B05 Amendment A00001 Attachment 3 - Dustin WST_Paint Analysis_May 2021.pdf

http://www.teklabinc.com/

May 07, 2021

WorkOrder: 21041550IHS Pb/Cr Samples Dustin OKRE:

Dear Brian Bridgers:

TEKLAB, INC received 2 samples on 4/27/2021 9:20:00 AM for the analysis presented in the following report.

Samples are analyzed on an as received basis unless otherwise requested and documented. The sample results contained in this report relate only to the requested analytes of interest as directed on the chain of custody. NELAP accredited fields of testing are indicated by the letters NELAP under the Certification column. Unless otherwise documented within this report, Teklab Inc. analyzes samples utilizing the most current methods in compliance with 40CFR.

All tests are performed in the Collinsville, IL laboratory unless otherwise noted in the Case Narrative.

All quality control criteria applicable to the test methods employed for this project have been satisfactorily met and are in accordance with NELAP except where noted. The following report shall not be reproduced, except in full, without the written approval of Teklab, Inc.

If you have any questions regarding these tests results, please feel free to call.

Sincerely, 1610 N. Minnesota Ave Sioux Falls, SD 57101

(501) 733-5502

(605) 334-9752

TEL:

FAX:

Brian Bridgers Maguire Iron, Inc.

Shelly A. Hennessy Project Manager (618)344-1004 ex 36 SHennessy@teklabinc.com

Illinois 100226

Kansas E-10374

Louisiana 05002

Louisiana 05003

Oklahoma 9978

This reporting package includes the following:

Report Contents

Client Project: IHS Pb/Cr Samples Dustin OK

Client: Maguire Iron, Inc.

Report Date: 07-May-21

Work Order: 21041550 http://www.teklabinc.com/

Cover Letter 1

Report Contents 2

Definitions 3

Case Narrative 5

Accreditations 6

Laboratory Results 7

Receiving Check List 9

Chain of Custody Appended

____TeklabHdrP

Definitions

Client Project: IHS Pb/Cr Samples Dustin OK

Client: Maguire Iron, Inc.

Report Date: 07-May-21

Work Order: 21041550 http://www.teklabinc.com/

Abbr Definition

* Analytes on report marked with an asterisk are not NELAP accredited

CCV Continuing calibration verification is a check of a standard to determine the state of calibration of an instrument between recalibration.

CRQL A Client Requested Quantitation Limit is a reporting limit that varies according to customer request. The CRQL may not be less than the MDL.

DF Dilution factor is the dilution performed during analysis only and does not take into account any dilutions made during sample preparation. The reported result is final and includes all dilution factors.

DNI Did not ignite

DUP Laboratory duplicate is a replicate aliquot prepared under the same laboratory conditions and independently analyzed to obtain a measure of precision.

ICV Initial calibration verification is a check of a standard to determine the state of calibration of an instrument before sample analysis is initiated.

IDPH IL Dept. of Public Health

LCS Laboratory control sample is a sample matrix, free from the analytes of interest,spiked with verified known amounts of analytes and analyzed exactly like a sample to establish intra-laboratory or analyst specific precision and bias or to assess the performance of all or a portion of the measurement system.

LCSD Laboratory control sample duplicate is a replicate laboratory control sample that is prepared and analyzed in order to determine the precision of the approved test method. The acceptable recovery range is listed in the QC Package (provided upon request).

MBLK Method blank is a sample of a matrix similar to the batch of associated sample (when available) that is free from the analytes of interest and is processed simultaneously with and under the same conditions as samples through all steps of the analytical procedures, and in which no target analytes or interferences should present at concentrations that impact the analytical results for sample analyses.

MDL "The method detection limit is defined as the minimum measured concentration of a substance that can be reported with 99% confidence that the measured concentration is distinguishable from method blank results."

MS Matrix spike is an aliquot of matrix fortified (spiked) with known quantities of specific analytes that is subjected to the entire analytical procedures in order to determine the effect of the matrix on an approved test method’s recovery system. The acceptable recovery range is listed in the QC Package (provided upon request).

MSD Matrix spike duplicate means a replicate matrix spike that is prepared and analyzed in order to determine the precision of the approved test method.

The acceptable recovery range is listed in the QC Package (provided upon request).

MW Molecular weight

NC Data is not acceptable for compliance purposes

ND Not Detected at the Reporting Limit

NELAP NELAP Accredited

PQL Practical quantitation limit means the lowest level that can be reliably achieved within specified limits of precision and accuracy during routine laboratory operation conditions.

RL The reporting limit the lowest level that the data is displayed in the final report. The reporting limit may vary according to customer request or sample dilution. The reporting limit may not be less than the MDL.

RPD Relative percent difference is a calculated difference between two recoveries (ie. MS/MSD). The acceptable recovery limit is listed in the QC Package (provided upon request).

SPK The spike is a known mass of target analyte added to a blank sample or sub-sample; used to determine recovery deficiency or for other quality control purposes.

Surr Surrogates are compounds which are similar to the analytes of interest in chemical composition and behavior in the analytical process, but which are not normally found in environmental samples.

TIC Tentatively identified compound: Analytes tentatively identified in the sample by using a library search. Only results not in the calibration standard will be reported as tentatively identified compounds. Results for tentatively identified compounds that are not present in the calibration standard, but are assigned a specific chemical name based upon the library search, are calculated using total peak areas from reconstructed ion chromatograms and a response factor of one. The nearest Internal Standard is used for the calculation. The results of any TICs must be considered estimated, and are flagged with a "T". If the estimated result is above the calibration range it is flagged "ET"

TNTC Too numerous to count ( > 200 CFU )

Definitions

Client Project: IHS Pb/Cr Samples Dustin OK

Client: Maguire Iron, Inc.

Report Date: 07-May-21

Work Order: 21041550 http://www.teklabinc.com/

Qualifiers # - Unknown hydrocarbon B - Analyte detected in associated Method Blank

C - RL shown is a Client Requested Quantitation Limit E - Value above quantitation range

H - Holding times exceeded I - Associated internal standard was outside method criteria

J - Analyte detected below quantitation limits M - Manual Integration used to determine area response

ND - Not Detected at the Reporting Limit R - RPD outside accepted recovery limits

S - Spike Recovery outside recovery limits T - TIC(Tentatively identified compound)

X - Value exceeds Maximum Contaminant Level

Case Narrative

Client Project: IHS Pb/Cr Samples Dustin OK

Client: Maguire Iron, Inc.

Report Date: 07-May-21

Work Order: 21041550 http://www.teklabinc.com/

Cooler Receipt Temp: NA °C

Locations

___________________________________Collinsville

5445 Horseshoe Lake Road

Collinsville, IL 62234-7425

(618) 344-1004

(618) 344-1005 jhriley@teklabinc.com

___________________________________Springfield

3920 Pintail Dr

Springfield, IL 62711-9415

(217) 698-1004

(217) 698-1005

KKlostermann@teklabinc.com

___________________________________Kansas City

8421 Nieman Road

Lenexa, KS 66214

(913) 541-1998

(913) 541-1998 jhriley@teklabinc.com

___________________________________Collinsville Air

5445 Horseshoe Lake Road

Collinsville, IL 62234-7425

(618) 344-1004

(618) 344-1005

EHurley@teklabinc.com

___________________________________Chicago

1319 Butterfield Rd.

Downers Grove, IL 60515

(630) 324-6855 arenner@teklabinc.com

Accreditations

Client Project: IHS Pb/Cr Samples Dustin OK

Client: Maguire Iron, Inc.

Report Date: 07-May-21

Work Order: 21041550 http://www.teklabinc.com/

NELAPState Cert # Exp Date LabDept

Illinois 100226 1/31/2022 CollinsvilleNELAPIEPA

Kansas E-10374 4/30/2022 CollinsvilleNELAPKDHE

Louisiana 05002 6/30/2021 CollinsvilleNELAPLDEQ

Louisiana 05003 6/30/2021 CollinsvilleNELAPLDEQ

Oklahoma 9978 8/31/2021 CollinsvilleNELAPODEQ

Arkansas 88-0966 3/14/2022 CollinsvilleADEQ

Illinois 17584 5/31/2021 CollinsvilleIDPH

Kentucky 0073 1/31/2022 CollinsvilleUST

Missouri 00930 5/31/2021 CollinsvilleMDNR

Missouri 930 1/31/2022 CollinsvilleMDNR

Page 6 of 9http://www.teklabinc.com/

TeklabHdrP

Laboratory Results

Client Project: IHS Pb/Cr Samples Dustin OK

Client: Maguire Iron, Inc.

Report Date: 07-May-21

Work Order: 21041550 http://www.teklabinc.com/

Analyses Result Units Date AnalyzedRL DFCertification Qual

Collection Date: 04/20/2021 10:00

Lab ID: 21041550-001 Client Sample ID: Dustin OK #1 Tank Legs

Matrix: SOLID

Batch

SW-846 3050B, 6010B, METALS BY ICP

Chromium 05/06/2021 1:5310.4 mg/Kg 51350NELAP 176520

Lead 05/06/2021 1:5341.7 mg/Kg 52850NELAP 176520

TeklabHdrP

Laboratory Results

Client Project: IHS Pb/Cr Samples Dustin OK

Client: Maguire Iron, Inc.

Report Date: 07-May-21

Work Order: 21041550 http://www.teklabinc.com/

Analyses Result Units Date AnalyzedRL DFCertification Qual

Collection Date: 04/20/2021 10:30

Lab ID: 21041550-002 Client Sample ID: Dustin OK #2 Tank Shell

Matrix: SOLID

Batch

SW-846 3050B, 6010B, METALS BY ICP

Chromium 05/06/2021 1:5610.0 mg/Kg 5691NELAP 176520

Lead 05/06/2021 1:5640.0 mg/Kg 59220NELAP 176520

Receiving Check List

Client Project: IHS Pb/Cr Samples Dustin OK

Client: Maguire Iron, Inc.

Report Date: 07-May-21

Work Order: 21041550 http://www.teklabinc.com/

Received By: PRYCarrier: Std US Mail

Completed by: Reviewed by:

On:

27-Apr-21

On:

27-Apr-21

Shipping container/cooler in good condition? Yes No Not Present

Chain of custody present? Yes No

Chain of custody signed when relinquished and received? Yes No

Chain of custody agrees with sample labels? Yes No

Samples in proper container/bottle? Yes No

Sample containers intact? Yes No

Sufficient sample volume for indicated test? Yes No

All samples received within holding time? Yes No

Container/Temp Blank temperature in compliance? Yes No

Temp °C

When thermal preservation is required, samples are compliant with a temperature between 0.1°C - 6.0°C, or when samples are received on ice the same day as collected.

Water – at least one vial per sample has zero headspace? Yes No No VOA vials

Water - pH acceptable upon receipt? Yes No NA

Type of thermal preservation? None Ice Blue Ice Dry Ice

Chain of custody 1 Extra pages included 0

Reported field parameters measured: Field Lab NA

Water - TOX containers have zero headspace? No TOX containersYes No

NPDES/CWA TCN interferences checked/treated in the field? Yes No NA

Marvin L. Darling Elizabeth A. Hurley

December 02, 2021

Mr. Pat McKinney, Mayor Dustin PWA PO Box 487 Dustin, Oklahoma 74839

Re: Permit No. WL000032210860 Town of Dustin - Elevated Steel Water Storage Tank Facility No. 1020511

Dear Mr. McKinney:

Enclosed is Permit No. WL000032210860 for the construction of 330 linear feet of six (6) inch PVC potable water line, one (1) new 50,000 gallon elevated spheroidal potable water storage tank, and all appurtenances to serve the Town of Dustin - Elevated Steel Water Storage Tank, Hughes County, Oklahoma.

The project authorized by this permit should be constructed in accordance with the plans approved by this Department on December 02, 2021. Any deviations from the approved plans and specifications affecting capacity, flow or operation of units must be approved, in writing, by the Department before changes are made.

Receipt of this permit should be noted in the minutes of the next regular meeting of the Dustin PWA, after which it should be made a matter of permanent record.

We are returning one (1) set of the approved plans to you, one (1) set to your engineer and retaining one

(1) set for our files.

Respectfully, D. Adam Divine, P.E.

Construction Permit Section Water Quality Division

AD/RC/md

Enclosure c: Vance Pennington, Regional Manager, DEQ

TECUMSEH DEQ OFFICE

Javier Franco, , Indian Health Service

PERMIT No. WL000032210860

WATER LINES

FACILITY No. 1020511

PERMIT TO CONSTRUCT

December 02, 2021

Pursuant to O.S. 27A 2-6-304, the Dustin PWA is hereby granted this Tier I Permit to construct 330 linear feet of six (6) inch PVC potable water line, one (1) new 50,000 gallon elevated spheroidal potable water storage tank, and all appurtenances to serve the Town of Dustin - Elevated Steel Water Storage Tank, located in NW 1/4 of Section 10, T-9-N, R-12-E, Hughes County, Oklahoma, in accordance with the plans approved December 02, 2021.

By acceptance of this permit, the permittee agrees to operate and maintain the facility in accordance with the Public Water Supply Operation rules (OAC 252:631) and to comply with the State Certification laws, Title 59, Section 1101-1116 O.S. and the rules and regulations adopted thereunder regarding the requirements for certified operators.

This permit is issued subject to the following provisions and conditions.

1) This water line does not provide fire flow.

2) That the recipient of the permit is responsible that the project receives supervision and inspection by competent and qualified personnel.

3) That construction of all phases of the project will be started within one year of the date of approval or the phases not under construction will be resubmitted for approval as a new project.

4) That no significant information necessary for a proper evaluation of the project has been omitted or no invalid information has been presented in applying for the permit.

5) That the Oklahoma Department of Environmental Quality shall be kept informed on occurrences which may affect the eventual performance of the works or that will unduly delay the progress of the project.

6) That wherever water and sewer lines are constructed with spacing of 10 feet or less, sanitary protection will be provided in accordance with Public Water Supply Construction Standards [OAC 252:626-19-2].

7) That before placing this facility into service, at least two samples of the water, taken on different days, shall be tested for bacteria to show that it is safe for drinking purposes.

8) That any deviations from approved plans or specifications affecting capacity, flow or operation of units must be approved by the Department before any such deviations are made in the construction of this project.

9) That the recipient of the permit is responsible for the continued operation and maintenance of these facilities in accordance with rules and regulations adopted by the Environmental Quality Board, and that this Department will be notified in writing of any sale or transfer of ownership of these facilities.

10) The issuance of this permit does not relieve the responsible parties of any obligations or liabilities which the permittee may be under pursuant to prior enforcement action taken by the Department.

11) That the permittee is required to inform the developer/builder that a DEQ Storm Water Construction

Permit is required for a construction site that will disturb one (1) acre or more in accordance with OPDES, 27A O.S. Section 2-6-201 et seq. For information or a copy of the GENERAL PERMIT (OKR10) FOR STORM WATER DISCHARGES FROM CONSTRUCTION ACTIVITIES, Notice of Intent (NOI) form, Notice of Termination (NOT) form, or guidance on preparation of a Pollution Prevention Plan, contact the Storm Water Unit of the Water Quality Division at P.O. Box 1677, Oklahoma City, OK 73101-1677 or by phone at (405) 702-8100.

12) That any notations or changes recorded on the official set of plans and specifications in the

Oklahoma Department of Environmental Quality files shall be part of the plans as approved.

13) That water lines shall be located at least fifteen (15) feet from all parts of septic tanks and absorption fields, or other sewage treatment and disposal systems.

14) That whenever plastic pipe is approved and used for potable water, it shall bear the seal of the

National Sanitation Foundation and meet the appropriate commercial standards.

15) That when it is impossible to obtain proper horizontal and vertical separation as stipulated in Public

Water Supply Construction Standards OAC 252:626-19-2(h)(1) and OAC 252:626-19-2(h)(2), respectively, the sewer shall be designed and constructed equal to water pipe, and shall be pressure tested to the highest pressure obtainable under the most severe head conditions of the collection system prior to backfilling.

Failure to appeal the conditions of this permit in writing within 30 days from the date of issue will constitute acceptance of the permit and all conditions and provisions.

AD

Rocky Chen, P.E., Engineering Manager, Construction Permit Section Water Quality Division