity in US Gallons shipped from the above batch in the above tank under DLA ENERGY Contract. This entry need not be completed if the same batch will be used for subsequent shipments. In this case, assure that the tank number, batch number and report date are on the DD-250-series documents for shipments made from this tank

Items 600-series: The JFTOT test, although done using one ASTM test method, can be performed at different temperatures. Also, results for separate JFTOT analysis performed at two different temperatures can be reported on the same report. If test results for only one temperature is being reported, use Item 600 A-C to report the temperature of the test and 601, 602 and 603 as appropriate to report the results. If a second temperature is being reported, use Item 604 to report the temperature of this second run and Items 605-607 to report the corresponding values for the second test.

Item 750: Use this item to report the result of the Water Separometer Index - Modified (WSIM) which is performed for product acceptance.

Item 751: This code for this item describes what additives were present in the fuel sample tested for WSIM and for which the result was reported in Item 750. Each code value represents a combination of the five additives possible in jet fuel. The codes and corresponding combinations are found in Table A below.

Item 750X: This item is used to report the special hand blend of all additives which are required by the fuel specification, regardless of whether or not the additives are required by contract. These additives include anti-oxidant, corrosion inhibitor, fuel system icing inhibitor, static dissipater additive and, if permitted by contract, metal deactivator. The result for this special test is a report only and is used as a base line in determining if the time and/or place of additive injection affects fuel quality. This reporting requirement is in addition to other reporting requirements for WSIM.

Items 801, 811, 821, 831, and 841: These codes indicate when an additive was injected during the procurement process. It is a one-character field and is “S” if the additive was blended into the shipping tank, “I” if the additive was line injected, or blank if the additive was not injected at the refinery or terminal location.

Table A

Code Additives Code Additives Code Additives Code Additives Code Additives Neat

AO/CI

CI/MDA

AO/CI/MDA

FSII/SDA/MDA

AO

AO/FSII

FSII/SDA

AO/FSII/MDA

AO/CI/FSII/SDA

CI

AO/SDA

FSII/MDA

AO/FSII/SDA

AO/FSII/SDA/MDA

FSII

AO/MDA

MDA/SDA

AO/SDA/MDA

CI/FSII/SDA/MDA

SDA

CI/FSII

AO/CI/FSII

CI/FSII/SDA

AO/CI/FSII/SDA/MDA

MDA

CI/SDA

AO/CI/SDA

CI/FSII/MDA

FIGURE I - STANDARD TEST REPORT FORMAT

REPORT DATE:

(MM/DD/YY)_______________________

2A

CONTRACTOR:

2B

REFINERY CITY:

2C

STATE/COUNTRY:

3A

CONTRACT NUMBER:

(SPO600-YY-D-NNNN)____________________

3B

CONTRACT LINE ITEM NUMBER:

3C

DLA ENERGY ORDER NUMBER

4A

TANK NUMBER:

4B BATCH NUMBER (In Tank):

4C

SAMPLE NUMBER:

PRODUCT:

6A

CRUDE OIL SLATE:

6B

CRUDE PROCESSING TECHNIQUE:

SHIPPED TO:

QUANTITY FROM TANK SHIPPED TO DLA ENERGY:

__________________________________USG

APPEARANCE

Code Method Test Unit Code Method Test Unit 010A D-156 Saybolt Color 1-Color

010B D-6045 Saybolt Color (Spectro) 1-Color

D-4176 Visual appearance C&B D-4176 Haze Rating Method

030A D-1500 ASTM Color 0.5-Color

030B D-6045 ASTM Color (Spectro) 0.5-Color

COMPOSITION

Code Method Test Unit Code Method Test Unit 100A D-664 Total Acid Number – Potent mg KOH/g

100B D-974 Acid Number - Color Titrat mg KOH/g 100C D-3242 Acidity in Aviation Fuels mg KOH/g

100D D-3339 Acid Number, Semi-Micro mg KOH/g

100IPA IP-354

Total Acidity mg KOH/g

IP-182

Inorganic Acid Number mg KOH/g

FTM-5101

Neutrality Method

D-1093 Acidity/Alkalinity Acidic/Basic/Neutral

110A D-1319 Aromatics vol%

110B D-4420 Aromatics by GC vol%

110C D-5580 Aromatics by GC vol%

110D D-6379 Aromatics by LC w/RI vol%

110IPA

IP-156

Aromatics -Flourescent Indicator vol%

110IPB

IP-436

Aromatics-LC w/RI vol%

D-1319 Olefins vol% D-1840 Naphthalene vol%125A D-4420 Benzene vol%

125B D-3606 Benzene vol%

125C D-5580 Benzene – GC vol%

D-3227 Mercaptan Sulfur mass %

130IPA

IP-342

Sulfur (Mercaptan) mass%

130ISA

ISO-3012

Mercaptan Sulfur mass%

135A D-3231 Phosphorous

0.1 mg/L

135D

IP-501

Phosphorous mg/kg

D-4952 Doctor Test Pos/Neg

140IPA

IP-30

Sulfur (Doctor Test) Pos/Neg

150A D-129 Sulfur by Oxygen Bomb mass %

150B D-1266 Sulfur by Lamp mass %

150C D-1552 Sulfur - Furnace mass %

150D D-2622 Sulfur by X-Ray Spec mass %

150E D-3120 Trace Sulfur ppm

150F D-4294 Sulfur by X-Ray Flour mass %

150G D-5453 Sulfur by UV ppm

150IPA

IP-336

Sulfur Content mass %

150IPB

IP-107

Sulfur Content mass %

150IPC

IP-243

Sulfur Content mg/kg(ppm)

150IPD

IP-373

Sulfur Content mg/kg

150IPE

IP-447

Sulfur Content mass %

150ISA

ISO-4260

Sulfur Content mass %

150ISB

ISO-8754

Sulfur – X-ray Fluoresence mass %

150ISC

ISO-14596

Sulfur Content mass %

150L D-6920 Total Sulfur ppm

150M D7039 Total Sulfur ppm 155A App A, Spec C-10 Content mass %

App A, Spec Other Hydrocarbon mass %

App A, Spec MCH Content mass %

160A D-3343 Hydrogen Content mass %

160B D-3701 Hydrogen Content - NMR mass % 160C D-4808 Hydrogen Cont LoRes NMR mass %

160D D-5291 Hydrogen Cont – Instrument mass%

160E D-7171 Hydrogen Cont LoRes NMR mass%

D-5184 Al plus Si (ISO 10478) ppm 165A

IP-501

Aluminum and Silicon mg/kg 170A D-3237 Lead in Gasoline by AA g/L

170B D-3341 Lead in Gasoline by ICl g/L

170C D-5059 Lead in Gasoline by X-Ray g/L

180A D-4815 Ethers and Alcohols by GC mass %

180B D-5845 Ethers and Alcohols by IR mass %

190A D-3605 Trace Metals - Calcium mg/L

190B D-7111 Trace Metals - Calcium mg/L 190C

IP-501

Calcium mg/kg 191A D-3605 Trace Metals - Lead mg/L

191B D-7111 Trace Metals - Lead mg/L

192A D-3605 Trace Metals - Na & K mg/L

192B D-7111 Trace Metals - Na & K mg/L

193A D-3605 Trace Metals - Vanadium mg/L

193B

ISO14597

Trace Metals – Vanadium mg/L 193C D-5863 Trace Metals-Vanadium mg/kg 193D D-7111 Trace Metals – Vanadium mg/L193E

IP-501

Vanadium mg/kg

IP-501

Zinc mg/kg

D-3703 Peroxide Content mg/kg

VOLATILITY

Code Method Test Unit Code Method Test Unit 200A D-86 Distillation by Auto/Manual

200B D-2887 Distillation by GC

200IPA

IP-123

Distillation by ATM °C

200IPB

IP-406

Distillation by ATM °C

2001SA

ISO-3405

Distillation by Apparatus °C

Initial Boiling Point oC

10% Recovered oC

20% Recovered oC

50% Recovered oC

85% Recovered oC

90% Recovered oC

95% Recovered oC

Evaporated @ 70oC vol%

Evaporated @ 100oC vol%

Evaporated @ 180oC vol%

Final Boiling Point oC

% Recovered vol%

% Residue vol%

% Loss vol%

% Residue + Loss vol%

220A D-56 Flash Point - Tag oC

220B D-93 Flash Point - P/M oC

220C D-3828 Flash Point - Seta, Method A oC

220D D-3828 Flash Point - Seta, Method B oC

220E D-92 Flash Point - COC oC

220F D-6450 Flash Point – CCCFP °C

220IPA

IP-170

Flash Point – Abel °C

220IPB

IP-523

Flash Point – RECC °C

220ISA

ISO-3679

Flash Point – Abel °C

D-3828 Flash Point - Seta (Flash/No F) “F” or “N”

230A D-1298 Density @ 15oC -Hydrom kg/L

230B D-4052 Density @ 15oC - Digital kg/L

230IPA

IP-365

Density @ 15°C Oscillation U-tube kg/m3

230IPB

IP-160

Density @15°C – Hydrom kg/m3

230ISA

ISO-3675

Density @15°C-Hydrom kg/L

230ISB

ISO-12185 Density @15°C-Digital g/mL 231A D-1298 API Gravity @ 60oF oAPI

231B D-4052 API Gravity @ 60oF oAPI

231C D-287 API Gravity @ 60oF oAPI

240A D-323

RVP

kPa

240B D-4953 Vapor Press - Dry Meth kPa

240C D-5190 Vapor Press - Automatic kPa

240D D-5191 Vapor Press - Mini Meth kPa

240E D-5482 Vapor Press - Mini -Atm kPa

250A D-2533 V/L Ratio - Buret Unit@oC

250B D-5188 V/L Ratio - Evac Chamb Unit@oC

250C D-4814 Estimated V/L Ratio Unit@oC

STANAG

7090 - Vapor Lock Index

FLUIDITY

Code Method Test Unit Code Method Test Unit 300A D-2386 Freezing Point oC

300B D-5901 Freezing Point oC

300C D-5972 Freezing Point oC

300D D-4305 Freezing Point, Low Temps oC

300E D-7153 Freezing Point oC 300F D-7154 Freezing Point °C

300IPA

IP16

Freezing Point °C

300IPB

IP-435

Freezing Point °C

300IPC

IP-528

Freezing Point °C

300IPD

IP-529

Freezing Point °C D-445 Viscosity cSt

310IPA

IP-71

Viscosity @ 20°C mm2/s

310ISA

ISO-3104

Viscostiy @20° C mm2/s D-445 Viscosity Temperature oC 320A D-2500 Cloud Point oC

320B D-5771 Cloud Point (Optical) oC

320C D-5772 Cloud Point (Linear Cool) oC

320D D-5773 Cloud Point (Constant Cool) oC

321A

IP-309

Cold Filter Plugging Point oC

321B D-6371 Cold Filter Plugging Point oC

321C D-6371(M)Cold Filter Plugging Point oC 321D D-4539 Low Temp Flow Test °C 330A D-97 Pour Point oC

330B D-5949 Pour Point – Pulsing Method oC

330C D-5950 Pour Point oC 330D D-5985 Pour Point-Rational Method °C

340A D-5001 Lubricity (BOCLE) 0.01mm

340B D-6079 Lubricity (Wear Scar)

0.01 mm

COMBUSTION

Code Method Test Unit Code Method Test Unit

400A D-240 Neat Heat by Bomb MJ/kg

400B D-1405 Net Heat (Anal-Grav(oF),S) MJ/kg

400C D-3338 Net Heat (Aromat,API,Dist,S) MJ/kg

400D D-4529 Net Heat (Dens-Anal(oC),S) MJ/kg

400E D-4809 Net Heat by Bomb-Precision MJ/kg

400F D-4868 Net and Gross Heat MJ/kg

400G D-6446 Net Heat of Aviation Fuels MJ/kg

400H D-2382 Net Heat by Bomb – Precision MJ/kg

400IPA

IP-12

Net Heat of Combustion-Av Fuels J/g

400IPB

IP-355

Net Heat of Combustion-Av Fuels MJ/kg

D-1740 Luminometer Number Unit D-1322 Smoke Point mm

420IPA

IP-57

Smoke Point mm

420ISA

ISO-3014

Smoke Point mm

D-482 Ash Content mass %

440A D-189 Conradson Carbon Res mass %

440B D-524 Ramsbottom Carbon Res mass %

440C D-4530 Carbon Residue - Micro mass %

CORROSION

Code Method Test Unit Code Method Test Unit

D-130 Copper Strip Corrosion Method

500IPA

IP-154

Copper Strip Corrosion Method

500ISA

ISO-2160

Copper Strip Corrosion Method

510A

IP-227

Silver Strip Corrosion Method

STABILITY

Code Method Test Unit Code Method Test Unit

600A D-3241 JFTOT @ 275oC Method

600B D-3241 JFTOT @ 260oC

600C

JFTOT @ 245oC Method

600IPA

IP-323

JFTOT@275°C

Method

600IPB

IP-323

JFTOT@260°C

Method

600IPC

IP-323

JFTOT@245°C

Pressure Change mm Hg

Visual Rating

Spun Rating Method

D-3241 Other JFTOT Temperature oC

D-3241 Pressure Change @ Other Temp mm Hg

D-3241 Visual Rating @ Other Temp Method

D-3241 Spun Rating @ Other Temp Method

Serial Number for 600A Tube

Serial Number for 604 Tube 610A D-525 Ox Stability -Gasoline minute

610C D-873 Ox Stability – Aviation Fuels mg/100mL

620A D-2274 Accelerated Stability mg/100mL

620B D-5304 Accelerated Stab - O2 Opres mg/100mL

620C

ISO10307

Tot Sed in Residual Fuels %mass

CONTAMINANTS

Code Method Test Unit Code Method Test Unit

IP-225

Copper Content ppb

D-381 Existent Gum mg/100mL

710IPA

IP-540

Existent Gum mg/100mL

D-381 Washed Gum mg/100mL

720A D-2276 Particulate Cont mg/L

720B D-5452 Particulate Cont mg/L

720D D-6217 Particulate Cont – Middle Dist mg/L

Annex Filtration Time minutes

D-1094 Water Reaction - Interface

D-1094 Water Reaction - Separation Method

D-1094 Water Reaction - Vol Chng Method

D-3948

WSIM

Method

Additives Present (See Note) (List A) 750X D-3948 WSIM - Special (See Note) Method

D-4814 Phase Separation (Haze) oC

D-4814 Phase Separation (Sep) oC

D-1401 Demulsification @ 25oC minutes

780A D-1796 Water & Sed vol%

780B D-2709 Water & Sed vol%

781A D-95 Water by Distillation vol%

781B D-6304 Water by Karl Fischer mg/kg

D-473 Sediment by Extraction mass %

SW-846

EPA Metals - As Method

SW-846

EPA Metals - Cd Method

SW-846

EPA Metals - Cr Method

SW-846

EPA Metals - Pb Method

SW-846

Total Halogens Method

ADDITIVES

Code Method Test/Additive Unit Code Method Test/Additive Unit 800A Antioxidant Topanol A mg/L

800B Antioxidant

HITEC 4733

mg/L

800C Antioxidant

AN 733

mg/L

800D Antioxidant

AO-31

mg/L

800E Antioxidant

AO-30

mg/L

800F Antioxidant

AO-29

mg/L

800G Antioxidant Nalco EC5208A mg/L

800H Antioxidant

TOLAD 3915

mg/L

800I Antioxidant

TOLAD 3920

mg/L

800J Antioxidant

TOPANOL AN

mg/L

800K Antioxidant

CHIMIC 4327

mg/L

800L Antioxidant

AO-37

mg/L

800M Antioxidant

BETZ BQ203

mg/L

800N Antioxidant Chemlink No 4650 mg/L

800O Antioxidant Petroxylin E219 mg/L

800P Antioxidant Kerobit TP-26 mg/L

800Q Antioxidant Pet411K mg/L

800R Antioxidant

ISONOX 133

mg/L

800S Antioxidant

AO-37B

mg/L

800T Antioxidant

ISONOX 75

mg/L

800U Antioxidant

HITEC 4775

mg/L

800V Antioxidant

BETZ 8Q2065

mg/L

800W Antioxidant

BHT

mg/L

800X Antioxidant

HITEC 4778

mg/L

800Y Antioxidant Octel 37/70 mg/L

Additive Injection Point (Note)

810A Metal Deactivator (DMD) mg/L

810B Metal Deactivator (DMD-2) mg/L

Additive Injection Point (Note)

Conductivity Improver mg/L

Additive Injection Point (Note)

830A

FSII (D-5006)

vol%

830B

FSII (FTM-5327)

vol%

830C

FSII (FTM-5340)

vol%

830D

FSII (FTM-5340) - EGME

vol%

830E FSII – Calculated vol%

Additive Injection Point (Note)

840A Corr Inhibitor

PRI-19

mg/L

840B Corr Inhibitor

DCI-4A

mg/L

840C Corr Inhibitor

DCI-6A

mg/L

840D Corr Inhibitor

HITEC 580

mg/L

840E Corr Inhibitor Petrolite NC-351 mg/L

840F Corr Inhibitor

NALCO 5403

mg/L

840G Corr Inhibitor

TOLAD 3220

mg/L

840H Corr Inhibitor

UNICOR J

mg/L

840I Corr Inhibitor

IPC-4410

mg/L

840J Corr Inhibitor

IPC-4445

mg/L

840K Corr Inhibitor

MOBILAD F800

mg/L

840L Corr Inhibitor

NALCO 5405

mg/L

840M Corr Inhibitor

NUCHEM PCI-105

mg/L

840N Corr Inhibitor

TOLAD 249

mg/L

840O Corr Inhibitor

WELCHEM 91120

mg/L

840P Corr Inhibitor

SPEC-AID 8021

mg/L

840Q Corr Inhibitor

RPS-613

mg/L

840R Corr Inhibitor

SPEC AID 8Q22

mg/L

840S Corr Inhibitor

TOLAD 4410

mg/L

Additive Injection Point (Note)

Thermal Stability Additive mg/L

Additive Injection Point (Note)

Diesel Fuel Stabilizer Additive mg/L

Additive Injection Point (Note)

Ignition Improver mg/L

Additive Injection Point (Note)

OTHER TESTS

Code Method Test Unit Code Method Test Unit D-2624 Conductivity pS/m

900IPA

IP-274

Conductivity pS/m D-2624 Temperature at Measurement oC

910A D-976 Calc Cetane Index - 2 Var Method

910B D-4737 Calc Cetane Index - 4 Var Method

D-613 Cetane Number Method

920A D-2699 Research Octane Number Method

920B D-2885 Research Octane Number Method

921A D-2700 Motor Octane Number Method

921B D-2885 Motor Octane Number Method

D-611 Aniline Point oC

D-4814 Water Tolerance oC