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ATTACHMENT 3
REQUIRED COMPOUNDS AND LIMITS OF QUANTITATION
VOCs - EPA 624
| Compounds |
| Required LOQ |
| Units |
| Compounds |
| Required LOQ |
| Units |
| 1,1,1-Trichloroethane |
| 5.0 |
| ug/L |
| 1,1,2,2-Tetrachloroethane |
| 5.0 |
| ug/L |
| 1,1,2-Trichloroethane |
| 5.0 |
| ug/L |
| 1,1-Dichloroethane |
| 5.0 |
| ug/L |
| 1,1-Dichloroethene |
| 5.0 |
| ug/L |
| cis-1,3-Dichloropropene |
| 5.0 |
| ug/L |
| 1,2-Dichlorobenzene |
| 5.0 |
| ug/L |
| Dibromochloromethane |
| 5.0 |
| ug/L |
| 1,2-Dichloroethane |
| 5.0 |
| ug/L |
| 1,2-Dichloropropane |
| 5.0 |
| ug/L |
| Methyl tert-butyl ether (MtBE) |
| 5.0 |
| ug/L |
| 1,3-Dichlorobenzene |
| 5.0 |
| ug/L |
| Methylene Chloride |
| 5.0 |
| ug/L |
| 1,4-Dichlorobenzene |
| 5.0 |
| ug/L |
| p-isopropyltoluene |
| 10 |
| ug/L |
| 2-Chloroethyl vinyl ether |
| 5.0 |
| ug/L |
| Tetrachloroethene |
| 5.0 |
| ug/L |
| trans-1,2-Dichloroethene |
| 5.0 |
| ug/L |
| trans-1,3-Dichloropropene |
| 5.0 |
| ug/L |
| Bromodichloromethane |
| 5.0 |
| ug/L |
| Trichlorofluoromethane |
| 5.0 |
| ug/L |
| Carbon Tetrachloride |
| 5.0 |
| ug/L |
BTEX in Soils by 8260x
Required
| Xylene (Total) |
| 0.006 |
| mg/kg |
(or 0.002 mg/kg for o-xylene and 0.004 mg/kg for m+p-toluene)
BTEX in water by 8260x
Required
(or 2 ug/L for o-xylene and 4 ug/L for m+p-toluene)
5030B/8260x in water
Required
Required
| 1,1,1,2-tetrachloroethane |
| 2 |
| ug/L |
| Chloroacetonitrile |
| 20 |
| ug/L |
| 1,1,1-trichloroethane |
| 2 |
| ug/L |
| 1,1,2,2-tetrachloroethane |
| 2 |
| ug/L |
| 1,1,2-trichloroethane |
| 2 |
| ug/L |
| 1,1-dichloroethane |
| 2 |
| ug/L |
| 1,1-dichloroethene |
| 2 |
| ug/L |
| cis-1,2-dichloroethene |
| 2 |
| ug/L |
| 1,1-dichloropropene |
| 2 |
| ug/L |
| cis-1,3-dichloropropene |
| 2 |
| ug/L |
| 1,2,3-trichlorobenzene |
| 2 |
| ug/L |
| Dibromochloromethane |
| 2 |
| ug/L |
| 1,2,3-trichloropropane |
| 2 |
| ug/L |
| 1,2,4-trichlorobenzene |
| 2 |
| ug/L |
| Dichlorodifluoromethane |
| 2 |
| ug/L |
| 1,2,4-trimethylbenzene |
| 2 |
| ug/L |
| 1,2-dibromo-3-chloropropane |
| 2 |
| ug/L |
| Ethyl methacrylate |
| 20 |
| ug/L |
| 1,2-dichlorobenzene |
| 2 |
| ug/L |
| Hexachlorobutadiene |
| 2 |
| ug/L |
| 1,2-dichloroethane |
| 2 |
| ug/L |
| 1,2-dichloropropane |
| 2 |
| ug/L |
| 1,3,5-trimethylbenzene |
| 2 |
| ug/L |
| 1,3-dichlorobenzene |
| 2 |
| ug/L |
| 1,3-dichloropropane |
| 2 |
| ug/L |
| Methacrylonitrile |
| 20 |
| ug/L |
| 1,4-dichlorobenzene |
| 2 |
| ug/L |
| Methyl methacrylate |
| 20 |
| ug/L |
| 2,2-dichloropropane |
| 2 |
| ug/L |
| Methylene chloride |
| 2 |
| ug/L |
| Methyl-t-butyl ether |
| 2 |
| ug/L |
| 4-isopropyltoluene |
| 2 |
| ug/L |
| 4-methyl-2-pentanone |
| 20 |
| ug/L |
| Bromochloromethane |
| 2 |
| ug/L |
| trans-1,2-dichloroethene |
| 2 |
| ug/L |
| bromodichloromethane |
| 2 |
| ug/L |
| trans-1,3-dichloropropene |
| 2 |
| ug/L |
| trans-1,4-dichloro-2-butene |
| 20 |
| ug/L |
| Trichlorofluoromethane |
| 2 |
| ug/L |
| Carbon tetrachloride |
| 2 |
| ug/L |
5035/8260x in soil
Required
Required
| 1,1,1,2-tetrachloroethane |
| 0.002 |
| mg/kg |
| Chloroacetonitrile |
| 0.02 |
| mg/kg |
| 1,1,1-trichloroethane |
| 0.002 |
| mg/kg |
| Chlorobenzene |
| 0.002 |
| mg/kg |
| 1,1,2,2-tetrachloroethane |
| 0.002 |
| mg/kg |
| 1,1,2-trichloroethane |
| 0.002 |
| mg/kg |
| 1,1-dichloroethane |
| 0.002 |
| mg/kg |
| Chloromethane |
| 0.002 |
| mg/kg |
| 1,1-dichloroethene |
| 0.002 |
| mg/kg |
| cis-1,2-dichloroethene |
| 0.002 |
| mg/kg |
| 1,1-dichloropropene |
| 0.002 |
| mg/kg |
| cis-1,3-dichloropropene |
| 0.002 |
| mg/kg |
| 1,2,3-trichlorobenzene |
| 0.002 |
| mg/kg |
| Dibromochloromethane |
| 0.002 |
| mg/kg |
| 1,2,3-trichloropropane |
| 0.002 |
| mg/kg |
| Dibromomethane |
| 0.002 |
| mg/kg |
| 1,2,4-trichlorobenzene |
| 0.002 |
| mg/kg |
| Dichlorodifluoromethane |
| 0.002 |
| mg/kg |
| 1,2,4-trimethylbenzene |
| 0.002 |
| mg/kg |
| 1,2-dibromo-3-chloropropane |
| 0.002 |
| mg/kg |
| Ethyl methacrylate |
| 0.02 |
| mg/kg |
| 1,2-dibromoethane |
| 0.002 |
| mg/kg |
| 1,2-dichlorobenzene |
| 0.002 |
| mg/kg |
| Hexachlorobutadiene |
| 0.002 |
| mg/kg |
| 1,2-dichloroethane |
| 0.002 |
| mg/kg |
| Hexachloroethane |
| 0.02 |
| mg/kg |
| 1,2-dichloropropane |
| 0.002 |
| mg/kg |
| 1,3,5-trimethylbenzene |
| 0.002 |
| mg/kg |
| Isopropylbenzene |
| 0.002 |
| mg/kg |
| 1,3-dichlorobenzene |
| 0.002 |
| mg/kg |
| 1,3-dichloropropane |
| 0.002 |
| mg/kg |
| Methacrylonitrile |
| 0.02 |
| mg/kg |
| 1,4-dichlorobenzene |
| 0.002 |
| mg/kg |
| Methyl acrylate |
| 0.02 |
| mg/kg |
| 1-chlorobutane |
| 0.02 |
| mg/kg |
| Methyl methacrylate |
| 0.02 |
| mg/kg |
| 2,2-dichloropropane |
| 0.002 |
| mg/kg |
| Methylene chloride |
| 0.002 |
| mg/kg |
| Methyl-t-butyl ether |
| 0.02 |
| mg/kg |
| 2-chlorotoluene |
| 0.002 |
| mg/kg |
| n-butylbenzene |
| 0.002 |
| mg/kg |
| 2-nitropropane |
| 0.02 |
| mg/kg |
| n-propylbenzene |
| 0.002 |
| mg/kg |
| 4-chlorotoluene |
| 0.002 |
| mg/kg |
| 4-isopropyltoluene |
| 0.002 |
| mg/kg |
| 4-methyl-2-pentanone |
| 0.02 |
| mg/kg |
| sec-butylbenzene |
| 0.002 |
| mg/kg |
| tert-butylbenzene |
| 0.002 |
| mg/kg |
| Allyl chloride |
| 0.02 |
| mg/kg |
| Tetrachloroethene |
| 0.002 |
| mg/kg |
| Tetrahydrofuran |
| 0.02 |
| mg/kg |
| Bromochloromethane |
| 0.002 |
| mg/kg |
| trans-1,2-dichloroethene |
| 0.002 |
| mg/kg |
| bromodichloromethane |
| 0.002 |
| mg/kg |
| trans-1,3-dichloropropene |
| 0.002 |
| mg/kg |
| trans-1,4-dichloro-2-butene |
| 0.02 |
| mg/kg |
| Trichloroethene |
| 0.002 |
| mg/kg |
| Carbon disulfide |
| 0.02 |
| mg/kg |
| Trichlorofluoromethane |
| 0.002 |
| mg/kg |
| Carbon tetrachloride |
| 0.002 |
| mg/kg |
| Vinyl chloride |
| 0.002 |
| mg/kg |
TO15 in air
Required
Required
| 1,1,1,2-tetrachloroethane |
| 0.5 |
| ppb(v) |
| 1,1,1-trichloroethane |
| 0.5 |
| ppb(v) |
| 1,1,2,2-tetrachloroethane |
| 0.5 |
| ppb(v) |
| cis-1,2-dichloroethene |
| 0.5 |
| ppb(v) |
| 1,1,2-trichloroethane |
| 0.5 |
| ppb(v) |
| cis-1,3-dichloropropene |
| 0.5 |
| ppb(v) |
| 1,1,2-trichloro-1,2,2-trifluoroethane |
| 0.5 |
| ppb(v) |
| 1,1-dichloroethane |
| 0.5 |
| ppb(v) |
| Dibromochloromethane |
| 0.5 |
| ppb(v) |
| 1,1-dichloroethene |
| 0.5 |
| ppb(v) |
| Dibromomethane |
| 0.5 |
| ppb(v) |
| 1,2,3-trichloropropane |
| 0.5 |
| ppb(v) |
| Dichlorodifluoromethane |
| 0.5 |
| ppb(v) |
| 1,2,4-trichlorobenzene |
| 2 |
| ppb(v) |
| Dichlorofluoromethane |
| 0.5 |
| ppb(v) |
| 1,2,4-trimethylbenzene |
| 0.5 |
| ppb(v) |
| 1,2-dibromoethane |
| 0.5 |
| ppb(v) |
| 1,2-dichlorobenzene |
| 0.5 |
| ppb(v) |
| Ethyl methacrylate |
| 1 |
| ppb(v) |
| 1,2-dichloroethane |
| 0.5 |
| ppb(v) |
| 1,2-dichloropropane |
| 0.5 |
| ppb(v) |
| 1,2-dichlorotetrafluoroethane |
| 0.5 |
| ppb(v) |
| Hexachlorobutadiene |
| 2 |
| ppb(v) |
| 1,3,5-trimethylbenzene |
| 0.5 |
| ppb(v) |
| Hexachloroethane |
| 1 |
| ppb(v) |
| 1,3-dichlorobenzene |
| 0.5 |
| ppb(v) |
| 1,4-dichlorobenzene |
| 0.5 |
| ppb(v) |
| Isopropylbenzene |
| 0.5 |
| ppb(v) |
| Methyl methacrylate |
| 1 |
| ppb(v) |
| 4-ethyltoluene |
| 0.5 |
| ppb(v) |
| Methylene chloride |
| 2 |
| ppb(v) |
| 4-methyl-2-pentanone |
| 5 |
| ppb(v) |
| Methyl styrene (alpha) |
| 1 |
| ppb(v) |
| Methyl-t-butyl ether |
| 0.5 |
| ppb(v) |
| Allyl chloride |
| 0.5 |
| ppb(v) |
| Tert-butyl alcohol |
| 1 |
| ppb(v) |
| Benzyl chloride |
| 0.5 |
| ppb(v) |
| Tetrachloroethene |
| 0.5 |
| ppb(v) |
| Tetrahydrofuran |
| 0.5 |
| ppb(v) |
| Bromodichloromethane |
| 0.5 |
| ppb(v) |
| trans-1,2-dichloroethene |
| 0.5 |
| ppb(v) |
| trans-1,3-dichloropropene |
| 0.5 |
| ppb(v) |
| Carbon disulfide |
| 1 |
| ppb(v) |
| Trichloroethene |
| 0.5 |
| ppb(v) |
| Carbon tetrachloride |
| 0.5 |
| ppb(v) |
| Trichlorofluoromethane |
| 0.5 |
| ppb(v) |
| Chlorodifluoromethane |
| 0.5 |
| ppb(v) |
| Vinyl chloride |
| 0.5 |
| ppb(v) |
PAH compound lists and required limits of quantitation (LOQ)
Standard GC/MS Full Scan and GC/MS SIM
| Compounds |
| Required LOQ |
| Units |
Units
PAHs in Water by SIM
PAHs in Water by GC/MS
| 1-Methylnaphthalene |
| 0.1 |
| ug/L |
| 1-Methylnaphthalene |
| 10 |
| ug/L |
| 2-Methylnaphthalene |
| 0.1 |
| ug/L |
| 2-Methylnaphthalene |
| 10 |
| ug/L |
| Benzo(a)anthracene |
| 0.1 |
| ug/L |
| Benzo(a)anthracene |
| 10 |
| ug/L |
| Benzo(b)fluoranthene |
| 0.1 |
| ug/L |
| Benzo(b)fluoranthene |
| 10 |
| ug/L |
| Benzo(g,h,i)perylene |
| 0.1 |
| ug/L |
| Benzo(g,h,i)perylene |
| 10 |
| ug/L |
| Benzo(k)fluoranthene |
| 0.1 |
| ug/L |
| Benzo(k)fluoranthene |
| 10 |
| ug/L |
| Dibenz(a,h)anthracene |
| 0.1 |
| ug/L |
| Dibenz(a,h)anthracene |
| 10 |
| ug/L |
| Indeno(1,2,3-cd)pyrene |
| 0.1 |
| ug/L |
| Indeno(1,2,3-cd)pyrene |
| 10 |
| ug/L |
PAHs in Soil by SIM
PAHs in Soil by GC/MS
| 1-Methylnaphthalene |
| 0.005 |
| mg/kg |
| 1-Methylnaphthalene |
| 0.33 |
| mg/kg |
| 2-Methylnaphthalene |
| 0.005 |
| mg/kg |
| 2-Methylnaphthalene |
| 0.33 |
| mg/kg |
| Acenaphthylene |
| 0.005 |
| mg/kg |
| Acenaphthylene |
| 0.33 |
| mg/kg |
| Benzo(a)anthracene |
| 0.005 |
| mg/kg |
| Benzo(a)anthracene |
| 0.33 |
| mg/kg |
| Benzo(a)pyrene |
| 0.005 |
| mg/kg |
| Benzo(a)pyrene |
| 0.33 |
| mg/kg |
| Benzo(b)fluoranthene |
| 0.005 |
| mg/kg |
| Benzo(b)fluoranthene |
| 0.33 |
| mg/kg |
| Benzo(g,h,i)perylene |
| 0.005 |
| mg/kg |
| Benzo(g,h,i)perylene |
| 0.33 |
| mg/kg |
| Benzo(k)fluoranthene |
| 0.005 |
| mg/kg |
| Benzo(k)fluoranthene |
| 0.33 |
| mg/kg |
| Dibenz(a,h)anthracene |
| 0.005 |
| mg/kg |
| Dibenz(a,h)anthracene |
| 0.33 |
| mg/kg |
| Indeno(1,2,3-cd)pyrene |
| 0.005 |
| mg/kg |
| Indeno(1,2,3-cd)pyrene |
| 0.33 |
| mg/kg |
8270x in water (with 3000 series extraction)
Required
Required
| 1,2,4-Trichlorobenzene |
| 10 |
| ug/L |
| Di-n-butylphthalate |
| 10 |
| ug/L |
| 1,2-Dichlorobenzene |
| 10 |
| ug/L |
| Di-n-octylphthalate |
| 10 |
| ug/L |
| 1,3-Dichlorobenzene |
| 10 |
| ug/L |
| 1,4-Dichlorobenzene |
| 10 |
| ug/L |
| Dibenz[a,h]anthracene |
| 10 |
| ug/L |
| 2,2’-oxybis(1-chloropropane) (CAS 108-60-1) |
| 10 |
| ug/L |
| 2,4,5-Trichlorophenol |
| 10 |
| ug/L |
| Dimethylphthalate |
| 10 |
| ug/L |
| 2,4,6-Trichlorophenol |
| 10 |
| ug/L |
| 2,4-Dichlorophenol |
| 10 |
| ug/L |
| 2,4-Dimethylphenol |
| 10 |
| ug/L |
| Hexachlorobenzene |
| 10 |
| ug/L |
| 2,4-Dinitrophenol |
| 10 |
| ug/L |
| Hexachlorobutadiene |
| 10 |
| ug/L |
| 2,4-Dinitrotoluene |
| 10 |
| ug/L |
| Hexachlorocyclopentadiene |
| 10 |
| ug/L |
| 2,6-Dinitrotoluene |
| 10 |
| ug/L |
| 2-Chloronaphthalene |
| 10 |
| ug/L |
| Indeno[1,2,3-cd]pyrene |
| 10 |
| ug/L |
| 2-Methyl-4,6-dinitrophenol |
| 10 |
| ug/L |
| m- + p-methylphenol |
| 20 |
| ug/L |
| 2-Methylnaphthalene |
| 10 |
| ug/L |
| N-Nitrosodimethylamine |
| 10 |
| ug/L |
| N-Nitrosodi-n-propylamine |
| 10 |
| ug/L |
| N-Nitrosodiphenylamine |
| 10 |
| ug/L |
| 4-Bromophenyl phenylether |
| 10 |
| ug/L |
| 4-Chloro-3-methylphenol |
| 10 |
| ug/L |
| 4-Chlorophenyl phenylether |
| 10 |
| ug/L |
| Pentachlorophenol |
| 10 |
| ug/L |
| Additional compounds to be requested for some projects |
| Not specified (NS) |
| 1,2-Diphenylhydrazine |
| 10 ug/L |
| Benzo[b]fluoranthene |
| 10 |
| ug/L |
| 3,3’-Dichlorobenzidine |
| 10 ug/L |
| Benzo[g,h,i]perylene |
| 10 |
| ug/L |
| Benzo[k]fluoranthene |
| 10 |
| ug/L |
| Benz[a]anthracene |
| 10 |
| ug/L |
| bis(2-Chloroethoxy)methane |
| 10 |
| ug/L |
| bis(2-Chloroethyl)ether |
| 10 |
| ug/L |
| bis(2-Ethylhexyl)phthalate |
| 10 |
| ug/L |
| Butylbenzylphthalate |
| 10 |
| ug/L |
8270 in soils (with 3000 series extraction)
Required
Required
| Compound Name (base list) |
| LOQ |
| Units |
| Compound Name (base list) |
| LOQ |
| Units |
| 1,2,4-Trichlorobenzene |
| 0.33 |
| mg/kg |
| Di-n-butylphthalate |
| 0.33 |
| mg/kg |
| 1,2-Dichlorobenzene |
| 0.33 |
| mg/kg |
| Di-n-octylphthalate |
| 0.33 |
| mg/kg |
| 1,3-Dichlorobenzene |
| 0.33 |
| mg/kg |
| 1,4-Dichlorobenzene |
| 0.33 |
| mg/kg |
| Dibenz[a,h]anthracene |
| 0.33 |
| mg/kg |
| 2,2’-oxybis(1-chloropropane) (CAS 108-60-1) |
| 0.33 |
| mg/kg |
| Diethylphthalate |
| 0.33 |
| mg/kg |
| 2,4,5-Trichlorophenol |
| 0.33 |
| mg/kg |
| Dimethylphthalate |
| 0.33 |
| mg/kg |
| 2,4,6-Trichlorophenol |
| 0.33 |
| mg/kg |
| 2,4-Dichlorophenol |
| 0.33 |
| mg/kg |
| 2,4-Dimethylphenol |
| 0.33 |
| mg/kg |
| Hexachlorobenzene |
| 0.33 |
| mg/kg |
| 2,4-Dinitrophenol |
| 0.33 |
| mg/kg |
| Hexachlorobutadiene |
| 0.33 |
| mg/kg |
| 2,4-Dinitrotoluene |
| 0.33 |
| mg/kg |
| Hexachlorocyclopentadiene |
| 0.33 |
| mg/kg |
| 2,6-Dinitrotoluene |
| 0.33 |
| mg/kg |
| Hexachloroethane |
| 0.33 |
| mg/kg |
| 2-Chloronaphthalene |
| 0.33 |
| mg/kg |
| Indeno[1,2,3-cd]pyrene |
| 0.33 |
| mg/kg |
| 2-Chlorophenol |
| 0.33 |
| mg/kg |
| 2-Methyl-4,6-dinitrophenol |
| 0.33 |
| mg/kg |
| m- + p-methylphenol |
| 0.66 |
| mg/kg |
| 2-Methylnaphthalene |
| 0.33 |
| mg/kg |
| N-Nitrosodimethylamine |
| 0.33 |
| mg/kg |
| 2-Nitroaniline |
| 0.33 |
| mg/kg |
| N-Nitrosodi-n-propylamine |
| 0.33 |
| mg/kg |
| N-Nitrosodiphenylamine |
| 0.33 |
| mg/kg |
| 3-Nitroaniline |
| 0.33 |
| mg/kg |
| 4-Bromophenyl phenylether |
| 0.33 |
| mg/kg |
| 4-Chloro-3-methylphenol |
| 0.33 |
| mg/kg |
| o-methylphenol |
| 0.33 |
| mg/kg |
| 4-Chlorophenyl phenylether |
| 0.33 |
| mg/kg |
| Pentachlorophenol |
| 0.33 |
| mg/kg |
| 4-Chloroaniline |
| 0.33 |
| mg/kg |
| 4-Nitroaniline |
| 0.33 |
| mg/kg |
| Acenaphthylene |
| 0.33 |
| mg/kg |
| Additional compounds to be requested for some projects |
| Not specified (NS) |
| Benzo[a]pyrene |
| 0.33 |
| mg/kg |
| Benzo[b]fluoranthene |
| 0.33 |
| mg/kg |
| 3,3’-Dichlorobenzidine |
| NS |
| Benzo[g,h,i]perylene |
| 0.33 |
| mg/kg |
| Benzo[k]fluoranthene |
| 0.33 |
| mg/kg |
| Benzyl alcohol |
| 0.33 |
| mg/kg |
| Benz[a]anthracene |
| 0.33 |
| mg/kg |
| bis(2-Chloroethoxy)methane |
| 0.33 |
| mg/kg |
| bis(2-Chloroethyl)ether |
| 0.33 |
| mg/kg |
| bis(2-Ethylhexyl)phthalate |
| 0.33 |
| mg/kg |
| Butylbenzylphthalate |
| 0.33 |
| mg/kg |
Acid Extractables and Base Neutrals – EPA 625
| Compounds |
| LOQ |
| Units |
| Compounds |
| LOQ |
| Units |
1,2,4-Trichlorobenzene
| 5.0 |
| ug/L |
| Benz(a)anthracene |
| 5.0 |
| ug/L |
| 1,2-Dichlorobenzene |
| 10 |
| ug/L |
| bis(2-Chloroethoxy)methane |
| 5.0 |
| ug/L |
| 1,3-Dichlorobenzene |
| 10 |
| ug/L |
| bis(2-Chloroethyl)ether |
| 5.0 |
| ug/L |
| 1,4-Dichlorobenzene |
| 10 |
| ug/L |
| bis(2-Ethylhexyl)phthalate |
| 5.0 |
| ug/L |
| 2,4,6-Trichlorophenol |
| 5.0 |
| ug/L |
| Butylbenzylphthalate |
| 5.0 |
| ug/L |
| 2,2’-oxybis(1-chloropropane) (CAS 108-60-1) |
| 5.0 |
| ug/L |
| Chrysene |
| 5.0 |
| ug/L |
| 2,4-Dichlorophenol |
| 5.0 |
| ug/L |
| Dibenz(a,h)anthracene |
| 5.0 |
| ug/L |
| 2,4-Dimethylphenol |
| 5.0 |
| ug/L |
| Diethylphthalate |
| 5.0 |
| ug/L |
| 2,4-Dinitrophenol |
| 30 |
| ug/L |
| Dimethylphthalate |
| 5.0 |
| ug/L |
| 2,4-Dinitrotoluene |
| 5.0 |
| ug/L |
| Di-n-butylphthalate |
| 5.0 |
| ug/L |
| 2,6-Dinitrotoluene |
| 5.0 |
| ug/L |
| Di-n-octylphthalate |
| 5.0 |
| ug/L |
| 2-Chloronaphthalene |
| 5.0 |
| ug/L |
| Fluoranthene |
| 5.0 |
| ug/L |
| 2-Chlorophenol |
| 5.0 |
| ug/L |
| Fluorene |
| 5.0 |
| ug/L |
| 2-Methyl-4,6-dinitrophenol |
| 15 |
| ug/L |
| Hexachlorobenzene |
| 5.0 |
| ug/L |
| 2-Nitrophenol |
| 5.0 |
| ug/L |
| Hexachlorobutadiene |
| 5.0 |
| ug/L |
| 3,3'-Dichlorobenzidine |
| 5.0 |
| ug/L |
| Hexachlorocyclopentadiene |
| 15 |
| ug/L |
| 4-Bromophenyl-phenylether |
| 5.0 |
| ug/L |
| Hexachloroethane |
| 5.0 |
| ug/L |
| 4-Chloro-3-methylphenol |
| 5.0 |
| ug/L |
| Indeno(1,2,3-cd)pyrene |
| 5.0 |
| ug/L |
| 4-Chlorophenyl-phenylether |
| 5.0 |
| ug/L |
| Isophorone |
| 5.0 |
| ug/L |
| 4-Nitrophenol |
| 10 |
| ug/L |
| Naphthalene |
| 5.0 |
| ug/L |
| Acenaphthene |
| 5.0 |
| ug/L |
| Nitrobenzene |
| 5.0 |
| ug/L |
| Acenaphthylene |
| 5.0 |
| ug/L |
| N-Nitrosodimethylamine |
| 5.0 |
| ug/L |
| Anthracene |
| 5.0 |
| ug/L |
| N-Nitrosodi-n-propylamine |
| 5.0 |
| ug/L |
| Benzidine |
| 60 |
| ug/L |
| N-Nitrosodiphenylamine |
| 5.0 |
| ug/L |
| Benzo(a)pyrene |
| 5.0 |
| ug/L |
| Pentachlorophenol |
| 15 |
| ug/L |
| Benzo(b)fluoranthene |
| 5.0 |
| ug/L |
| Phenanthrene |
| 5.0 |
| ug/L |
| Benzo(g,h,i)perylene |
| 5.0 |
| ug/L |
| Phenol |
| 5.0 |
| ug/L |
| Benzo(k)fluoranthene |
| 5.0 |
| ug/L |
| Pyrene |
| 5.0 |
| ug/L |
OC Pesticides and PCBs (Aroclors) – EPA 608
Required
| Chlordane (technical) |
| 1.0 |
| ug/L |
| Endosulfan Sulfate |
| 0.05 |
| ug/L |
| Endrin Aldehyde |
| 0.05 |
| ug/L |
| Gamma BHC (Lindane) |
| 0.05 |
| ug/L |
| Heptachlor Epoxide |
| 0.05 |
| ug/L |
TCLP Organics
TCLP Acid Base/Neutrals
TCLP VOCs
| 1,4-Dichlorobenzene |
| 0.7 |
| mg/L |
| 1,1-Dichloroethene |
| 0.07 |
| mg/L |
| 2,4,5-Trichlorophenol |
| 40 |
| mg/L |
| 1,2-Dichloroethane |
| 0.05 |
| mg/L |
| 2,4,6-Trichlorophenol |
| 0.2 |
| mg/L |
| 2-Butanone (Methyl ethyl ketone) |
| 20 |
| mg/L |
| 2,4-Dinitrotoluene |
| 0.01 |
| mg/L |
| Carbon Tetrachloride |
| 0.05 |
| mg/L |
| 4-Methylphenol + 3-Methylphenol |
| 20 |
| mg/L |
| Hexachlorobenzene |
| 0.01 |
| mg/L |
| Hexachlorobutadiene |
| 0.05 |
| mg/L |
| Tetrachloroethene |
| 0.07 |
| mg/L |
| Hexachloroethane |
| 0.3 |
| mg/L |
| Trichloroethene |
| 0.05 |
| mg/L |
| Pentachlorophenol |
| 10 |
| mg/L |
TCLP Herbicides
TCLP Pesticides
| Gamma BHC - Lindane |
| 0.04 |
| mg/L |
| Heptachlor Epoxide |
| 0.0008 |
| mg/L |
GRO, DRO, ORO, and HEM
| GRO by 8015x or 8260x, mod- soil |
| 0.5 |
| mg/kg |
| DRO by 8015x- soil |
| 10 |
| mg/kg |
(C10-C28)
| GRO by 8015x or 8260x, mod- water |
| 0.04 |
| mg/L |
| DRO by 8015x- water |
| 0.04 |
| mg/L |
(C10-C28)
| ORO by 8015x or equivalent – soil |
| 50 |
| mg/kg |
(C28-C40)
| ORO by 8015x or equivalent – water |
| 1 |
| mg/L |
(C28-C40)
| HEM by 1664A- water |
| 5 |
| mg/L |
Explosives - EPA 8330x
WATER
SOIL
| Compound |
| Required LOQ (or LOD) |
| Units |
| Compound |
| Required LOQ (or LOD) |
| Units |
| 2,4,6-Trinitrotoluene |
| 0.2 |
| ug/L |
| 2,4,6-Trinitrotoluene |
| 0.1 |
| mg/kg |
| 2,4-Dinitrotoluene |
| 0.2 |
| ug/L |
| 2,4-Dinitrotoluene |
| 0.1 |
| mg/kg |
| 4-Amino-2,6-dinitrotoluene |
| 0.5 |
| ug/L |
| 4-Amino-2,6-dinitrotoluene |
| 0.1 |
| mg/kg |
| 2-Amino-4,6-dinitrotoluene |
| 0.5 |
| ug/L |
| 2-Amino-4,6-dinitrotoluene |
| 0.1 |
| mg/kg |
| 2,6-Dinitrotoluene |
| 0.2 |
| ug/L |
| 2,6-Dinitrotoluene |
| 0.1 |
| mg/kg |
| 1,3,5-Trinitrobenzene |
| 0.2 |
| ug/L |
| 1,3,5-Trinitrobenzene |
| 0.1 |
| mg/kg |
| 1,3-Dinitrobenzene |
| 0.2 |
| ug/L |
| 1,3-Dinitrobenzene |
| 0.1 |
| mg/kg |
LOD = limit of detection, as defined by DoD (DoD Quality System Manual, most recent version)
OC Pesticides - EPA 8081x
OC Pesticides - EPA 8081x
Water
Soil
| Compound Description |
| Required |
| Units |
| Compound Description |
| Required |
| Units |
LOQ
LOQ
| 1,2-Dibromo-3-chloropropane* |
| 0.1 |
| ug/L |
| 1,2-Dibromo-3-chloropropane* |
| 0.1 |
| mg/kg |
| alpha-HCH {alpha-BHC} |
| 0.02 |
| ug/L |
| alpha-HCH {alpha-BHC} |
| 0.01 |
| mg/kg |
| alpha-Chlordane |
| 0.02 |
| ug/L |
| alpha-Chlordane |
| 0.02 |
| mg/kg |
| beta-HCH {beta-BHC} |
| 0.02 |
| ug/L |
| beta-HCH {beta-BHC} |
| 0.01 |
| mg/kg |
| Chlordane, CAS 57-74-9 or Technical Chlordane,12789-03-6 |
| 0.1 |
| ug/L |
| Chlordane, CAS 57-74-9 or Technical Chlordane,12789-03-6 |
| 0.01 |
| mg/kg |
| Chlorobenzilate* |
| 0.2 |
| ug/L |
| Chlorobenzilate* |
| 0.1 |
| mg/kg |
| delta-HCH {delta-BHC} |
| 0.02 |
| ug/L |
| delta-HCH {delta-BHC} |
| 0.02 |
| mg/kg |
| Endosulfan sulfate |
| 0.05 |
| ug/L |
| Endosulfan sulfate |
| 0.02 |
| mg/kg |
| Endrin aldehyde |
| 0.03 |
| mg/kg |
| gamma-HCH {gamma-BHC, |
| 0.02 |
| ug/L |
| gamma-HCH {gamma-BHC, Lindane) |
| 0.005 |
| mg/kg |
| gamma-Chlordane |
| 0.02 |
| ug/L |
| gamma-Chlordane |
| 0.02 |
| mg/kg |
| Heptachlor epoxide |
| 0.05 |
| ug/L |
| Heptachlor epoxide |
| 0.02 |
| mg/kg |
| Hexachlorobenzene |
| 0.1 |
| ug/L |
| Hexachlorobenzene |
| 0.1 |
| mg/kg |
| Hexachlorocyclopentadiene* |
| 0.2 |
| ug/L |
| Hexachlorocyclopentadiene* |
| 0.1 |
| mg/kg |
PCBs- 8082x- Water
PCBs- 8082x- Soil
*not required to be on DoD ELAP scope Herbicides – EPA 8151A Water
Soil
| Compound Description |
| Required |
| Units |
| Compound Description |
| Required |
| Units |
LOQ
LOQ
| 2,4,5-TP {Silvex} |
| 0.5 |
| ug/L |
| 2,4,5-TP {Silvex} |
| 0.05 |
| mg/kg |
| 3,5-Dichlorobenzoic acid* |
| 0.5 |
| ug/L |
| 3,5-Dichlorobenzoic acid* |
| 0.05 |
| mg/kg |
| Pentachlorophenol |
| 0.05 |
| mg/kg |
| Pentachlorophenol |
| 0.5 |
| ug/L |
*not required to be on DoD ELAP scope PFAS – LCMSMS, Compliant with QSM 5.1 (or most current version), Table B-15
Water
| Compound Description |
| Required |
| Units |
LOQ
| N-ethyl perfluorooctanesulfonamidoacetic acid, NEtFOSAA |
| 10 |
| ng/L |
| N-methyl perfluorooctanesulfonamidoacetic acid, NMeFOSAA |
| 10 |
| ng/L |
| Perfluorobutanesulfonic acid, PFBS |
| 5 |
| ng/L |
| Perfluorodecanoic acid, PFDA |
| 5 |
| ng/L |
| Perfluorododecanoic acid, PFDoA |
| 5 |
| ng/L |
| Perfluoroheptanoic acid, PFHpA |
| 5 |
| ng/L |
| Perfluorohexanesulfonic acid, PFHxS |
| 5 |
| ng/L |
| Perfluorohexanoic acid, PFHxA |
| 5 |
| ng/L |
| Perfluorononanoic acid, PFNA |
| 5 |
| ng/L |
| Perfluorooctanesulfonic acid, PFOS |
| 5 |
| ng/L |
| Perfluorooctanoic acid, PFOA |
| 5 |
| ng/L |
| Perfluorotetradecanoic acid, PFTA |
| 5 |
| ng/L |
| Perfluorotridecanoic acid, PFTrDA |
| 5 |
| ng/L |
| Perfluoroundecanoic acid, PFUnA |
| 5 |
| ng/L |
METALS
TCLP for Analysis of TCLP Extract for Metals
| PARAMETER |
| METHOD |
| Limit of Quantitation (LOQ), mg/L |
ICPMS 6020 for Waters and Solids Water
| PARAMETER |
| METHOD |
| Maximum Limit of Quantitation (LOQ), mg/L |
SOIL/SEDIMENT/SLUDGE
| PARAMETER |
| METHOD |
| Maximum Limit of Quantitation (LOQ), mg/kg |
ICPMS 200.8 for Waters
WATERS
| PARAMETER |
| METHOD |
| Maximum Limit of Quantitation (LOQ), mg/L |
Mercury by EPA 200 and 7000 Series – Soils, Sediments, Sludges, and Waters
| PARAMETER |
| METHOD |
| Maximum Limit of Quantitation (LOQ) |
| UNIT |
EPA Method 6010 for Soils, Sediments, Sludges, Bulk, and Waters
SOILS/SEDIMENT/BULK
| PARAMETER |
| METHOD |
| Maximum Limit of Quantitation (LOQ), mg/kg |
EPA Method 6010 for Soils, Sediments, Sludges, Bulk, and Waters
| PARAMETER |
| METHOD |
| Maximum Limit of Quantitation (LOQ), mg/L |
EPA Method 200.7 for Water
| PARAMETER |
| METHOD |
| Maximum Limit of Quantitation (LOQ), mg/L |
| PARAMETER |
| METHOD |
| Maximum Limit of Quantitation (LOQ), mg/L |
| Alkalinity, Total (water) |
| SM 2320B or other 40CFR136 approved method |
| Please specify LOQ |
| Alkalinity, Bicarbonate (water) |
| SM 2320B or other applicable 40CFR136 approved method for total alkalinity |
| Please specify LOQ |
| Ammonia (water) |
| EPA 350.1 (rev 2.0), or SM 4500-NH3 F, G, or H |
| Please specify LOQ |
| BOD (water) |
| SM 5210B |
| Please specify LOQ |
Bromide (water)
| EPA 300.0 (rev 2.1), EPA 300.1 (rev 1.0), or other 40CFR136 approved ion chromatography method |
| Please specify LOQ |
Chloride (water)
| EPA 300.0 (rev 2.1) or EPA 300.1 (rev 1.0), or other 40CFR136 approved ion chromatography method |
| Please specify LOQ |
| Chromium VI (water) |
| EPA 218.6 or SM 3500 B or C |
| Please specify LOQ |
| Chromium VI (soil) |
| EPA 7000 series (modified) or other (specify method) |
| Please specify LOQ |
COD (water)
| EPA 410.4, SM 5220D, or other 40CFR136 approved method |
| Please specify LOQ |
Color (water)
| SM 2120B |
| Please specify LOQ |
| Conductivity (Specific Conductance) (water) |
| EPA 120.1 or SM 2510B |
| Please specify LOQ |
Cyanide, Total (water)
| EPA 335.4 or other 40CFR136 approved SM 4500-CN method combination |
| 0.005 mg/L |
| Cyanide, Amenable to Chlorination (water) |
| SM 4500-CN G |
| 0.005 mg/L |
Cyanide, Available (water)
| OIA-1677 or other 40CFR 136 approved method |
| 0.005 mg/L |
| Dissolved Organic Carbon (DOC) (water) |
| Any 40CFR136 approved method for total organic carbon |
| Please specify LOQ |
| Flashpoint (liquids) |
| EPA 1010A (ASTM D93) |
| Please specify LOQ |
Fluoride (water)
| EPA 300.0 (rev 2.1), EPA 300.1 (rev 1.0), or other 40CFR136 approved method |
| Please specify LOQ |
| Hardness (water) |
| SM 2340B (by calculation, using Ca and Mg concentrations determined by ICP) |
| Please specify LOQ |
| Ignitability/burn rate test (solids) |
| EPA 1030 |
| Please specify LOQ |
| PARAMETER |
| MATRIX |
| METHODOLOGY |
Moisture/Solids (percent) (soil, sludge, sediment)
| Laboratory SOP, gravimetric |
| Please specify LOQ |
Nitrate-Nitrite (water)
| EPA 353.2 or other 40CFR136 approved method |
| Please specify LOQ |
Nitrate only (water)
| EPA 300.0 (rev 2.1), EPA 300.1 (rev 1.0), or other 40CFR136 approved method |
| Please specify LOQ |
Nitrite only (water)
| EPA 300.0 (rev 2.1), EPA 300.1 (rev 1.0), or other 40CFR136 approved method |
| Please specify LOQ |
ortho-Phosphate (water)
| EPA 300.0 (rev 2.1), EPA 300.1 (rev 1.0), or other 40CFR136 approved method |
| Please specify LOQ |
| Paint Filter Liquids Test (solids, semisolids) |
| EPA 9095B |
| Please specify LOQ |
| Perchlorate* (water) |
| EPA 6850 or 6860 |
| Please specify LOQ |
| Perchlorate* (soil, sludge, sediment) |
| EPA 6850 or 6860 |
| Please specify LOQ |
pH (water)
| EPA SW846 9040x (specifiy version) |
| Please specify LOQ |
pH (soil, sludge, sediment)
| EPA SW846 9045x (specify version) |
| Please specify LOQ |
pH (water)
| EPA 150.2 or SM 4500-H+ B |
| Please specify LOQ |
Phosphorus, Total (water)
| Any 40CFR136 approved method or method combination that includes digestion |
| Please specify LOQ |
| Silica (water) |
| Any 40CFR136 approved method |
| Please specify LOQ |
Sulfate (water)
| EPA 300.0 (rev 2.1) or EPA 300.1 (rev 1.0), or other 40CFR136 approved ion chromatography method |
| Please specify LOQ |
Surfactants (MBAS) (water)
| SM 5540C |
| Please specify LOQ |
Total Kjeldahl nitrogen (TKN) (water)
| SM 4500-Norg B combined with any 40CFR136 approved method |
| Please specify LOQ |
Total Dissolved Solids (TDS) (water)
| SM 2540C |
| Please specify LOQ |
Total Organic Carbon (TOC) (water)
| Any 40CFR136 approved method |
| Please specify LOQ |
Total Organic Carbon (TOC)
(soil, sludge, sediment)
| Methods of Soil Analysis 29-3.5.2 or equivalent (submit method for APHC approval) |
| Please specify LOQ |
Total Suspended Solids (TSS) (water)
| SM 2540D |
| Please specify LOQ |
Turbidity (water)
| EPA 180.1 or SM 2130B |
| Please specify LOQ |
Department of the Army Medical Command