81029AttH7 - Technical Spec - Test Method References.docx
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- Attached to
- Laboratory Analytical Services for Fish TissuesBid Documents State and local contract opportunity
- Solicitation number
- RFP 25-81029
- Issued by
- Marion County, Indiana
About this file
This file is a technical specification document listing test method references for laboratory analytical services, issued by the Indiana Department of Environmental Management (IDEM) as part of RFP-25-81029. The document provides a comprehensive list of 59 standardized testing methods and reference materials that must be followed for analyzing fish tissues and sediment samples, including methods from the American Public Health Association, American Society for Testing and Materials, U.S. Environmental Protection Agency, and other authoritative sources.
The references cover a wide range of analytical procedures for detecting and measuring various substances including metals, organic compounds, PCBs, cyanide, mercury, arsenic, and PFAS in environmental samples. The document specifically highlights current versions of methods, with the most recent being the 2024 EPA Method 1633A for PFAS analysis and the 2023 Standard Methods for the Examination of Water and Wastewater (24th Edition). This technical specification appears to be a supporting document that establishes the required testing methodology standards for the broader laboratory services contract.
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RFP-25-81029
Attachment H7 Test Method References
1. American Public Health Association. 2023. Standard Methods for the Examination of Water and Wastewater, 24th Edition. Washington, DC. American Public Health Association, American Water Works Association, Water Environment Federation.
2. American Society for Testing and Materials, 1982, Standard Test Method for Particle-Size Analysis of Soils, D422-63(1998), Philadelphia, Pennsylvania.
3. American Society for Testing and Materials, 1982, Standard Test Methods for Specific Gravity of Soil Solids by Water Pycnometer, D854-00, Philadelphia, Pennsylvania.
4. American Society for Testing and Materials, 1982, Standard Test Methods for Total and Organic Carbon in Water Oxidation by Colourometric Detection, D4129-81, Philadelphia, Pennsylvania.
5. AOAC International, Official Methods of Analysis, 18th edition, 2006.
6. Contractor Supplied Methodology. Due the various specialized techniques utilized for these determinations, IDEM/OWM will evaluate each Contractor’s methodology.
7. Erickson, M.D. 1991, Analytical Chemistry of PCBs. Lewis Publ., Inc. Chelsea, MI.
8. IDEM. Office of Water Quality, Assessment Branch, 2023. WAPB Quality Assurance Project Plan (QAPP) for Indiana Surface Waters. Indianapolis, IN.
9. National Guidance for the Permitting, Monitoring, and Enforcement of Water Quality-Based Effluent Limitations Set Below Analytical Detection/Quantitation Levels. U.S. Environmental Protection Agency. March 22, 1994. Draft.
10. Office of the Federal Register. 1994 (or most recent revision). Code of Federal Regulations Title 40, Part 136. Washington, DC. Office of the Federal Register National Archives and Records Administration.
11. Randall, R.C., H. Lee, R.J. Ozretich, J.L. Lake and R.J. Pruell. 1991. Evaluation of Selected Lipid Methods for Normalizing Pollutant Bioaccumulation. Env. Tox and Chem. 10:1431-1436.
12. Schmacher, Brian, Plumb, Russell H., Jr., and Fox, Richard. 1994. Great Lakes Dredged Material Testing and Evaluation Manual, Appendix F: Methods for Chemical and Physical Analyses. Las Vegas, NV: Environmental Monitoring Systems Laboratory. U.S. Environmental Protection Agency: Great Lakes National Program Office and U.S. Army Corps of Engineers, North Central Division.
13. U.S. EPA. 1980. Prescribed Procedures for Measurement of Radioactivity in Drinking Water. U.S. Environmental Protection Agency, EMSL. Washington, DC: EPA/600/4/80/032.
14. U.S. EPA. 1983. Methods for the Chemical Analysis of Water and Wastes. U.S. Environmental Protection Agency. Washington, DC EPA/600/4-79-020.
15. U.S. EPA. 1986. Method 8310: Polynuclear Aromatic Hydrocarbons. U.S. Environmental Protection Agency. Washington, DC.
16. U.S. EPA. 1990. Methods for the Determination of Organic Compounds in Drinking Water, Supplement I. U.S. Environmental Protection Agency. Washington, DC. EPA/600/4-90/020.
17. U.S. EPA. 1991a. Draft Analytical Methods for Determination of Acid Volatile Sulfide (AVS) in Sediment. U.S. Environmental Protection Agency Office of Water Office of Science and Technology, Health and Ecological Criteria Division, Washington, D.C. EPA/821/R-91/100.
18. U.S. EPA. 1991b. Methods for the Determination of Metals in Environmental Samples. U.S. Environmental Protection Agency. Washington, DC. EPA/600/4-
19. U.S. EPA. 1992. Methods for the Determination of Organic Compounds in Drinking Water, Supplement II. U.S. Environmental Protection Agency. Washington, DC. EPA/600/R-92/129.
20. U.S. EPA. 1993. Methods for the Determination of Inorganic Substances in Environmental Samples. U.S. Environmental Protection Agency. Washington, DC. EPA/600/R-93/100.
21. U.S. EPA. 1994a. Methods for the Determination of Metals in Environmental Samples, Supplement I. U.S. Environmental Protection Agency. Washington, DC. EPA/600/4-94/111.
22. U.S. EPA. 1994b. Method 1613 Revision B: Tetra- Through Octa- Chlorinated Dioxins and Furans by Isotope Dilution HRGC/HRMS, U.S. Environmental Protection Agency. Washington, DC. EPA/821/B-94/005.
23. U.S. EPA. 1994c. Technical Notes on Drinking Water Methods. U.S Environmental Protection Agency, Office of Research and Development. Washington, DC. EPA/600/R-94/173
24. U.S. EPA. 1994d. Test Methods for Evaluating Solid Waste Physical/Chemical Methods, (SW-846) Revision II, Third Edition. U.S. Environmental Protection Agency. Washington, DC.
25. U.S. EPA. 1994e. Method 7474: Mercury in Sediments and Tissue Samples by Atomic Fluorescence Spectrometry. U.S. Environmental Protection Agency, Office of Water. Washington, DC.
26. U.S. EPA. 1994f. Method 7742: Selenium (Atomic Absorption, Borohydride Reduction). U.S. Environmental Protection Agency, Office of Water. Washington, DC.
27. U.S. EPA. 1995. Methods for the Determination of Organic Compounds in Drinking Water, Supplement III. U.S. Environmental Protection Agency. Washington, DC. EPA/600/R-95/131.
28. U.S. EPA. 1996a. Method 1636: Determination of Hexavalent Chromium by Ion Chromatography. U.S. Environmental Protection Agency, Office of Water Engineering and Analysis Division. Washington, DC. EPA/821/R-96/003.
29. U.S. EPA. 1996b. Method 1637: Determination of Trace Elements in Ambient Waters by Chelation Preconcentration with Graphite Furnace Atomic Absorption. U.S. Environmental Protection Agency. Office of Water. Washington, DC. EPA/821/R-96/004.
30. U.S. EPA. 1996c. Method 1638: Determination of Trace Elements in Ambient Waters by Inductively Coupled Plasma-Mass Spectrometry. U.S. Environmental Protection Agency. Office of Water. Washington, DC. EPA/821/R-96/005.
31. U.S. EPA. 1996d. Method 1639: Determination of Trace Elements in Ambient Waters by Stabilized Temperature Graphite Furnace Atomic Absorption. U.S. Environmental Protection Agency. Office of Water. Washington, DC. EPA/821/R-96/006.
32. U.S. EPA. 1996e. Method 3540C Revision 3: Soxhlet Extraction. U.S. Environmental Protection Agency. Office of Water. Washington, DC.
33. U.S. EPA. 1996f. Method 9014 Revision 0: Titrimetric and Manual Spectrophotometric Determinative. U.S. Environmental Protection Agency. Office of Water. Washington, DC.
34. U.S. EPA. 1996g. Method 1640: Determination of Trace Elements in Ambient Waters by On-Line Chelation Preconcentration and Inductively Coupled Plasma-Mass Spectrometry. U.S. Environmental Protection Agency. Office of Water. Washington, DC. EPA/821/R-96/007.
35. U.S. EPA. 1998. Method 1632 Rev A: Chemical Speciation of Arsenic in Water and Tissue by Hydride Generation Quartz Furnace Atomic Absorption SpectrometryU.S. Environmental Protection Agency. Office of Water Engineering and Analysis Division. Washington, DC.
36. U.S. EPA. 1999a. Method OIA-1678: Total Cyanide Determination. U.S. Environmental Protection Agency. Office of Water Engineering and Analysis Division. Washington, DC.
37. U.S. EPA. 1999b. Method 1664, Revision A: N-Hexane Extractable Material (HEM; Oil and Grease) and Silica Get Treated N_Hexane Extractable Material (SGT-HEM; Non-polar Material) by Extraction and Gravimetry. U.S. Environmental Protection Agency. Office of Water Engineering and Analysis Division. Washington, DC. EPA/821/R-94/004b.
38. U.S. EPA. 2000a. Method OIA-1677: Available Cyanide by Flow Injection, Ligand Exchange, and Amperometry. U.S. Environmental Protection Agency. Office of Water Engineering and Analysis Division. Washington, DC. EPA/821/R-99/013.
39. U.S. EPA. 2000b. Method 1625, Revision C: Semivolatile Organic Compounds by Isotope Dilution GC/MS. Washington, DC: U.S. Environmental Protection Agency, Office of Water. NEMI. Washington, DC.
40. U.S. EPA. 2001a. Method 1630, Methyl Mercury in Water by Distillation, Aqueous Ethylation, Purge and Trap, and CVAFS. U.S. Environmental Protection Agency. Office of Science and Technology. Engineering and Analysis Division. Washington, DC. DRAFT EPA 821/R-01/020
41. U.S. EPA. 2001b. Appendix to Method 1631. Total Mercury in Tissue, Sludge, Sediment, and Soil by Acid Digestion and BrCl Oxidation. U.S. Environmental Protection Agency. Office of Water Engineering and Analysis Division. Washington, DC. EPA 821/R-01/013.
42. U.S. EPA. 2002a. Method 1631. Revision E: Mercury in Water by Oxidation, Purge and Trap, and Cold Vapor Atomic Fluorescence Spectrometry. U.S. Environmental Protection Agency. Office of Water Engineering and Analysis Division. Washington, DC. EPA 821/R-02/019.
43. U.S. EPA. 2002b. Methods for the Determination of Total Organic Carbon (Toc) In Soils and Sediments. U.S. Environmental Protection Agency, Environmental Sciences Division. Exposure Research Laboratory, Las Vegas, NV.
44. U.S. EPA. 2003a. Method 1614 DRAFT: Brominated Diphenyl Ethers in Water, Soil, Sediment, and Tissue by HRGC/HRMS. U.S. Environmental Protection Agency. Washington, DC.
45. U.S. EPA. 2003b. Method 8323 Revision 0: Determination of Organotins by Micro-Liquid Chromatography- Electrospray Ion Trap Mass Spectrometry. U.S. Environmental Protection Agency. Washington, DC.
46. U.S. EPA. 2004a. Method 9012B Revision 2: Total and Amenable Cyanide (Automated Colorimetric, With Off-Line Distillation). U.S. Environmental Protection Agency. Washington, DC
47. U.S. EPA. 2004b. Method 9060: Total Organic Carbon. U.S. Environmental Protection Agency. Washington, DC.
48. U.S. EPA. 2006. Method 8260 Revision C: Volatile Organic Compounds by Gas Chromatography/Mass Spectrometry (GC/MS). U.S. Environmental Protection Agency. Washington, DC:
49. U.S. EPA. 2007a. Method 6020A, Inductively Coupled Plasma-Mass Spectrometry (ICP-MS), Revision 1. Washington, DC: U.S. Environmental Protection Agency, Office of Water. Washington, DC.
50. U.S. EPA. 2007b. Method 7471, Revision B: Mercury in Solid and Semisolid Waste (Manual Cold-Vapor Technique). Environmental Protection Agency, Office of Water. Washington, DC.
51. U.S. EPA. 2007c. Method 8081B Revision 2: Organochlorine Pesticides by Gas Chromatography. U.S. Environmental Protection Agency. Washington, DC:
52. U.S. EPA. 2007d. Method 8082A Revision 1. Polychlorinated Biphenyls (PCBs) by Gas Chromatography. U.S. Environmental Protection Agency. Washington, DC.
53. U.S. EPA. 2007e. Method 8270D Revision D: Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS). U.S. Environmental Protection Agency. Washington, DC.
54. U.S. EPA. 2007f. Method 7473 Revision 0: Mercury in Solids and Solutions by Thermal Decomposition, Amalgamation, and Atomic Absorption Spectrophotometry. U.S. Environmental Protection Agency. Washington, DC.
55. U.S. EPA. 2007g. Method 8141B Revision 2: Organophosphorus Compounds By Gas Chromotography. U.S. Environmental Protection Agency. Washington, DC.
56. U.S. EPA. 2008. Method 1668B, Revision B: Chlorinated Biphenyls Congeners in Water, Soil, Sediment, and Tissue by HRGC/HRMS. Washington, DC: U.S. Environmental Protection Agency, Office of Water. Washington, DC. EPA/821/R-08/020.
57. U.S. EPA. 2024. Method 1633A, Analysis of Per- and Polyfluoroalkyl Substances (PFAS) in Aqueous, Solids, Biosolids, and Tissue Samples by LC-MS/MS. Washington, DC: U.S. Environmental Protection Agency, Office of Water. Washington, DC. EPA 820-R-24-001.
58. USGS. 1978, National Handbook of Recommended Methods for Water Data Acquisition, Chapter 3, Sediment. (June 1978 Revision). U.S. Geological Survey.
59. WI ESS. 2010. ESS-ORG Method 1480: Analysis of Perfluorinated Compounds in Fish Tissue by HPLC-MS/MS. Environmental Sciences Section, Organic Chemistry Unit, Wisconsin State Lab of Hygiene, Madison, WI.
RFP-25-81029
Technical Specifications H7
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