INFORMATION_ONLY_Profile_Analysis_Data.pdf

(Check all that apply)OTHER CHARACTERISTICS

HAZARDOUS WASTE PROFILE SHEET

PART II

PHYSICAL STATE SOLID LIQUID SEMI-SOLID GAS OTHER

IGNITABLE (D001)

WASTEWATERTREATMENT GROUP NON-WASTEWATER

FLASH POINT

CORROSIVE (D002)

PH

TOXICITY CHARACTERISTIC(D004 CORRODES STEEL

HIGH TOC (>10%) LOW TOC (<10%)

WATER REACTIVE CYANIDE REACT SULFIDE REACTIVE

REACTIVE (D003)

3. CHEMICAL / MATERIAL CONSTITUENTS (List all components and contaminants, including PCB's and any applicable F-Listed and Underlying Hazardous Constituents)

X

X

X

1. MATERIAL CHARACTERIZATION (Optional - Unless otherwise indicated)

TOTAL SOLIDS LAYERINGASH CONTENT MULTILAYERED BILAYERED SINGLE PHASE0.00 0.00

COLOR

A. GENERAL INFORMATION

1. GENERATOR'S NAME

WASTE PROFILE NO.

2. FACILITY ADDRESS

5. GENERATOR STATE ID

4. GENERATOR USEPA ID

3. ZIP CODE

6. TECHNICAL CONTACT 7. TITLE 8.PHONE

1. NAME OF WASTE

2A. EPA WASTE CODE(S)

4. PROJECTED ANNUAL VOL.

6. IS THIS WASTE A DIOXIN LISTED WASTE AS DEFINED IN

5. MODE OF COLLECTION

HAS AN EXEMPTION BEEN GRANTED?

7. IS THIS WASTE RESTRICTED FROM LAND DISPOSAL?

DOES THE WASTE MEET APPLICABLE TREATMENT STANDARDS ALREADY?

PART I

YES NO

YES NO

YES NO

YES NO

ANNISTON ARMY DEPOT

171028

7 FRANKFORD AVENUE, , Anniston, AL 36201

RANDY BRIGHT Chief - Industrial Support Div 256-235-6350

BLAST MEDIA IN ROLL-OFF BOXES FROM DEPAINTING

OPERATIONS

AL

AL3210020027

X

X

X

X

B. WASTE INFORMATION

DEMIL CODE A B C D E

F G P Q

3. PROCESS GENERATING WASTE G06 Painting and coating

(If Yes, Enter Reference Standards in Part II, Block 6)

2B. STATE WASTE CODE(S)

BTU / LB 0DENSITY

40 CFR 261.31?

(40 CFR 268)

D006

D007

D008

START DATE: END DATE:7/31/2017 1/31/2020

WASTE TYPE: HW | Hazardous Waste

WASTE STREAM: 15 | BLASTING MEDIA

OTHER COMMENTS:

2. RCRA CHARACTERISTICS

Page: 1 of 3FOR OFFICIAL USE ONLYReport Date: 11-20-2017

MATERIAL CONSTITUENTS

METHOD OF SHIPMENT

ADDITIONAL DESCRIPTION

U.N or N.A. NO.HAZARD CLASS

PROPER SHIPPING NAME

BULK DRUM OTHER

9 3077

4. SHIPPING INFORMATION

RANGE TOTAL MUST EQUAL AT LEAST 100%

DOT HAZARDOUS MATERIAL? YES NOX If "NO" skip to block 5)

PACKING GROUP III

EMERGENCY RESPONSE GUIDE EDITION

DOT REPORTABLE QTY (RQ) LBS

5.SPECIAL HANDLING INFORMATION

USE PERSONAL PROTECTIVE CLOTHING AND EQUIPMENT

6. GENERATOR CERTIFICATION X CHEMICAL ANALYSIS (ATTACH TEST RESULTS) USER KNOWLEDGE (ATTACH SUPPORTING DOCUMENTS)

(Explain how and why these documents comply with RCRA requirements)

CERTIFICATION

CERTIFY THAT ALL INFORMATION SUBMITTED IN THIS AND ALL ATTACHED DOCUMENTS

IS TO THE BEST OF MY KNOWLEDGE AN ACCURATE REPRESENTATION OF THE WASTE TURNED IN. ALL KNOWN OR SUSPECTED HAZARDS HAVE BEEN DISCLOSED.

HEREBYI,

2016 EMERGENCY RESPONSE NO 171

HAZARDOUS WASTE SOLID, N.O.S.

(REF. 49 CFR 172.101, Appendix A)

CAS #

COMPONENT

Be as descriptive as possible. Chemical names, such generic descriptions, e.g. 'sludge', paint solids 'water' etc. are acceptable).

CONCENTRATION RANGE

7439-92-1 LEAD 5 PPM 0.000000 -

0.000000

7440-02-0 NICKEL 1.1 PPM 0.000000 -

0.000000

7440-36-0 ANTIMONY 0 % 0.000000 -

0.000000

7440-43-9 CADMIUM 1 PPM 0.000000 -

0.000000

7440-47-3 CHROMIUM 5 PPM 0.000000 -

0.000000

7440-66-6 ZINC 15 PPM 0.000000 -

0.000000

Additional Description:

Additional RCRA Requirements (MSDS Codes):

Constituent Name (e.g. rags and wipes) # Concentration (e.g. 80%) # Range Percent #

BLASTING MEDIA FROM MECHANICAL DEPAINTING O 99-100% 100

CONTRACT NUMBER SP450015D0011 CLIN TX16

DESCRIPTION METALS-BEARING SOLIDS/SLUDGES/SOME FREE LIQUIDS, LOW (<1%) TCLP METALS, TOTAL CR+6 <100 PPM, TOTAL HG <260 PPM, CHARACTERISTIC. PHYSICAL STATE: VARIOUS. PERMISSIBLE WASTE CODES: D004-D011*BLAST MEDIA FROM

Page: 2 of 3FOR OFFICIAL USE ONLYReport Date: 11-20-2017

Signature of Generator's Representative

DATE:

Page: 3 of 3FOR OFFICIAL USE ONLYReport Date: 11-20-2017

Analytical Report

L7E0215

Project

Blast Media from Roo-off Boxes

Project Number

B17129-1

May 19, 2017

Anniston Army Depot

7 Frankford Avenue

Anniston, Alabama 36201

Minority Women Business Enterprise

Small Disadvantaged Business Enterprise

1412 Tech Blvd Phone #: 813-620-2000

Website: www.ftsanalytical.comTampa, FL 33619

Minority Women Business Enterprise

Small Disadvantaged Business Enterprise

May 19, 2017

Anniston Army Depot

7 Frankford Avenue

Nathan L Corburn

RE: Blast Media from Roo-off Boxes

We are reporting the results of the analyses performed on the samples recieved on 5/16/2017 under the project name referenced above and identified as the lab Work Order L7E0215. All results being reported under this Report apply to the samples analyzed and properly identified with a Laboratory ID number.

Subcontracted analyses are identified in this report with either the NELAC certification number of the subcontracted lab, or the complete subcontracted report attached to this report.

Unless otherwise noted in a Case Narrative, all data reported in this Analytical Report are in compliance with

NELAC standards. The uncertainty of measurement associated with the results of analysis reported is available upon request. Should insufficient sample be provided to the laboratory to meet the method and

NELAC Matrix Duplicate and Matrix Spike requirements, then the data will be analyzed, evaluated and reporting using all other available quality control methods.

The validity and integrity of this report will remain intact as long as it is accompanied by this letter and reproduced in full, unless written approval is granted by FTS Analytical Laboratories. This report will be filed for at least 5 years in our archives after which time it will be destroyed without further notice, unless otherwise agreed upon. The samples received, and described as recorded in Work Order L7E0215 will be filed for 60 days, and after that time they will be properly disposed without further notice, unless otherwise agreed upon. We reserve the right to return to you any unused samples, extracts, or solutions if we consider so necessary (e.g., samples identified as hazardous waste, sample sizes exceeding standard practices, controlled/regulated substances, etc.)

We thank you for selecting FTS Analytical to serve your analytical needs. If you have any questions concerning this report, please do not hesitate to contact us at any time. We will be happy to help.

Anniston, Alabama 36201

Sincerely, J. Derek Rounsley For Derek Rounsley

Project Manager

Project:

Project Number:

Project Manager:

Reported:

Anniston Army Depot

7 Frankford Avenue

Blast Media from Roo-off Boxes

B17129-1

Nathan L Corburn 5/19/17 16:30

MWBE SDBE

NELAC DoD Accredited

Anniston, Alabama 36201

Samples in this Report

Sample Lab ID Matrix Date Sampled Date Received

86837/DPBM4330-RB SolidL7E0215-01 16-May-2017 11:3209-May-2017 13:55

86610/DPBM114-RB SolidL7E0215-02 16-May-2017 11:3209-May-2017 14:30

86612/DPBM409W-RB SolidL7E0215-03 16-May-2017 11:3209-May-2017 14:45

86535/DPBM409E-RB SolidL7E0215-04 16-May-2017 11:3209-May-2017 14:50

The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.

No duplication of this report is allowed, except in its entirety. Page 3 of 43

Project Manager:

Reported:

Anniston Army Depot

7 Frankford Avenue

Blast Media from Roo-off Boxes

B17129-1

Nathan L Corburn 5/19/17 16:30

MWBE SDBE

NELAC DoD Accredited

Anniston, Alabama 36201

Hits Summary (Not Including Subcontracted Analysis)

Sample: 86837/DPBM4330-RB

MethodCAS #Date AnalyzedDilUnitsMDLResult PQLQual Analyte

Lab ID: L7E0215-01

250 ug/L50.0 1556 5/17/17 14:14 7440-47-3 EPA 6010CChromium

250 ug/L50.0 11090 5/17/17 14:14 7440-02-0 EPA 6010CNickel

250 ug/L50.0 14400 5/17/17 14:14 7440-66-6 EPA 6010CZinc

Sample: 86610/DPBM114-RB

MethodCAS #Date AnalyzedDilUnitsMDLResult PQLQual Analyte

Lab ID: L7E0215-02

250 ug/L50.0 1834 5/17/17 14:16 7440-39-3 EPA 6010CBarium

250 ug/L50.0 1328 5/17/17 14:16 7440-43-9 EPA 6010CCadmium

250 ug/L50.0 1506 5/17/17 14:16 7440-02-0 EPA 6010CNickel

Sample: 86612/DPBM409W-RB

MethodCAS #Date AnalyzedDilUnitsMDLResult PQLQual Analyte

Lab ID: L7E0215-03

250 ug/L50.0 1339 5/17/17 14:19 7440-47-3 EPA 6010CChromium

250 ug/L50.0 1482 5/17/17 14:19 7440-02-0 EPA 6010CNickel

250 ug/L50.0 114900 5/17/17 14:19 7440-66-6 EPA 6010CZinc

Sample: 86535/DPBM409E-RB

MethodCAS #Date AnalyzedDilUnitsMDLResult PQLQual Analyte

Lab ID: L7E0215-04

250 ug/L50.0 1395 5/17/17 14:21 7440-39-3 EPA 6010CBarium

250 ug/L50.0 1365 5/17/17 14:21 7440-43-9 EPA 6010CCadmium

250 ug/L50.0 1455 5/17/17 14:21 7440-47-3 EPA 6010CChromium

250 ug/L50.0 17270 5/17/17 14:21 7440-66-6 EPA 6010CZinc

The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.

No duplication of this report is allowed, except in its entirety. Page 4 of 43

Project Manager:

Reported:

Anniston Army Depot

7 Frankford Avenue

Blast Media from Roo-off Boxes

B17129-1

Nathan L Corburn 5/19/17 16:30

MWBE SDBE

NELAC DoD Accredited

Anniston, Alabama 36201

Sample Results

ResultAnalyte MDL Date AnalyzedQual Units

Lab Sample ID: L7E0215-01 (Solid)

Client Sample ID: 86837/DPBM4330-RB

PQL Dil Date Prepared

Sampled:5/9/17 13:55

CAS #

TCLP Mercury Analysis by Method 7470A

0.200 ug/L0.0700 10.0700 U 5/18/17 14:465/18/17 14:45 7439-97-6Mercury

TCLP Metal Analysis by Method 6010C

250 ug/L50.0 150.0 U 5/17/17 14:145/17/17 9:30 7440-36-0Antimony

250 ug/L50.0 150.0 U 5/17/17 14:145/17/17 9:30 7440-41-7Beryllium

250 ug/L50.0 150.0 U 5/17/17 14:145/17/17 9:30 7440-38-2Arsenic

250 ug/L50.0 150.0 U 5/17/17 14:145/17/17 9:30 7440-39-3Barium

250 ug/L50.0 150.0 U 5/17/17 14:145/17/17 9:30 7440-43-9Cadmium

250 ug/L50.0 1556 5/17/17 14:145/17/17 9:30 7440-47-3Chromium

250 ug/L50.0 11090 5/17/17 14:145/17/17 9:30 7440-02-0Nickel

250 ug/L50.0 150.0 U 5/17/17 14:145/17/17 9:30 7440-28-0Thallium

250 ug/L50.0 150.0 U 5/17/17 14:145/17/17 9:30 7439-92-1Lead

250 ug/L50.0 150.0 U 5/17/17 14:145/17/17 9:30 7440-62-2Vanadium

250 ug/L50.0 14400 5/17/17 14:145/17/17 9:30 7440-66-6Zinc

250 ug/L50.0 150.0 U 5/17/17 14:145/17/17 9:30 7782-49-2Selenium

250 ug/L50.0 150.0 U 5/17/17 14:145/17/17 9:30 7440-22-4Silver

The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.

No duplication of this report is allowed, except in its entirety. Page 5 of 43

Project Manager:

Reported:

Anniston Army Depot

7 Frankford Avenue

Blast Media from Roo-off Boxes

B17129-1

Nathan L Corburn 5/19/17 16:30

MWBE SDBE

NELAC DoD Accredited

Anniston, Alabama 36201

Sample Results

(Continued)

ResultAnalyte MDL Date AnalyzedQual Units

Lab Sample ID: L7E0215-02 (Solid)

Client Sample ID: 86610/DPBM114-RB

PQL Dil Date Prepared

Sampled:5/9/17 14:30

CAS #

TCLP Mercury Analysis by Method 7470A

0.200 ug/L0.0700 10.0700 U 5/18/17 14:465/18/17 14:45 7439-97-6Mercury

TCLP Metal Analysis by Method 6010C

250 ug/L50.0 150.0 U 5/17/17 14:165/17/17 9:30 7440-36-0Antimony

250 ug/L50.0 150.0 U 5/17/17 14:165/17/17 9:30 7440-41-7Beryllium

250 ug/L50.0 150.0 U 5/17/17 14:165/17/17 9:30 7440-38-2Arsenic

250 ug/L50.0 1834 5/17/17 14:165/17/17 9:30 7440-39-3Barium

250 ug/L50.0 1328 5/17/17 14:165/17/17 9:30 7440-43-9Cadmium

250 ug/L50.0 150.0 U 5/17/17 14:165/17/17 9:30 7440-47-3Chromium

250 ug/L50.0 1506 5/17/17 14:165/17/17 9:30 7440-02-0Nickel

250 ug/L50.0 150.0 U 5/17/17 14:165/17/17 9:30 7440-28-0Thallium

250 ug/L50.0 150.0 U 5/17/17 14:165/17/17 9:30 7439-92-1Lead

250 ug/L50.0 150.0 U 5/17/17 14:165/17/17 9:30 7440-62-2Vanadium

250 ug/L50.0 150.0 U 5/17/17 14:165/17/17 9:30 7440-66-6Zinc

250 ug/L50.0 150.0 U 5/17/17 14:165/17/17 9:30 7782-49-2Selenium

250 ug/L50.0 150.0 U 5/17/17 14:165/17/17 9:30 7440-22-4Silver

The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.

No duplication of this report is allowed, except in its entirety. Page 6 of 43

Project Manager:

Reported:

Anniston Army Depot

7 Frankford Avenue

Blast Media from Roo-off Boxes

B17129-1

Nathan L Corburn 5/19/17 16:30

MWBE SDBE

NELAC DoD Accredited

Anniston, Alabama 36201

Sample Results

(Continued)

ResultAnalyte MDL Date AnalyzedQual Units

Lab Sample ID: L7E0215-03 (Solid)

Client Sample ID: 86612/DPBM409W-RB

PQL Dil Date Prepared

Sampled:5/9/17 14:45

CAS #

TCLP Mercury Analysis by Method 7470A

0.200 ug/L0.0700 10.0700 U 5/18/17 14:465/18/17 14:45 7439-97-6Mercury

TCLP Metal Analysis by Method 6010C

250 ug/L50.0 150.0 U 5/17/17 14:195/17/17 9:30 7440-36-0Antimony

250 ug/L50.0 150.0 U 5/17/17 14:195/17/17 9:30 7440-41-7Beryllium

250 ug/L50.0 150.0 U 5/17/17 14:195/17/17 9:30 7440-38-2Arsenic

250 ug/L50.0 150.0 U 5/17/17 14:195/17/17 9:30 7440-39-3Barium

250 ug/L50.0 150.0 U 5/17/17 14:195/17/17 9:30 7440-43-9Cadmium

250 ug/L50.0 1339 5/17/17 14:195/17/17 9:30 7440-47-3Chromium

250 ug/L50.0 1482 5/17/17 14:195/17/17 9:30 7440-02-0Nickel

250 ug/L50.0 150.0 U 5/17/17 14:195/17/17 9:30 7440-28-0Thallium

250 ug/L50.0 150.0 U 5/17/17 14:195/17/17 9:30 7439-92-1Lead

250 ug/L50.0 150.0 U 5/17/17 14:195/17/17 9:30 7440-62-2Vanadium

250 ug/L50.0 114900 5/17/17 14:195/17/17 9:30 7440-66-6Zinc

250 ug/L50.0 150.0 U 5/17/17 14:195/17/17 9:30 7782-49-2Selenium

250 ug/L50.0 150.0 U 5/17/17 14:195/17/17 9:30 7440-22-4Silver

The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.

No duplication of this report is allowed, except in its entirety. Page 7 of 43

Project Manager:

Reported:

Anniston Army Depot

7 Frankford Avenue

Blast Media from Roo-off Boxes

B17129-1

Nathan L Corburn 5/19/17 16:30

MWBE SDBE

NELAC DoD Accredited

Anniston, Alabama 36201

Sample Results

(Continued)

ResultAnalyte MDL Date AnalyzedQual Units

Lab Sample ID: L7E0215-04 (Solid)

Client Sample ID: 86535/DPBM409E-RB

PQL Dil Date Prepared

Sampled:5/9/17 14:50

CAS #

TCLP Mercury Analysis by Method 7470A

0.200 ug/L0.0700 10.0700 U 5/18/17 14:465/18/17 14:45 7439-97-6Mercury

TCLP Metal Analysis by Method 6010C

250 ug/L50.0 150.0 U 5/17/17 14:215/17/17 9:30 7440-36-0Antimony

250 ug/L50.0 150.0 U 5/17/17 14:215/17/17 9:30 7440-41-7Beryllium

250 ug/L50.0 150.0 U 5/17/17 14:215/17/17 9:30 7440-38-2Arsenic

250 ug/L50.0 1395 5/17/17 14:215/17/17 9:30 7440-39-3Barium

250 ug/L50.0 1365 5/17/17 14:215/17/17 9:30 7440-43-9Cadmium

250 ug/L50.0 1455 5/17/17 14:215/17/17 9:30 7440-47-3Chromium

250 ug/L50.0 150.0 U 5/17/17 14:215/17/17 9:30 7440-02-0Nickel

250 ug/L50.0 150.0 U 5/17/17 14:215/17/17 9:30 7440-28-0Thallium

250 ug/L50.0 150.0 U 5/17/17 14:215/17/17 9:30 7439-92-1Lead

250 ug/L50.0 150.0 U 5/17/17 14:215/17/17 9:30 7440-62-2Vanadium

250 ug/L50.0 17270 5/17/17 14:215/17/17 9:30 7440-66-6Zinc

250 ug/L50.0 150.0 U 5/17/17 14:215/17/17 9:30 7782-49-2Selenium

250 ug/L50.0 150.0 U 5/17/17 14:215/17/17 9:30 7440-22-4Silver

The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.

No duplication of this report is allowed, except in its entirety. Page 8 of 43

Project Manager:

Reported:

Anniston Army Depot

7 Frankford Avenue

Blast Media from Roo-off Boxes

B17129-1

Nathan L Corburn 5/19/17 16:30

MWBE SDBE

NELAC DoD Accredited

Anniston, Alabama 36201

Result PQL Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD

LimitQual Analyte

Quality Control

Total Metal Analysis by Method 6010C

MDL

Batch: B7E0279

Prepared & Analyzed: 5/16/2017Blank (B7E0279-BLK1)

0.500 mg/Kg wet0.0200 U, 0.0200Cadmium

Prepared & Analyzed: 5/16/2017LCS (B7E0279-BS1)

0.500 100 80-120114mg/Kg wet114 0.0200Cadmium

Prepared & Analyzed: 5/16/2017LCS Dup (B7E0279-BSD1)

0.500 100 2080-120116 1mg/Kg wet116 0.0200Cadmium

Prepared & Analyzed: 5/16/2017Source: L7E0215-01Duplicate (B7E0279-DUP1)

0.501 12.5 3010mg/Kg dry11.3 0.0200Cadmium

Prepared & Analyzed: 5/16/2017Source: L7E0215-01Matrix Spike (B7E0279-MS1)

0.501 100 12.5 80-120107mg/Kg dry120 0.0200Cadmium

Prepared & Analyzed: 5/16/2017Source: L7E0215-01Matrix Spike Dup (B7E0279-MSD1)

0.496 99.2 12.5 2080-120106 2mg/Kg dry117 0.0198Cadmium

The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.

No duplication of this report is allowed, except in its entirety. Page 9 of 43

Project Manager:

Reported:

Anniston Army Depot

7 Frankford Avenue

Blast Media from Roo-off Boxes

B17129-1

Nathan L Corburn 5/19/17 16:30

MWBE SDBE

NELAC DoD Accredited

Anniston, Alabama 36201

Result PQL Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD

LimitQual Analyte

Quality Control (Continued)

Total Metal Analysis by Method 6010C

MDL

Batch: B7E0279

Prepared & Analyzed: 5/16/2017Blank (B7E0279-BLK1)

5.00 mg/Kg wet0.398 U, 0.398Thallium

Prepared & Analyzed: 5/16/2017LCS (B7E0279-BS1)

5.00 100 80-120116mg/Kg wet116 0.398Thallium

Prepared & Analyzed: 5/16/2017LCS Dup (B7E0279-BSD1)

5.00 100 2080-120117 1mg/Kg wet117 0.398Thallium

Prepared & Analyzed: 5/16/2017Source: L7E0215-01Duplicate (B7E0279-DUP1)

5.01 ND 30mg/Kg dry0.399 U, 0.399Thallium

Prepared & Analyzed: 5/16/2017Source: L7E0215-01Matrix Spike (B7E0279-MS1)

5.01 100 ND 80-120100mg/Kg dry100 0.399Thallium

Prepared & Analyzed: 5/16/2017Source: L7E0215-01Matrix Spike Dup (B7E0279-MSD1)

4.96 99.2 ND 2080-120102 1mg/Kg dry101 0.395Thallium

The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.

No duplication of this report is allowed, except in its entirety. Page 10 of 43

Project Manager:

Reported:

Anniston Army Depot

7 Frankford Avenue

Blast Media from Roo-off Boxes

B17129-1

Nathan L Corburn 5/19/17 16:30

MWBE SDBE

NELAC DoD Accredited

Anniston, Alabama 36201

Result PQL Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD

LimitQual Analyte

Quality Control (Continued)

Total Metal Analysis by Method 6010C

MDL

Batch: B7E0279

Prepared & Analyzed: 5/16/2017Blank (B7E0279-BLK1)

5.00 mg/Kg wet0.477 U, 0.477Antimony

Prepared & Analyzed: 5/16/2017LCS (B7E0279-BS1)

5.00 100 80-120114mg/Kg wet114 0.477Antimony

Prepared & Analyzed: 5/16/2017LCS Dup (B7E0279-BSD1)

5.00 100 2080-120117 3mg/Kg wet117 0.477Antimony

Prepared & Analyzed: 5/16/2017Source: L7E0215-01Duplicate (B7E0279-DUP1)

5.01 1.03 307mg/Kg dry0.966 0.478Antimony

Prepared & Analyzed: 5/16/2017Source: L7E0215-01Matrix Spike (B7E0279-MS1)

5.01 100 1.03 80-12095mg/Kg dry95.8 0.478Antimony

Prepared & Analyzed: 5/16/2017Source: L7E0215-01Matrix Spike Dup (B7E0279-MSD1)

4.96 99.2 1.03 2080-12095 0.4mg/Kg dry95.5 0.473Antimony

The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.

No duplication of this report is allowed, except in its entirety. Page 11 of 43

Project Manager:

Reported:

Anniston Army Depot

7 Frankford Avenue

Blast Media from Roo-off Boxes

B17129-1

Nathan L Corburn 5/19/17 16:30

MWBE SDBE

NELAC DoD Accredited

Anniston, Alabama 36201

Result PQL Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD

LimitQual Analyte

Quality Control (Continued)

Total Metal Analysis by Method 6010C

MDL

Batch: B7E0279

Prepared & Analyzed: 5/16/2017Blank (B7E0279-BLK1)

5.00 mg/Kg wet0.858 U, 0.858Arsenic

Prepared & Analyzed: 5/16/2017LCS (B7E0279-BS1)

5.00 100 80-120118mg/Kg wet118 0.858Arsenic

Prepared & Analyzed: 5/16/2017LCS Dup (B7E0279-BSD1)

5.00 100 2080-120120 2mg/Kg wet120 0.858Arsenic

Prepared & Analyzed: 5/16/2017Source: L7E0215-01Duplicate (B7E0279-DUP1)

5.01 3.34 303mg/Kg dry3.45 0.859Arsenic

Prepared & Analyzed: 5/16/2017Source: L7E0215-01Matrix Spike (B7E0279-MS1)

5.01 100 3.34 80-120111mg/Kg dry114 0.859Arsenic

Prepared & Analyzed: 5/16/2017Source: L7E0215-01Matrix Spike Dup (B7E0279-MSD1)

4.96 99.2 3.34 2080-120111 0.4mg/Kg dry114 0.851Arsenic

The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.

No duplication of this report is allowed, except in its entirety. Page 12 of 43

Project Manager:

Reported:

Anniston Army Depot

7 Frankford Avenue

Blast Media from Roo-off Boxes

B17129-1

Nathan L Corburn 5/19/17 16:30

MWBE SDBE

NELAC DoD Accredited

Anniston, Alabama 36201

Result PQL Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD

LimitQual Analyte

Quality Control (Continued)

Total Metal Analysis by Method 6010C

MDL

Batch: B7E0279

Prepared & Analyzed: 5/16/2017Blank (B7E0279-BLK1)

5.00 mg/Kg wet0.204 U, 0.204Barium

Prepared & Analyzed: 5/16/2017LCS (B7E0279-BS1)

5.00 100 80-120115mg/Kg wet115 0.204Barium

Prepared & Analyzed: 5/16/2017LCS Dup (B7E0279-BSD1)

5.00 100 2080-120117 2mg/Kg wet117 0.204Barium

Prepared & Analyzed: 5/16/2017Source: L7E0215-01Duplicate (B7E0279-DUP1)

5.01 58.6 302mg/Kg dry57.5 0.204Barium

Prepared & Analyzed: 5/16/2017Source: L7E0215-01Matrix Spike (B7E0279-MS1)

5.01 100 58.6 80-120105mg/Kg dry164 0.204Barium

Prepared & Analyzed: 5/16/2017Source: L7E0215-01Matrix Spike Dup (B7E0279-MSD1)

4.96 99.2 58.6 2080-120107 0.2mg/Kg dry164 0.202Barium

The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.

No duplication of this report is allowed, except in its entirety. Page 13 of 43

Project Manager:

Reported:

Anniston Army Depot

7 Frankford Avenue

Blast Media from Roo-off Boxes

B17129-1

Nathan L Corburn 5/19/17 16:30

MWBE SDBE

NELAC DoD Accredited

Anniston, Alabama 36201

Result PQL Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD

LimitQual Analyte

Quality Control (Continued)

Total Metal Analysis by Method 6010C

MDL

Batch: B7E0279

Prepared & Analyzed: 5/16/2017Blank (B7E0279-BLK1)

5.00 mg/Kg wet0.0120 U, 0.0120Beryllium

Prepared & Analyzed: 5/16/2017LCS (B7E0279-BS1)

5.00 100 80-120110mg/Kg wet110 0.0120Beryllium

Prepared & Analyzed: 5/16/2017LCS Dup (B7E0279-BSD1)

5.00 100 2080-120113 2mg/Kg wet113 0.0120Beryllium

Prepared & Analyzed: 5/16/2017Source: L7E0215-01Duplicate (B7E0279-DUP1)

5.01 3.23 303mg/Kg dry3.14 0.0120Beryllium

Prepared & Analyzed: 5/16/2017Source: L7E0215-01Matrix Spike (B7E0279-MS1)

5.01 100 3.23 80-120103mg/Kg dry107 0.0120Beryllium

Prepared & Analyzed: 5/16/2017Source: L7E0215-01Matrix Spike Dup (B7E0279-MSD1)

4.96 99.2 3.23 2080-120105 0.6mg/Kg dry107 0.0119Beryllium

The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.

No duplication of this report is allowed, except in its entirety. Page 14 of 43

Project Manager:

Reported:

Anniston Army Depot

7 Frankford Avenue

Blast Media from Roo-off Boxes

B17129-1

Nathan L Corburn 5/19/17 16:30

MWBE SDBE

NELAC DoD Accredited

Anniston, Alabama 36201

Result PQL Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD

LimitQual Analyte

Quality Control (Continued)

Total Metal Analysis by Method 6010C

MDL

Batch: B7E0279

Prepared & Analyzed: 5/16/2017Blank (B7E0279-BLK1)

5.00 mg/Kg wet0.0600 U, 0.0600Chromium

Prepared & Analyzed: 5/16/2017LCS (B7E0279-BS1)

5.00 100 80-120115mg/Kg wet115 0.0600Chromium

Prepared & Analyzed: 5/16/2017LCS Dup (B7E0279-BSD1)

5.00 100 2080-120117 2mg/Kg wet117 0.0600Chromium

Prepared & Analyzed: 5/16/2017Source: L7E0215-01Duplicate (B7E0279-DUP1)

5.01 192 3018mg/Kg dry229 0.0601Chromium

Prepared & Analyzed: 5/16/2017Source: L7E0215-01Matrix Spike (B7E0279-MS1)

5.01 100 192 80-12095mg/Kg dry287 0.0601Chromium

Prepared & Analyzed: 5/16/2017Source: L7E0215-01Matrix Spike Dup (B7E0279-MSD1)

4.96 99.2 192 2080-12050 17mg/Kg dry242 0.0595Chromium

The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.

No duplication of this report is allowed, except in its entirety. Page 15 of 43

Project Manager:

Reported:

Anniston Army Depot

7 Frankford Avenue

Blast Media from Roo-off Boxes

B17129-1

Nathan L Corburn 5/19/17 16:30

MWBE SDBE

NELAC DoD Accredited

Anniston, Alabama 36201

Result PQL Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD

LimitQual Analyte

Quality Control (Continued)

Total Metal Analysis by Method 6010C

MDL

Batch: B7E0279

Prepared & Analyzed: 5/16/2017Blank (B7E0279-BLK1)

5.00 mg/Kg wet0.279 U, 0.279Lead

Prepared & Analyzed: 5/16/2017LCS (B7E0279-BS1)

5.00 100 80-120115mg/Kg wet115 0.279Lead

Prepared & Analyzed: 5/16/2017LCS Dup (B7E0279-BSD1)

5.00 100 2080-120117 1mg/Kg wet117 0.279Lead

Prepared & Analyzed: 5/16/2017Source: L7E0215-01Duplicate (B7E0279-DUP1)

5.01 37.2 3014mg/Kg dry32.2 0.279Lead

Prepared & Analyzed: 5/16/2017Source: L7E0215-01Matrix Spike (B7E0279-MS1)

5.01 100 37.2 80-120105mg/Kg dry142 0.279Lead

Prepared & Analyzed: 5/16/2017Source: L7E0215-01Matrix Spike Dup (B7E0279-MSD1)

4.96 99.2 37.2 2080-120104 2mg/Kg dry140 0.277Lead

The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.

No duplication of this report is allowed, except in its entirety. Page 16 of 43

Project Manager:

Reported:

Anniston Army Depot

7 Frankford Avenue

Blast Media from Roo-off Boxes

B17129-1

Nathan L Corburn 5/19/17 16:30

MWBE SDBE

NELAC DoD Accredited

Anniston, Alabama 36201

Result PQL Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD

LimitQual Analyte

Quality Control (Continued)

Total Metal Analysis by Method 6010C

MDL

Batch: B7E0279

Prepared & Analyzed: 5/16/2017Blank (B7E0279-BLK1)

5.00 mg/Kg wet0.132 U, 0.132Nickel

Prepared & Analyzed: 5/16/2017LCS (B7E0279-BS1)

5.00 100 80-120116mg/Kg wet116 0.132Nickel

Prepared & Analyzed: 5/16/2017LCS Dup (B7E0279-BSD1)

5.00 100 2080-120119 2mg/Kg wet119 0.132Nickel

Prepared & Analyzed: 5/16/2017Source: L7E0215-01Duplicate (B7E0279-DUP1)

5.01 74.5 3010mg/Kg dry67.6 0.132Nickel

Prepared & Analyzed: 5/16/2017Source: L7E0215-01Matrix Spike (B7E0279-MS1)

5.01 100 74.5 80-120153mg/Kg dry228 0.132Nickel

Prepared & Analyzed: 5/16/2017Source: L7E0215-01Matrix Spike Dup (B7E0279-MSD1)

4.96 99.2 74.5 2080-120109 22mg/Kg dry183 0.131Nickel

The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.

No duplication of this report is allowed, except in its entirety. Page 17 of 43

Project Manager:

Reported:

Anniston Army Depot

7 Frankford Avenue

Blast Media from Roo-off Boxes

B17129-1

Nathan L Corburn 5/19/17 16:30

MWBE SDBE

NELAC DoD Accredited

Anniston, Alabama 36201

Result PQL Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD

LimitQual Analyte

Quality Control (Continued)

Total Metal Analysis by Method 6010C

MDL

Batch: B7E0279

Prepared & Analyzed: 5/16/2017Blank (B7E0279-BLK1)

5.00 mg/Kg wet0.760 U, 0.760Selenium

Prepared & Analyzed: 5/16/2017LCS (B7E0279-BS1)

5.00 100 80-120118mg/Kg wet118 0.760Selenium

Prepared & Analyzed: 5/16/2017LCS Dup (B7E0279-BSD1)

5.00 100 2080-120120 2mg/Kg wet120 0.760Selenium

Prepared & Analyzed: 5/16/2017Source: L7E0215-01Duplicate (B7E0279-DUP1)

5.01 1.52 3050mg/Kg dry2.53 0.761Selenium

Prepared & Analyzed: 5/16/2017Source: L7E0215-01Matrix Spike (B7E0279-MS1)

5.01 100 1.52 80-120104mg/Kg dry105 0.761Selenium

Prepared & Analyzed: 5/16/2017Source: L7E0215-01Matrix Spike Dup (B7E0279-MSD1)

4.96 99.2 1.52 2080-120108 3mg/Kg dry109 0.754Selenium

The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.

No duplication of this report is allowed, except in its entirety. Page 18 of 43

Project Manager:

Reported:

Anniston Army Depot

7 Frankford Avenue

Blast Media from Roo-off Boxes

B17129-1

Nathan L Corburn 5/19/17 16:30

MWBE SDBE

NELAC DoD Accredited

Anniston, Alabama 36201

Result PQL Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD

LimitQual Analyte

Quality Control (Continued)

Total Metal Analysis by Method 6010C

MDL

Batch: B7E0279

Prepared & Analyzed: 5/16/2017Blank (B7E0279-BLK1)

5.00 mg/Kg wet0.0300 U, 0.0300Silver

Prepared & Analyzed: 5/16/2017LCS (B7E0279-BS1)

5.00 100 80-120108mg/Kg wet108 0.0300Silver

Prepared & Analyzed: 5/16/2017LCS Dup (B7E0279-BSD1)

5.00 100 2080-120111 2mg/Kg wet111 0.0300Silver

Prepared & Analyzed: 5/16/2017Source: L7E0215-01Duplicate (B7E0279-DUP1)

5.01 0.596 307mg/Kg dry0.555 0.0301Silver

Prepared & Analyzed: 5/16/2017Source: L7E0215-01Matrix Spike (B7E0279-MS1)

5.01 100 0.596 80-12099mg/Kg dry99.9 0.0301Silver

Prepared & Analyzed: 5/16/2017Source: L7E0215-01Matrix Spike Dup (B7E0279-MSD1)

4.96 99.2 0.596 2080-12099 1mg/Kg dry98.8 0.0298Silver

The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.

No duplication of this report is allowed, except in its entirety. Page 19 of 43

Project Manager:

Reported:

Anniston Army Depot

7 Frankford Avenue

Blast Media from Roo-off Boxes

B17129-1

Nathan L Corburn 5/19/17 16:30

MWBE SDBE

NELAC DoD Accredited

Anniston, Alabama 36201

Result PQL Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD

LimitQual Analyte

Quality Control (Continued)

Total Metal Analysis by Method 6010C

MDL

Batch: B7E0279

Prepared & Analyzed: 5/16/2017Blank (B7E0279-BLK1)

5.00 mg/Kg wet0.0620 U, 0.0620Vanadium

Prepared & Analyzed: 5/16/2017LCS (B7E0279-BS1)

5.00 100 80-120115mg/Kg wet115 0.0620Vanadium

Prepared & Analyzed: 5/16/2017LCS Dup (B7E0279-BSD1)

5.00 100 2080-120117 2mg/Kg wet117 0.0620Vanadium

Prepared & Analyzed: 5/16/2017Source: L7E0215-01Duplicate (B7E0279-DUP1)

5.01 5.50 301mg/Kg dry5.56 0.0621Vanadium

Prepared & Analyzed: 5/16/2017Source: L7E0215-01Matrix Spike (B7E0279-MS1)

5.01 100 5.50 80-120109mg/Kg dry114 0.0621Vanadium

Prepared & Analyzed: 5/16/2017Source: L7E0215-01Matrix Spike Dup (B7E0279-MSD1)

4.96 99.2 5.50 2080-120111 0.7mg/Kg dry115 0.0615Vanadium

The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.

No duplication of this report is allowed, except in its entirety. Page 20 of 43

Project Manager:

Reported:

Anniston Army Depot

7 Frankford Avenue

Blast Media from Roo-off Boxes

B17129-1

Nathan L Corburn 5/19/17 16:30

MWBE SDBE

NELAC DoD Accredited

Anniston, Alabama 36201

Result PQL Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD

LimitQual Analyte

Quality Control (Continued)

Total Metal Analysis by Method 6010C

MDL

Batch: B7E0279

Prepared & Analyzed: 5/16/2017Blank (B7E0279-BLK1)

5.00 mg/Kg wet0.0980 U, 0.0980Zinc

Prepared & Analyzed: 5/16/2017LCS (B7E0279-BS1)

5.00 100 80-120121mg/Kg wet121 0.0980Zinc

Prepared & Analyzed: 5/16/2017LCS Dup (B7E0279-BSD1)

5.00 100 2080-120123 2mg/Kg wet123 0.0980Zinc

Prepared & Analyzed: 5/16/2017Source: L7E0215-01Duplicate (B7E0279-DUP1)

5.01 240 306mg/Kg dry225 0.0982Zinc

Prepared & Analyzed: 5/16/2017Source: L7E0215-01Matrix Spike (B7E0279-MS1)

5.01 100 240 80-12088mg/Kg dry329 0.0982Zinc

Prepared & Analyzed: 5/16/2017Source: L7E0215-01Matrix Spike Dup (B7E0279-MSD1)

4.96 99.2 240 2080-12093 1mg/Kg dry332 0.0972Zinc

The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.

No duplication of this report is allowed, except in its entirety. Page 21 of 43

Project Manager:

Reported:

Anniston Army Depot

7 Frankford Avenue

Blast Media from Roo-off Boxes

B17129-1

Nathan L Corburn 5/19/17 16:30

MWBE SDBE

NELAC DoD Accredited

Anniston, Alabama 36201

Result PQL Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD

LimitQual Analyte

Quality Control (Continued)

TCLP Metal Analysis by Method 6010C

MDL

Batch: B7E0278

Prepared & Analyzed: 5/16/2017Blank (B7E0278-BLK1)

250 ug/L50.0 U, 50.0Antimony

Prepared & Analyzed: 5/16/2017LCS (B7E0278-BS1)

250 2000 85-115116ug/L2330 50.0Antimony

Prepared & Analyzed: 5/16/2017LCS Dup (B7E0278-BSD1)

250 2000 2085-115116 0.007ug/L2330 50.0Antimony

Prepared & Analyzed: 5/16/2017Source: A7E0008-01Duplicate (B7E0278-DUP1)

250 1320 204ug/L1260 50.0Antimony

Prepared & Analyzed: 5/16/2017Source: L7E0105-02Matrix Spike (B7E0278-MS1)

250 2000 ND 85-115120ug/L2400 50.0Antimony

Prepared & Analyzed: 5/16/2017Source: L7E0105-02Matrix Spike Dup (B7E0278-MSD1)

250 2000 ND 2085-115117 2ug/L2340 50.0Antimony

The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.

No duplication of this report is allowed, except in its entirety. Page 22 of 43

Project Manager:

Reported:

Anniston Army Depot

7 Frankford Avenue

Blast Media from Roo-off Boxes

B17129-1

Nathan L Corburn 5/19/17 16:30

MWBE SDBE

NELAC DoD Accredited

Anniston, Alabama 36201

Result PQL Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD

LimitQual Analyte

Quality Control (Continued)

TCLP Metal Analysis by Method 6010C

MDL

Batch: B7E0278

Prepared & Analyzed: 5/16/2017Blank (B7E0278-BLK1)

250 ug/L50.0 U, 50.0Arsenic

Prepared & Analyzed: 5/16/2017LCS (B7E0278-BS1)

250 2000 85-115125ug/L2490 50.0Arsenic

Prepared & Analyzed: 5/16/2017LCS Dup (B7E0278-BSD1)

250 2000 2085-115123 1ug/L2470 50.0Arsenic

Prepared & Analyzed: 5/16/2017Source: A7E0008-01Duplicate (B7E0278-DUP1)

250 ND 20ug/L50.0 U, 50.0Arsenic

Prepared & Analyzed: 5/16/2017Source: L7E0105-02Matrix Spike (B7E0278-MS1)

250 2000 ND 85-115125ug/L2500 50.0Arsenic

Prepared & Analyzed: 5/16/2017Source: L7E0105-02Matrix Spike Dup (B7E0278-MSD1)

250 2000 ND 2085-115126 0.6ug/L2510 50.0Arsenic

The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.

No duplication of this report is allowed, except in its entirety. Page 23 of 43

Project Manager:

Reported:

Anniston Army Depot

7 Frankford Avenue

Blast Media from Roo-off Boxes

B17129-1

Nathan L Corburn 5/19/17 16:30

MWBE SDBE

NELAC DoD Accredited

Anniston, Alabama 36201

Result PQL Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD

LimitQual Analyte

Quality Control (Continued)

TCLP Metal Analysis by Method 6010C

MDL

Batch: B7E0278

Prepared & Analyzed: 5/16/2017Blank (B7E0278-BLK1)

250 ug/L50.0 U, 50.0Barium

Prepared & Analyzed: 5/16/2017LCS (B7E0278-BS1)

250 2000 85-115101ug/L2030 50.0Barium

Prepared & Analyzed: 5/16/2017LCS Dup (B7E0278-BSD1)

250 2000 2085-115101 0.2ug/L2020 50.0Barium

Prepared & Analyzed: 5/16/2017Source: A7E0008-01Duplicate (B7E0278-DUP1)

250 1580 204ug/L1520 50.0Barium

Prepared & Analyzed: 5/16/2017Source: L7E0105-02Matrix Spike (B7E0278-MS1)

250 2000 ND 85-115102ug/L2040 50.0Barium

Prepared & Analyzed: 5/16/2017Source: L7E0105-02Matrix Spike Dup (B7E0278-MSD1)

250 2000 ND 2085-115102 0.05ug/L2040 50.0Barium

The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.

No duplication of this report is allowed, except in its entirety. Page 24 of 43

Project Manager:

Reported:

Anniston Army Depot

7 Frankford Avenue

Blast Media from Roo-off Boxes

B17129-1

Nathan L Corburn 5/19/17 16:30

MWBE SDBE

NELAC DoD Accredited

Anniston, Alabama 36201

Result PQL Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD

LimitQual Analyte

Quality Control (Continued)

TCLP Metal Analysis by Method 6010C

MDL

Batch: B7E0278

Prepared & Analyzed: 5/16/2017Blank (B7E0278-BLK1)

250 ug/L50.0 U, 50.0Beryllium

Prepared & Analyzed: 5/16/2017LCS (B7E0278-BS1)

250 2000 85-115112ug/L2230 50.0Beryllium

Prepared & Analyzed: 5/16/2017LCS Dup (B7E0278-BSD1)

250 2000 2085-115111 0.3ug/L2230 50.0Beryllium

Prepared & Analyzed: 5/16/2017Source: A7E0008-01Duplicate (B7E0278-DUP1)

250 ND 20ug/L50.0 U, 50.0Beryllium

Prepared & Analyzed: 5/16/2017Source: L7E0105-02Matrix Spike (B7E0278-MS1)

250 2000 ND 85-115112ug/L2240 50.0Beryllium

Prepared & Analyzed: 5/16/2017Source: L7E0105-02Matrix Spike Dup (B7E0278-MSD1)

250 2000 ND 2085-115112 0.08ug/L2240 50.0Beryllium

The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.

No duplication of this report is allowed, except in its entirety. Page 25 of 43

Project Manager:

Reported:

Anniston Army Depot

7 Frankford Avenue

Blast Media from Roo-off Boxes

B17129-1

Nathan L Corburn 5/19/17 16:30

MWBE SDBE

NELAC DoD Accredited

Anniston, Alabama 36201

Result PQL Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD

LimitQual Analyte

Quality Control (Continued)

TCLP Metal Analysis by Method 6010C

MDL

Batch: B7E0278

Prepared & Analyzed: 5/16/2017Blank (B7E0278-BLK1)

250 ug/L50.0 U, 50.0Cadmium

Prepared & Analyzed: 5/16/2017LCS (B7E0278-BS1)

250 2000 85-115113ug/L2270 50.0Cadmium

Prepared & Analyzed: 5/16/2017LCS Dup (B7E0278-BSD1)

250 2000 2085-115113 0.3ug/L2260 50.0Cadmium

Prepared & Analyzed: 5/16/2017Source: A7E0008-01Duplicate (B7E0278-DUP1)

250 ND 20ug/L50.0 U, 50.0Cadmium

Prepared & Analyzed: 5/16/2017Source: L7E0105-02Matrix Spike (B7E0278-MS1)

250 2000 ND 85-115114ug/L2270 50.0Cadmium

Prepared & Analyzed: 5/16/2017Source: L7E0105-02Matrix Spike Dup (B7E0278-MSD1)

250 2000 ND 2085-115114 0.04ug/L2270 50.0Cadmium

The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.

No duplication of this report is allowed, except in its entirety. Page 26 of 43

Project Manager:

Reported:

Anniston Army Depot

7 Frankford Avenue

Blast Media from Roo-off Boxes

B17129-1

Nathan L Corburn 5/19/17 16:30

MWBE SDBE

NELAC DoD Accredited

Anniston, Alabama 36201

Result PQL Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD

LimitQual Analyte

Quality Control (Continued)

TCLP Metal Analysis by Method 6010C

MDL

Batch: B7E0278

Prepared & Analyzed: 5/16/2017Blank (B7E0278-BLK1)

250 ug/L50.0 U, 50.0Chromium

Prepared & Analyzed: 5/16/2017LCS (B7E0278-BS1)

250 2000 85-115111ug/L2210 50.0Chromium

Prepared & Analyzed: 5/16/2017LCS Dup (B7E0278-BSD1)

250 2000 2085-115110 0.2ug/L2210 50.0Chromium

Prepared & Analyzed: 5/16/2017Source: A7E0008-01Duplicate (B7E0278-DUP1)

250 ND 20ug/L50.0 U, 50.0Chromium

Prepared & Analyzed: 5/16/2017Source: L7E0105-02Matrix Spike (B7E0278-MS1)

250 2000 ND 85-115111ug/L2220 50.0Chromium

Prepared & Analyzed: 5/16/2017Source: L7E0105-02Matrix Spike Dup (B7E0278-MSD1)

250 2000 ND 2085-115112 0.7ug/L2230 50.0Chromium

The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.

No duplication of this report is allowed, except in its entirety. Page 27 of 43

Project Manager:

Reported:

Anniston Army Depot

7 Frankford Avenue

Blast Media from Roo-off Boxes

B17129-1

Nathan L Corburn 5/19/17 16:30

MWBE SDBE

NELAC DoD Accredited

Anniston, Alabama 36201

Result PQL Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD

LimitQual Analyte

Quality Control (Continued)

TCLP Metal Analysis by Method 6010C

MDL

Batch: B7E0278

Prepared & Analyzed: 5/16/2017Blank (B7E0278-BLK1)

250 ug/L50.0 U, 50.0Lead

Prepared & Analyzed: 5/16/2017LCS (B7E0278-BS1)

250 2000 85-115109ug/L2190 50.0Lead

Prepared & Analyzed: 5/16/2017LCS Dup (B7E0278-BSD1)

250 2000 2085-115109 0.2ug/L2180 50.0Lead

Prepared & Analyzed: 5/16/2017Source: A7E0008-01Duplicate (B7E0278-DUP1)

250 378 206ug/L357 50.0Lead

Prepared & Analyzed: 5/16/2017Source: L7E0105-02Matrix Spike (B7E0278-MS1)

250 2000 ND 85-115111ug/L2220 50.0Lead

Prepared & Analyzed: 5/16/2017Source: L7E0105-02Matrix Spike Dup (B7E0278-MSD1)

250 2000 ND 2085-115110 0.6ug/L2210 50.0Lead

The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.

No duplication of this report is allowed, except in its entirety. Page 28 of 43

Project Manager:

Reported:

Anniston Army Depot

7 Frankford Avenue

Blast Media from Roo-off Boxes

B17129-1

Nathan L Corburn 5/19/17 16:30

MWBE SDBE

NELAC DoD Accredited

Anniston, Alabama 36201

Result PQL Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD

LimitQual Analyte

Quality Control (Continued)

TCLP Metal Analysis by Method 6010C

MDL

Batch: B7E0278

Prepared & Analyzed: 5/16/2017Blank (B7E0278-BLK1)

250 ug/L50.0 U, 50.0Nickel

Prepared & Analyzed: 5/16/2017LCS (B7E0278-BS1)

250 2000 85-115113ug/L2260 50.0Nickel

Prepared & Analyzed: 5/16/2017LCS Dup (B7E0278-BSD1)

250 2000 2085-115115 1ug/L2290 50.0Nickel

Prepared & Analyzed: 5/16/2017Source: A7E0008-01Duplicate (B7E0278-DUP1)

250 ND 20ug/L50.0 U, 50.0Nickel

Prepared & Analyzed: 5/16/2017Source: L7E0105-02Matrix Spike (B7E0278-MS1)

250 2000 ND 85-115116ug/L2310 50.0Nickel

Prepared & Analyzed: 5/16/2017Source: L7E0105-02Matrix Spike Dup (B7E0278-MSD1)

250 2000 ND 2085-115114 2ug/L2270 50.0Nickel

The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.

No duplication of this report is allowed, except in its entirety. Page 29 of 43

Project Manager:

Reported:

Anniston Army Depot

7 Frankford Avenue

Blast Media from Roo-off Boxes

B17129-1

Nathan L Corburn 5/19/17 16:30

MWBE SDBE

NELAC DoD Accredited

Anniston, Alabama 36201

Result PQL Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD

LimitQual Analyte

Quality Control (Continued)

TCLP Metal Analysis by Method 6010C

MDL

Batch: B7E0278

Prepared & Analyzed: 5/16/2017Blank (B7E0278-BLK1)

250 ug/L50.0 U, 50.0Selenium

Prepared & Analyzed: 5/16/2017LCS (B7E0278-BS1)

250 2000 85-115128ug/L2550 50.0Selenium

Prepared & Analyzed: 5/16/2017LCS Dup (B7E0278-BSD1)

250 2000 2085-115128 0.6ug/L2570 50.0Selenium

Prepared & Analyzed: 5/16/2017Source: A7E0008-01Duplicate (B7E0278-DUP1)

250 ND 20ug/L50.0 U, 50.0Selenium

Prepared & Analyzed: 5/16/2017Source: L7E0105-02Matrix Spike (B7E0278-MS1)

250 2000 ND 85-115132ug/L2650 50.0Selenium

Prepared & Analyzed: 5/16/2017Source: L7E0105-02Matrix Spike Dup (B7E0278-MSD1)

250 2000 ND 2085-115128 3ug/L2560 50.0Selenium

The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.

No duplication of this report is allowed, except in its entirety. Page 30 of 43

Project Manager:

Reported:

Anniston Army Depot

7 Frankford Avenue

Blast Media from Roo-off Boxes

B17129-1

Nathan L Corburn 5/19/17 16:30

MWBE SDBE

NELAC DoD Accredited

Anniston, Alabama 36201

Result PQL Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD

LimitQual Analyte

Quality Control (Continued)

TCLP Metal Analysis by Method 6010C

MDL

Batch: B7E0278

Prepared & Analyzed: 5/16/2017Blank (B7E0278-BLK1)

250 ug/L50.0 U, 50.0Silver

Prepared & Analyzed: 5/16/2017LCS (B7E0278-BS1)

250 2000 85-115110ug/L2210 50.0Silver

Prepared & Analyzed: 5/16/2017LCS Dup (B7E0278-BSD1)

250 2000 2085-115110 0.3ug/L2200 50.0Silver

Prepared & Analyzed: 5/16/2017Source: A7E0008-01Duplicate (B7E0278-DUP1)

250 ND 20ug/L50.0 U, 50.0Silver

Prepared & Analyzed: 5/16/2017Source: L7E0105-02Matrix Spike (B7E0278-MS1)

250 2000 ND 85-115113ug/L2260 50.0Silver

Prepared & Analyzed: 5/16/2017Source: L7E0105-02Matrix Spike Dup (B7E0278-MSD1)

250 2000 ND 2085-115110 3ug/L2200 50.0Silver

The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.

No duplication of this report is allowed, except in its entirety. Page 31 of 43

Project Manager:

Reported:

Anniston Army Depot

7 Frankford Avenue

Blast Media from Roo-off Boxes

B17129-1

Nathan L Corburn 5/19/17 16:30

MWBE SDBE

NELAC DoD Accredited

Anniston, Alabama 36201

Result PQL Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD

LimitQual Analyte

Quality Control (Continued)

TCLP Metal Analysis by Method 6010C

MDL

Batch: B7E0278

Prepared & Analyzed: 5/16/2017Blank (B7E0278-BLK1)

250 ug/L50.0 U, 50.0Thallium

Prepared & Analyzed: 5/16/2017LCS (B7E0278-BS1)

250 2000 85-115106ug/L2120 50.0Thallium

Prepared & Analyzed: 5/16/2017LCS Dup (B7E0278-BSD1)

250 2000 2085-115106 0.4ug/L2120 50.0Thallium

Prepared & Analyzed: 5/16/2017Source: A7E0008-01Duplicate (B7E0278-DUP1)

250 ND 20ug/L50.0 U, 50.0Thallium

Prepared & Analyzed: 5/16/2017Source: L7E0105-02Matrix Spike (B7E0278-MS1)

250 2000 ND 85-115109ug/L2180 50.0Thallium

Prepared & Analyzed: 5/16/2017Source: L7E0105-02Matrix Spike Dup (B7E0278-MSD1)

250 2000 ND 2085-115106 2ug/L2130 50.0Thallium

The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.

No duplication of this report is allowed, except in its entirety. Page 32 of 43

Project Manager:

Reported:

Anniston Army Depot

7 Frankford Avenue

Blast Media from Roo-off Boxes

B17129-1

Nathan L Corburn 5/19/17 16:30

MWBE SDBE

NELAC DoD Accredited

Anniston, Alabama 36201

Result PQL Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD

LimitQual Analyte

Quality Control (Continued)

TCLP Metal Analysis by Method 6010C

MDL

Batch: B7E0278

Prepared & Analyzed: 5/16/2017Blank (B7E0278-BLK1)

250 ug/L50.0 U, 50.0Vanadium

Prepared & Analyzed: 5/16/2017LCS (B7E0278-BS1)

250 2000 85-115111ug/L2220 50.0Vanadium

Prepared & Analyzed: 5/16/2017LCS Dup (B7E0278-BSD1)

250 2000 2085-115111 0.06ug/L2220 50.0Vanadium

Prepared & Analyzed: 5/16/2017Source: A7E0008-01Duplicate (B7E0278-DUP1)

250 ND 20ug/L50.0 U, 50.0Vanadium

Prepared & Analyzed: 5/16/2017Source: L7E0105-02Matrix Spike (B7E0278-MS1)

250 2000 ND 85-115111ug/L2210 50.0Vanadium

Prepared & Analyzed: 5/16/2017Source: L7E0105-02Matrix Spike Dup (B7E0278-MSD1)

250 2000 ND 2085-115111 0.7ug/L2230 50.0Vanadium

The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.

No duplication of this report is allowed, except in its entirety. Page 33 of 43

Project Manager:

Reported:

Anniston Army Depot

7 Frankford Avenue

Blast Media from Roo-off Boxes

B17129-1

Nathan L Corburn 5/19/17 16:30

MWBE SDBE

NELAC DoD Accredited

Anniston, Alabama 36201

Result PQL Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD

LimitQual Analyte

Quality Control (Continued)

TCLP Metal Analysis by Method 6010C

MDL

Batch: B7E0278

Prepared & Analyzed: 5/16/2017Blank (B7E0278-BLK1)

250 ug/L50.0 U, 50.0Zinc

Prepared & Analyzed: 5/16/2017LCS (B7E0278-BS1)

250 2000 85-115124ug/L2480 50.0Zinc

Prepared & Analyzed: 5/16/2017LCS Dup (B7E0278-BSD1)

250 2000 2085-115124 0.05ug/L2480 50.0Zinc

Prepared & Analyzed: 5/16/2017Source: A7E0008-01Duplicate (B7E0278-DUP1)

250 ND 20ug/L50.0 U, 50.0Zinc

Prepared & Analyzed: 5/16/2017Source: L7E0105-02Matrix Spike (B7E0278-MS1)

250 2000 ND 85-115124ug/L2490 50.0Zinc

Prepared & Analyzed: 5/16/2017Source: L7E0105-02Matrix Spike Dup (B7E0278-MSD1)

250 2000 ND 2085-115125 0.6ug/L2500 50.0Zinc

The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.

No duplication of this report is allowed, except in its entirety. Page 34 of 43

Project Manager:

Reported:

Anniston Army Depot

7 Frankford Avenue

Blast Media from Roo-off Boxes

B17129-1

Nathan L Corburn 5/19/17 16:30

MWBE SDBE

NELAC DoD Accredited

Anniston, Alabama 36201

Result PQL Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD

LimitQual Analyte

Quality Control (Continued)

TCLP Mercury Analysis by Method 7470A

MDL

Batch: B7E0335

Prepared & Analyzed: 5/18/2017Blank (B7E0335-BLK1)

0.200 ug/L0.0700 U, 0.0700Mercury

Prepared & Analyzed: 5/18/2017LCS (B7E0335-BS1)

0.200 2.50 85-115112ug/L2.79 0.0700Mercury

Prepared & Analyzed: 5/18/2017LCS Dup (B7E0335-BSD1)

0.200 2.50 2085-11592 20ug/L2.29 0.0700Mercury

Prepared & Analyzed: 5/18/2017Source: L7E0215-01Duplicate (B7E0335-DUP1)

0.200 ND 20ug/L0.0700 U, 0.0700Mercury

The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.

No duplication of this report is allowed, except in its entirety. Page 35 of 43

Project Manager:

Reported:

Anniston Army Depot

7 Frankford Avenue

Blast Media from Roo-off Boxes

B17129-1

Nathan L Corburn 5/19/17 16:30

MWBE SDBE

NELAC DoD Accredited

Anniston, Alabama 36201

Result PQL Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD

LimitQual Analyte

Quality Control (Continued)

Percent Moisture by Method 2540G

MDL

Batch: B7E0288

Prepared: 5/16/2017 Analyzed: 5/17/2017Source: L7E0215-01Duplicate (B7E0288-DUP1)

0.100 99.8 200.0007%99.8 0.100% Solids

0.100 0.170 200.4%0.170 0.100Percent Moisture

The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.

No duplication of this report is allowed, except in its entirety. Page 36 of 43

Project Manager:

Reported:

Anniston Army Depot

7 Frankford Avenue

Blast Media from Roo-off Boxes

B17129-1

Nathan L Corburn 5/19/17 16:30

MWBE SDBE

NELAC DoD Accredited

Anniston, Alabama 36201

List of Certifications for FTS - Florida

CodeDescriptionNumber ExpiresFacility

LANELAC04176 LA CERTIFICATE 12/31/2017FTSA

ANC483 NC CERTIFICATE 12/31/2017FTSL

KENTUKY85 KENTUKY CERTIFICATE FTSA

LFLNELACE84098 FL NELAC CERTIFICATE 06/30/2017FTSL

AFLNELACE87429 FL NELAC CERTIFICATE 06/30/2017FTSA

DODLI0-135 DoD CERTIFICATE Renewal in Process 11/30/2016FTSL

USDAP330-07-00105 USDA CERTIFICATE FTSA

Notes and Definitions

Item Definition

U Compound was not detected.

Dry Sample results reported on a dry weight basis.

I Value estimated to be between the Laboratory Detection and Reporting Limit

J QC Failure see Case Narrative

L Concentration exceeds calibration range

N Tentatively Identified Compound

Q Hold time exceeded

V Analyte equal to or above detection limit in the method blank

TNTC Bacteria is present but Too Numerous To Count

RPD Relative Percent Difference

%REC Percent Recovery

Source Sample that was matrix spiked or duplicated.

The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.

No duplication of this report is allowed, except in its entirety. Page 37 of 43

WORK ORDER

Printed: 05/17/2017 5:19 pm

Blast Media from Roo-off BoxesProject:

Project Number: B17129-1

Project Manager: Derek Rounsley Status

Anniston Army Depot

Dilip Kothari

7 Frankford Avenue DRK - Bidg 199

Anniston, ALABAMA 36201

Phone: (256) 235-4854

Anniston Army Depot

Patricia E. Dodson

7 Frankford Avenue

Anniston, Alabama 36201

Phone: (256) 235-6700

Report To: Invoice To:

Logged In By: Lourdes Arevalo

Samples Received at: 1.8°C

3. COC (Chain of Custody)/Labels Agree?

1. Temperature of Coolers Checked?

2. Containers Properly Preserved

4. Received On Ice?

Yes

Yes

Yes

Yes

5. COC properly signed?

6. COC/Labels Agree?

7. Container Labels legible and intact?

8. Sample Matrix agree with COC?

Yes

Yes

Yes

Yes

Yes

Yes

Yes

Yes

9. Samples in proper containers?

10. Preservation Confirmed?

11. Containers Intact?

12. Sufficient Sample Amount for all analyses?

Date Due: 05/19/2017 (3 day TAT)

Cooler Data

Received By:Date Received: Lourdes Arevalo05/16/2017 11:32 AM

Date Logged In: 05/16/2017 12:03 PM

Work Order Comments:RUSH

Analysis Due TAT Expires CommentsStatus

L7E0215-01 86837/DPBM4330-RB [Solid] Sampled 5/9/2017 1:55:00PM

3 11/05/201705/19/2017TM 6010 Tot Chromium Cancelled

3 11/05/201705/19/2017TM 6010 Tot Vanadium Cancelled

3 11/05/201705/19/2017TM 6010 Tot Zinc Cancelled

3 06/06/201705/19/2017TM 7470 TCLP Mercury 25-Received

3 11/05/201705/19/2017AG AAD STD Total Metals [Group]

3 06/06/201705/19/2017TM 7470 Tot Mercury Cancelled

3 11/05/201705/19/2017TM 6010 Tot Thallium Cancelled

3 11/05/201705/19/2017TM 6010 Tot Silver Cancelled

3 11/05/201705/19/2017TM 6010 Tot Selenium Cancelled

3 11/05/201705/19/2017TM 6010 Tot Lead Cancelled

3 11/05/201705/19/2017TM 6010 Tot Cadmium Cancelled

3 11/05/201705/19/2017TM 6010 Tot Beryllium Cancelled

3 11/05/201705/19/2017TM 6010 Tot Barium Cancelled

3 11/05/201705/19/2017TM 6010 Tot Arsenic Cancelled

3 11/05/201705/19/2017TM 6010 Tot Antimony Cancelled

3 11/05/201705/19/2017TM 6010 TCLP Chromium 50-Reviewed

3 11/05/201705/19/2017TM 6010 Tot Nickel Cancelled

3 11/05/201705/19/2017TM 6010 TCLP Antimony 50-Reviewed

3 11/05/201705/19/2017TM 6010 TCLP Zinc 50-Reviewed

3 11/05/201705/19/2017TM 6010 TCLP Barium 50-Reviewed

3 11/05/201705/19/2017TM 6010 TCLP Cadmium 50-Reviewed

3 11/05/201705/19/2017TM 6010 TCLP Arsenic 50-Reviewed

3 06/23/201705/19/2017AW PerMois TotSol SM2540G Cancelled

3 11/05/201705/19/2017TM 6010 TCLP Lead 50-Reviewed

3 06/06/201705/19/2017AL TCLP Metal Extraction 25-Received

3 11/05/201705/19/2017TM 6010 TCLP Nickel 50-Reviewed

3 11/05/201705/19/2017TM 6010 TCLP Selenium 50-Reviewed

3 11/05/201705/19/2017TM 6010 TCLP Silver 50-Reviewed

3 11/05/201705/19/2017TM 6010 TCLP Thallium 50-Reviewed

Page 1 of 5Page 39 of 43

Printed: 05/17/2017 5:19 pm

Blast Media from Roo-off BoxesProject:

Project Number: B17129-1

Project Manager: Derek Rounsley

(Continued)

Status

Analysis Due TAT Expires…