Flint Bishop Addendum 2.pdf

PDF 1 MB Posted Jul 9, 2026

Attached to: 761/25250. SAR; Bishop Airport Landfill
Solicitation number: RFQ 171 260000000323 3
Issued by: Genesee County, Michigan

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Written by GovTribe AI · Jul 10, 2026

Summary of Flint Bishop Addendum 2 and Associated Sampling Data

This is a Construction Bid Addendum No. 2 issued by the Michigan Department of Technology, Management and Budget (DTMB) State Facilities Administration Design & Construction Division for the Bishop Airport Landfill project (Site ID #25000453, File Number 761/25250.SAR). The addendum, issued on July 9, 2026, by professional DLZ Michigan, Inc., modifies the bidding documents for this environmental remediation project. Key modifications include: the bid opening due date has been moved to July 22, 2026, at 2:00 PM Eastern; additional questions will be accepted until July 14, 2026, at noon Eastern; and additional 2025 sampling data including PFAS results have been provided as Attachment 1. Bidders must acknowledge this addendum in their bid submission, as failure to do so may result in bid rejection. The addendum becomes part of the contract documents and is incorporated with all other contract requirements.

The attached sampling data report from Metiri Group - Holt analytical laboratory, dated November 19, 2025, provides comprehensive environmental testing results for two water samples collected from the Bishop Airport Landfill on November 4, 2025. The report includes analysis of volatile organic compounds (VOCs), semi-volatile organic compounds, polychlorinated biphenyls (PCBs), per- and polyfluoroalkyl substances (PFAS), metals, and Toxicity Characteristic Leaching Procedure (TCLP) results. Notable PFAS detections include PFOA, PFOS, PFHxA, and other fluorinated compounds in concentrations ranging from single-digit to three-digit ng/L. The testing was conducted in accordance with EPA methods and NELAC standards, with quality assurance procedures documented throughout. Sample disposal timelines are specified as 7 calendar days for TO-15 samples and 30 days for all other samples post-reporting.

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Other files

File	Type	Posted
Flint Bishop Addendum 1 25250.pdf	PDF	Jul 9, 2026
Flint Bishop Landfill Cap Div 1-3, Drawings.pdf	PDF	Jul 9, 2026
Flint Bishop Landfill Cap Advertisement Rev.pdf	PDF	Jul 9, 2026
Flint Bishop Landfill Cap Div 0, Appendices.pdf	PDF	Jul 9, 2026
Service Disabled Veteran Owned Business Info Sheet 2025.pdf	PDF	Jul 9, 2026

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DTMB-0414 (Rev 6/25)

DEPARTMENT OF TECHNOLOGY, MANAGEMENT AND

BUDGET

State Facilities Administration Design & Construction Division

CONSTRUCTION BID ADDENDUM NO. 2

This form identifies an Addendum to Bidding Documents, and incorporates interpretations or clarifications, modifications, acceptance of proposed “or equal” materials, and other information into the Bidding Documents. Addenda will be numbered by the Professional and distributed through www.michigan.gov/SIGMAVSS as an attachment.

TO:

ALL BIDDERS

DATE ISSUED

7/9/2026

PROJECT NAME

Bishop Airport Landfill (Site ID #25000453)

FILE NUMBER

761/25250.SAR

PROFESSIONAL

DLZ Michigan, Inc.

PROJECT DIRECTOR

Project Director

BID OPENING DATE:

7/22/2026

ADDENDUM ITEMS:

1. Bid opening due date has been moved to July 22, 2026 at 2:00 PM Eastern.

2. Additional questions will be accepted until July 14, 2026 at noon Eastern

3. Additional 2025 sampling data, including PFAS results (Attachment 1).

ACKNOWLEDGEMENT: This Addendum must be acknowledged by the Bidder in the space provided in the Bid Summary and Bid Form. Failing to acknowledge Addenda may be cause for the Bid to be rejected. Addenda will become part of the Contract Documents.

PROFESSIONAL: DLZ Michigan, Inc. DATE: 7/9/2026

APPROVED BY:

PROJECT DIRECTOR: DATE: Click to enter date

Metiri Group - Holt

1914 Holloway Dr, Holt, MI 48842 - Phone (517) 699-0345 - www.metirigroup.com

November 19, 2025

EGLE - State Overflow

Lansing, MI 48906

3350 N Martin Luther King Jr Blvd

Brian Kuberski

Thank you for selecting Metiri Group - Holt as your analytical laboratory. The samples submitted have been analyzed in accordance with all method and NELAC standards, as applicable. Any exceptions to compliance are noted in the report.

Please note that TO-15 samples will be disposed of 7 calendar days after the reporting date. All other samples will be disposed of 30 days after the reporting date.

If you have any questions regarding these results, or if we may be of further assistance to you, please contact us at (517) 699-0345.

RE: Flint Bishop Airport Landfill / 2341-7650-81 2341-7650-81

25K0043

[TOC_1]Cover

Letter[TOC]

Sincerely, Sophie Snow Project Manager

Page 1 of 88 25K0043_1 HoltGeneralFormat 11 19 25 1521 11/19/25 15:22:11

Table of Contents mailto://sophie.snow@metirigroup.com?subject=25K0043 FINAL

Cover Letter 1

Samples in Report 3

Case Narratives Analyses 3

Sample Results 4

Quality Assurance Results 39

Qualifiers and Definitions 82

Chain of Custody 88

Page 2 of 88 25K0043_1 HoltGeneralFormat 11 19 25 1521 11/19/25 15:22:11

Project:

Project Number:

Project Manager:

EGLE - State Overflow

3350 N Martin Luther King Jr Blvd

Lansing, MI 48906

Flint Bishop Airport Landfill / 2341-7650-81

2341-7650-81

Brian Kuberski Reported: 11/19/2025 15:21

Metiri Group - Holt - 1914 Holloway Dr, Holt, MI 48842

[TOC_1]Samples in

Report[TOC]Work Order Case Narrative

In regards to this project: Flint Bishop Airport Landfill

File No.: 761/24124.AGY

Contract Order No.: Y24136

Permanent ISD No.: 00869

Location Code is: 6838

Sample -01 will be qualified as potentially biased low due to headspace in all of the sample containers.

Samples -01 and -02 were qualified for several Extracted Internal Standard recoveries that were outside the acceptance criteria by less than 50% of the control limit. This does not bias the reported results, as the instrument�s calibration inherently accounts for this level of variability.

Sample -01 was qualified for multiple compounds due to the Extracted Internal Standard Area recovery being outside the control limits by more than 50%. There may be a bias in the results.

[TOC_1]Case Narratives -

Analyses[TOC]

Samples in this Report

Sample Lab ID Matrix Date Sampled Date ReceivedQualifiers

Vent #125K0043-01 11/04/2025 16:00 11/05/2025Water

Comp-0125K0043-02 11/04/2025 17:00 11/05/2025Water

The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.

No duplication of this report is allowed, except in its entirety.

Page 3 of 88 25K0043_1 HoltGeneralFormat 11 19 25 1521 11/19/25 15:22:11

Project Manager:

EGLE - State Overflow

3350 N Martin Luther King Jr Blvd

Lansing, MI 48906

Flint Bishop Airport Landfill / 2341-7650-81

2341-7650-81

Brian Kuberski Reported: 11/19/2025 15:21

Metiri Group - Holt - 1914 Holloway Dr, Holt, MI 48842

Sample Results

Sample:

25K0043-01 (Water) Sampled: 11/04/25 16:00

Vent #1

Analyte Result PQL

Date

Analyzed Method/Qual Units DF

Prep

Batch

Organochlorine Herbicides

Dalapon ND 5.4 EPA 8151A11/12/25 BEK01435ug/L 1 L-, V+

Dicamba ND 5.4 EPA 8151A11/12/25 BEK01435ug/L 2

Dichlorprop ND 5.4 EPA 8151A11/12/25 BEK01435ug/L 3

2,4-D ND 5.4 EPA 8151A11/12/25 BEK01435ug/L 4 L-

2,4,5-TP ND 5.4 EPA 8151A11/12/25 BEK01435ug/L 5

2,4,5-T ND 5.4 EPA 8151A11/12/25 BEK01435ug/L� 6

2,4-DB ND 5.4 EPA 8151A11/12/25 BEK01435ug/L 7 V-

Dinoseb ND 5.4 EPA 8151A11/12/25 BEK01435ug/L 8 V+

Surrogate: DCAA(S) 113% 10-120 EPA 8151A11/12/25 5

Analyte Result PQL

Date

Analyzed Method/Qual Units DF

Prep

Batch

Base/Neutral/Acid Semivolatiles by GC/MS : EPA 3510/EPA 8270E

1,2,4-Trichlorobenzene ND 5.0 EPA 8270E11/13/25 BEK01781ug/L 1

2,2'-Oxybis(1-chloropropane) ND 5.0 EPA 8270E11/13/25 BEK01781ug/L 2

2,4,5-Trichlorophenol ND 5.0 EPA 8270E11/13/25 BEK01781ug/L 3

2,4,6-Trichlorophenol ND 4.0 EPA 8270E11/13/25 BEK01781ug/L 4

2,4-Dichlorophenol ND 5.0 EPA 8270E11/13/25 BEK01781ug/L 5

2,4-Dimethylphenol ND 5.0 EPA 8270E11/13/25 BEK01781ug/L 6

2,4-Dinitrophenol ND 20 EPA 8270E11/13/25 BEK01781ug/L 7 *, L-, V-

2,4-Dinitrotoluene ND 5.0 EPA 8270E11/13/25 BEK01781ug/L 8

2,6-Dinitrotoluene ND 5.0 EPA 8270E11/13/25 BEK01781ug/L 9

2-Chloronaphthalene ND 5.0 EPA 8270E11/13/25 BEK01781ug/L 10

2-Chlorophenol ND 5.0 EPA 8270E11/13/25 BEK01781ug/L 11

2-Methyl-4,6-dinitrophenol ND 20 EPA 8270E11/13/25 BEK01781ug/L 12

2-Methylnaphthalene ND 5.0 EPA 8270E11/13/25 BEK01781ug/L 13

2-Methylphenol ND 5.0 EPA 8270E11/13/25 BEK01781ug/L 14

2-Nitroaniline ND 20 EPA 8270E11/13/25 BEK01781ug/L 15

2-Nitrophenol ND 5.0 EPA 8270E11/13/25 BEK01781ug/L 16

3&4-Methylphenol ND 10 EPA 8270E11/13/25 BEK01781ug/L 17

3-Nitroaniline ND 20 EPA 8270E11/13/25 BEK01781ug/L 18 V+

4-Bromophenyl Phenylether ND 5.0 EPA 8270E11/13/25 BEK01781ug/L 19

4-Chloro-3-methylphenol ND 5.0 EPA 8270E11/13/25 BEK01781ug/L 20

[TOC_1]Sample Results[TOC]

The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.

No duplication of this report is allowed, except in its entirety.

Page 4 of 88 25K0043_1 HoltGeneralFormat 11 19 25 1521 11/19/25 15:22:11

Project Manager:

EGLE - State Overflow

3350 N Martin Luther King Jr Blvd

Lansing, MI 48906

Flint Bishop Airport Landfill / 2341-7650-81

2341-7650-81

Brian Kuberski Reported: 11/19/2025 15:21

Metiri Group - Holt - 1914 Holloway Dr, Holt, MI 48842

Sample Results

(Continued)

Sample:

25K0043-01 (Water) Sampled: 11/04/25 16:00

Vent #1 (Continued)

Analyte Result PQL

Date

Analyzed Method/Qual Units DF

Prep

Batch

Base/Neutral/Acid Semivolatiles by GC/MS : EPA 3510/EPA 8270E (Continu

4-Chlorophenyl Phenylether ND 5.0 EPA 8270E11/13/25 BEK01781ug/L 21

4-Nitroaniline ND 20 EPA 8270E11/13/25 BEK01781ug/L 22 F+, ICV+, L+, V+

4-Nitrophenol ND 20 EPA 8270E11/13/25 BEK01781ug/L 23 L-

Acenaphthene ND 5.0 EPA 8270E11/13/25 BEK01781ug/L 24

Acenaphthylene ND 5.0 EPA 8270E11/13/25 BEK01781ug/L 25

Aniline ND 4.0 EPA 8270E11/13/25 BEK01781ug/L 26 L+

Anthracene ND 5.0 EPA 8270E11/13/25 BEK01781ug/L 27

Azobenzene ND 5.0 EPA 8270E11/13/25 BEK01781ug/L 28

Benzo(a)anthracene ND 1.0 EPA 8270E11/13/25 BEK01781ug/L 29

Benzo(a)pyrene ND 1.0 EPA 8270E11/13/25 BEK01781ug/L 30

Benzo(b)fluoranthene ND 1.0 EPA 8270E11/13/25 BEK01781ug/L 31

Benzo(ghi)perylene ND 1.0 EPA 8270E11/13/25 BEK01781ug/L 32 V+

Benzo(k)fluoranthene ND 1.0 EPA 8270E11/13/25 BEK01781ug/L 33

Benzyl Alcohol ND 5.0 EPA 8270E11/13/25 BEK01781ug/L 34

Bis(2-chloroethoxy)methane ND 5.0 EPA 8270E11/13/25 BEK01781ug/L 35

Bis(2-chloroethyl)ether ND 1.0 EPA 8270E11/13/25 BEK01781ug/L 36

Bis(2-ethylhexyl)phthalate ND 5.0 EPA 8270E11/13/25 BEK01781ug/L 37

Butyl Benzyl Phthalate ND 5.0 EPA 8270E11/13/25 BEK01781ug/L 38

Carbazole ND 5.0 EPA 8270E11/13/25 BEK01781ug/L 39

Chrysene ND 1.0 EPA 8270E11/13/25 BEK01781ug/L 40 F+, ICV+, L+

Di-n-butyl Phthalate ND 5.0 EPA 8270E11/13/25 BEK01781ug/L 41

Di-n-octyl Phthalate ND 5.0 EPA 8270E11/13/25 BEK01781ug/L 42 L+

Dibenzo(a,h)anthracene ND 2.0 EPA 8270E11/13/25 BEK01781ug/L 43 F+, ICV+, L+, V+

Dibenzofuran ND 4.0 EPA 8270E11/13/25 BEK01781ug/L 44

Diethyl Phthalate ND 5.0 EPA 8270E11/13/25 BEK01781ug/L 45

Dimethyl Phthalate ND 5.0 EPA 8270E11/13/25 BEK01781ug/L 46

Fluoranthene ND 1.0 EPA 8270E11/13/25 BEK01781ug/L 47

Fluorene ND 5.0 EPA 8270E11/13/25 BEK01781ug/L 48

Hexachlorobenzene ND 5.0 EPA 8270E11/13/25 BEK01781ug/L 49

Hexachlorobutadiene ND 5.0 EPA 8270E11/13/25 BEK01781ug/L 50

The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.

No duplication of this report is allowed, except in its entirety.

Page 5 of 88 25K0043_1 HoltGeneralFormat 11 19 25 1521 11/19/25 15:22:11

Project Manager:

EGLE - State Overflow

3350 N Martin Luther King Jr Blvd

Lansing, MI 48906

Flint Bishop Airport Landfill / 2341-7650-81

2341-7650-81

Brian Kuberski Reported: 11/19/2025 15:21

Metiri Group - Holt - 1914 Holloway Dr, Holt, MI 48842

Sample Results

(Continued)

Sample:

25K0043-01 (Water) Sampled: 11/04/25 16:00

Vent #1 (Continued)

Analyte Result PQL

Date

Analyzed Method/Qual Units DF

Prep

Batch

Base/Neutral/Acid Semivolatiles by GC/MS : EPA 3510/EPA 8270E (Continu

Hexachlorocyclopentadiene ND 5.0 EPA 8270E11/13/25 BEK01781ug/L 51 L-

Hexachloroethane ND 5.0 EPA 8270E11/13/25 BEK01781ug/L 52

Indeno(1,2,3-cd)pyrene ND 2.0 EPA 8270E11/13/25 BEK01781ug/L 53 V+

Isophorone ND 5.0 EPA 8270E11/13/25 BEK01781ug/L 54

N-Nitrosodi-n-propylamine ND 5.0 EPA 8270E11/13/25 BEK01781ug/L 55

N-Nitrosodimethylamine ND 5.0 EPA 8270E11/13/25 BEK01781ug/L 56

N-Nitrosodiphenylamine ND 5.0 EPA 8270E11/13/25 BEK01781ug/L 57

Naphthalene ND 5.0 EPA 8270E11/13/25 BEK01781ug/L 58

Nitrobenzene ND 3.0 EPA 8270E11/13/25 BEK01781ug/L� 59

Pentachlorophenol ND 20 EPA 8270E11/13/25 BEK01781ug/L 60

Phenanthrene ND 2.0 EPA 8270E11/13/25 BEK01781ug/L 61

Phenol ND 5.0 EPA 8270E11/13/25 BEK01781ug/L 62 L-

Pyrene ND 5.0 EPA 8270E11/13/25 BEK01781ug/L 63

Pyridine ND 5.0 EPA 8270E11/13/25 BEK01781ug/L 64 B, L-

Internal Standard: 1,4-Dichlorobenzene-d4(I) 1.00% 50-200 EPA 8270E11/13/25 1

Internal Standard: Acenaphthene-d10(I) 1.00% 50-200 EPA 8270E11/13/25 1

Internal Standard: Chrysene-d12(I) 1.00% 50-200 EPA 8270E11/13/25 1

Internal Standard: Naphthalene-d8(I) 1.00% 50-200 EPA 8270E11/13/25 1

Internal Standard: Perylene-d12(I) 1.00% 50-200 EPA 8270E11/13/25 1

Internal Standard: Phenanthrene-d10(I) 1.00% 50-200 EPA 8270E11/13/25 1

Surrogate: 1-Fluoronaphthalene(S) 81.9% 44-103 EPA 8270E11/13/25 1

Surrogate: 2,4,6-Tribromophenol(S) 91.7% 38-138 EPA 8270E11/13/25 1

Surrogate: 2-Fluorobiphenyl(S) 92.7% 44-109 EPA 8270E11/13/25 1

Surrogate: 2-Fluorophenol(S) 47.4% 22-85 EPA 8270E11/13/25 1

Surrogate: 4-Terphenyl-d14(S) 101% 44-124 EPA 8270E11/13/25 1

Surrogate: Phenol-d6(S) 32.5% 11-60 EPA 8270E11/13/25 1

Analyte Result PQL

Date

Analyzed Method/Qual Units DF

Prep

Batch

TCLP Semivolatiles - Prep EPA 1311/3510C

2,4,5-Trichlorophenol ND 0.10 EPA 8270E11/13/25 BEK02081mg/L 1

2,4,6-Trichlorophenol ND 0.10 EPA 8270E11/13/25 BEK02081mg/L 2

2,4-Dinitrotoluene ND 0.025 EPA 8270E11/13/25 BEK02081mg/L 3

2-Methylphenol ND 0.10 EPA 8270E11/13/25 BEK02081mg/L 4

3&4-Methylphenol ND 0.10 EPA 8270E11/13/25 BEK02081mg/L 5

Hexachlorobenzene ND 0.025 EPA 8270E11/13/25 BEK02081mg/L 6

The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.

No duplication of this report is allowed, except in its entirety.

Page 6 of 88 25K0043_1 HoltGeneralFormat 11 19 25 1521 11/19/25 15:22:11

Project Manager:

EGLE - State Overflow

3350 N Martin Luther King Jr Blvd

Lansing, MI 48906

Flint Bishop Airport Landfill / 2341-7650-81

2341-7650-81

Brian Kuberski Reported: 11/19/2025 15:21

Metiri Group - Holt - 1914 Holloway Dr, Holt, MI 48842

Sample Results

(Continued)

Sample:

25K0043-01 (Water) Sampled: 11/04/25 16:00

Vent #1 (Continued)

Analyte Result PQL

Date

Analyzed Method/Qual Units DF

Prep

Batch

TCLP Semivolatiles - Prep EPA 1311/3510C (Continued)

Hexachlorobutadiene ND 0.10 EPA 8270E11/13/25 BEK02081mg/L 7

Hexachloroethane ND 0.10 EPA 8270E11/13/25 BEK02081mg/L 8

Nitrobenzene ND 0.10 EPA 8270E11/13/25 BEK02081mg/L� 9

Pentachlorophenol ND 0.10 EPA 8270E11/13/25 BEK02081mg/L 10

Pyridine ND 0.10 EPA 8270E11/13/25 BEK02081mg/L 11 B, L-

Surrogate: 1-Fluoronaphthalene(S) 76.1% 46-114 EPA 8270E11/13/25 1

Surrogate: 2,4,6-Tribromophenol(S) 114% 25-118 EPA 8270E11/13/25 1

Surrogate: 2-Fluorobiphenyl(S) 86.6% 49-115 EPA 8270E11/13/25 1

Surrogate: 2-Fluorophenol(S) 83.8% 31-112 EPA 8270E11/13/25 1

Surrogate: 4-Terphenyl-d14(S) 101% 48-117 EPA 8270E11/13/25 1

Surrogate: Phenol-d6(S) 81.2% 32-113 EPA 8270E11/13/25 1

Analyte Result PQL

Date

Analyzed Method/Qual Units DF

Prep

Batch

Polychlorinated Biphenyls (PCBs)

AROCLOR 1016 ND 0.16 EPA 8082A11/14/25 BEK02451ug/L 1

AROCLOR 1221 ND 0.16 EPA 8082A11/14/25 BEK02451ug/L 2

AROCLOR 1232 ND 0.16 EPA 8082A11/14/25 BEK02451ug/L 3

AROCLOR 1242 ND 0.16 EPA 8082A11/14/25 BEK02451ug/L 4

AROCLOR 1248 ND 0.16 EPA 8082A11/14/25 BEK02451ug/L 5

AROCLOR 1254 ND 0.16 EPA 8082A11/14/25 BEK02451ug/L 6

AROCLOR 1260 ND 0.16 EPA 8082A11/14/25 BEK02451ug/L 7 L+, V+

AROCLOR 1262 ND 0.16 EPA 8082A11/14/25 BEK02451ug/L 8

AROCLOR 1268 ND 0.16 EPA 8082A11/14/25 BEK02451ug/L 9

Surrogate: Decachlorobiphenyl(S) 88.5% 14-124 EPA 8082A11/14/25 1

Surrogate: 2,4,5,6-Tetrachloro-m-xylene(S) 96.2% 26-136 EPA 8082A11/14/25 1

Analyte Result PQL

Date

Analyzed Method/Qual Units DF

Prep

Batch

Volatile Organic Compounds (VOCs) by GC/MS, 5030C

1,1,1,2-Tetrachloroethane ND 1.0 EPA 8260D11/06/25 BEK00731ug/L 1 J-

1,1,1-Trichloroethane ND 1.0 EPA 8260D11/06/25 BEK00731ug/L 2 J-

1,1,2,2-Tetrachloroethane ND 1.0 EPA 8260D11/06/25 BEK00731ug/L 3 J-

1,1,2-Trichloroethane ND 1.0 EPA 8260D11/06/25 BEK00731ug/L 4 J-

1,1-Dichloroethane ND 1.0 EPA 8260D11/06/25 BEK00731ug/L 5 J-

The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.

No duplication of this report is allowed, except in its entirety.

Page 7 of 88 25K0043_1 HoltGeneralFormat 11 19 25 1521 11/19/25 15:22:11

Project Manager:

EGLE - State Overflow

3350 N Martin Luther King Jr Blvd

Lansing, MI 48906

Flint Bishop Airport Landfill / 2341-7650-81

2341-7650-81

Brian Kuberski Reported: 11/19/2025 15:21

Metiri Group - Holt - 1914 Holloway Dr, Holt, MI 48842

Sample Results

(Continued)

Sample:

25K0043-01 (Water) Sampled: 11/04/25 16:00

Vent #1 (Continued)

Analyte Result PQL

Date

Analyzed Method/Qual Units DF

Prep

Batch

Volatile Organic Compounds (VOCs) by GC/MS, 5030C (Continued)

1,1-Dichloroethene ND 1.0 EPA 8260D11/06/25 BEK00731ug/L 6 J-

1,2,3-Trichloropropane ND 1.0 EPA 8260D11/06/25 BEK00731ug/L 7 J-

1,2,3-Trimethylbenzene 7.5 1.0 EPA 8260D11/06/25 BEK00731ug/L 8 J-

1,2,4-Trichlorobenzene ND 5.0 EPA 8260D11/06/25 BEK00731ug/L 9 J-

1,2,4-Trimethylbenzene 15 1.0 EPA 8260D11/06/25 BEK00731ug/L 10 J-

1,2-Dibromo-3-chloropropane (SIM) ND 1.0 EPA 8260D11/06/25 BEK00731ug/L� 11 J-

1,2-Dichlorobenzene ND 1.0 EPA 8260D11/06/25 BEK00731ug/L 12 J-

1,2-Dichloroethane ND 1.0 EPA 8260D11/06/25 BEK00731ug/L 13 J-

1,2-Dichloropropane ND 1.0 EPA 8260D11/06/25 BEK00731ug/L 14 J-

1,3,5-Trimethylbenzene 4.5 1.0 EPA 8260D11/06/25 BEK00731ug/L 15 J-

1,3-Dichlorobenzene ND 1.0 EPA 8260D11/06/25 BEK00731ug/L 16 J-

1,4-Dichlorobenzene 8.8 1.0 EPA 8260D11/06/25 BEK00731ug/L 17 J-

2-Butanone ND 5.0 EPA 8260D11/06/25 BEK00731ug/L 18 J-, L-

2-Chlorotoluene ND 1.0 EPA 8260D11/06/25 BEK00731ug/L 19 J-

2-Hexanone ND 5.0 EPA 8260D11/06/25 BEK00731ug/L 20 J-

2-Methylnaphthalene ND 10 EPA 8260D11/06/25 BEK00731ug/L 21 *, ICV+, J-, L+, V-

4-Methyl-2-pentanone ND 5.0 EPA 8260D11/06/25 BEK00731ug/L 22 J-

Acetone ND 50 EPA 8260D11/06/25 BEK00731ug/L 23 J-, L-

Acrylonitrile ND 2.0 EPA 8260D11/06/25 BEK00731ug/L 24 J-, V-

Benzene 6.4 1.0 EPA 8260D11/06/25 BEK00731ug/L 25 J-

Bromobenzene ND 1.0 EPA 8260D11/06/25 BEK00731ug/L 26 J-

Bromochloromethane ND 1.0 EPA 8260D11/06/25 BEK00731ug/L 27 J-

Bromodichloromethane ND 1.0 EPA 8260D11/06/25 BEK00731ug/L 28 J-

Bromoform (SIM) ND 1.0 EPA 8260D11/06/25 BEK00731ug/L� 29 J-

Bromomethane ND 5.0 EPA 8260D11/06/25 BEK00731ug/L 30 J-

Carbon Disulfide ND 1.0 EPA 8260D11/06/25 BEK00731ug/L 31 J-, L+, V+

Carbon Tetrachloride ND 1.0 EPA 8260D11/06/25 BEK00731ug/L 32 J-, JS, L-, V-

Chlorobenzene ND 1.0 EPA 8260D11/06/25 BEK00731ug/L 33 J-

Chloroethane ND 5.0 EPA 8260D11/06/25 BEK00731ug/L 34 J-, V+

Chloroform ND 1.0 EPA 8260D11/06/25 BEK00731ug/L 35 J-

Chloromethane ND 5.0 EPA 8260D11/06/25 BEK00731ug/L 36 J-, V-cis-1,2-Dichloroethene ND 1.0 EPA 8260D11/06/25 BEK00731ug/L 37 J-

The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.

No duplication of this report is allowed, except in its entirety.

Page 8 of 88 25K0043_1 HoltGeneralFormat 11 19 25 1521 11/19/25 15:22:11

Project Manager:

EGLE - State Overflow

3350 N Martin Luther King Jr Blvd

Lansing, MI 48906

Flint Bishop Airport Landfill / 2341-7650-81

2341-7650-81

Brian Kuberski Reported: 11/19/2025 15:21

Metiri Group - Holt - 1914 Holloway Dr, Holt, MI 48842

Sample Results

(Continued)

Sample:

25K0043-01 (Water) Sampled: 11/04/25 16:00

Vent #1 (Continued)

Analyte Result PQL

Date

Analyzed Method/Qual Units DF

Prep

Batch

Volatile Organic Compounds (VOCs) by GC/MS, 5030C (Continued) cis-1,3-Dichloropropene ND 0.50 EPA 8260D11/06/25 BEK00731ug/L 38 J-

Dibromochloromethane ND 1.0 EPA 8260D11/06/25 BEK00731ug/L 39 J-

Dibromomethane ND 1.0 EPA 8260D11/06/25 BEK00731ug/L 40 J-

Dichlorodifluoromethane ND 5.0 EPA 8260D11/06/25 BEK00731ug/L 41 J-

Ethylbenzene ND 1.0 EPA 8260D11/06/25 BEK00731ug/L 42 J-

Ethylene Dibromide ND 1.0 EPA 8260D11/06/25 BEK00731ug/L� 43 J-

Isopropylbenzene 1.9 1.0 EPA 8260D11/06/25 BEK00731ug/L 44 J-m&p-Xylene 22 2.0 EPA 8260D11/06/25 BEK00731ug/L 45 J-

Methylene Chloride ND 5.0 EPA 8260D11/06/25 BEK00731ug/L 46 J-

MTBE ND 1.0 EPA 8260D11/06/25 BEK00731ug/L 47 J-

Naphthalene 8.2 5.0 EPA 8260D11/06/25 BEK00731ug/L 48 J-, V-n-Butylbenzene ND 1.0 EPA 8260D11/06/25 BEK00731ug/L 49 J-n-Propylbenzene 1.9 1.0 EPA 8260D11/06/25 BEK00731ug/L 50 J-o-Xylene ND 1.0 EPA 8260D11/06/25 BEK00731ug/L� 51 J-sec-Butylbenzene ND 1.0 EPA 8260D11/06/25 BEK00731ug/L 52 J-

Styrene ND 1.0 EPA 8260D11/06/25 BEK00731ug/L 53 J-tert-Butylbenzene ND 1.0 EPA 8260D11/06/25 BEK00731ug/L 54 J-

Tetrachloroethene ND 1.0 EPA 8260D11/06/25 BEK00731ug/L 55 J-

Toluene ND 1.0 EPA 8260D11/06/25 BEK00731ug/L 56 J-trans-1,2-Dichloroethene ND 1.0 EPA 8260D11/06/25 BEK00731ug/L 57 J-trans-1,3-Dichloropropene ND 0.50 EPA 8260D11/06/25 BEK00731ug/L 58 J-

Trichloroethene ND 1.0 EPA 8260D11/06/25 BEK00731ug/L 59 J-

Trichlorofluoromethane ND 1.0 EPA 8260D11/06/25 BEK00731ug/L 60 J-, V+

Vinyl Chloride ND 1.0 EPA 8260D11/06/25 BEK00731ug/L 61 J-

Xylenes 22 3.0 EPA 8260D11/06/25 BEK00731ug/L 62 J-

Surrogate: 1,2-Dichloroethane-d4(S) 86.2% 80-120 EPA 8260D11/06/25J- 1

Surrogate: 4-Bromofluorobenzene(S) 96.0% 80-120 EPA 8260D11/06/25J- 1

Surrogate: Dibromofluoromethane(S) 90.0% 80-120 EPA 8260D11/06/25J- 1

Surrogate: Toluene-d8(S) 100% 80-120 EPA 8260D11/06/25J- 1

Analyte Result PQL

Date

Analyzed Method/Qual Units DF

Prep

Batch

TCLP Volatiles - Prep EPA 1311/5030B

Tumble Date 11/7/25 EPA 8260C

TCLP

11/07/25 BEK01191[blank] 1

The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.

No duplication of this report is allowed, except in its entirety.

Page 9 of 88 25K0043_1 HoltGeneralFormat 11 19 25 1521 11/19/25 15:22:11

Project Manager:

EGLE - State Overflow

3350 N Martin Luther King Jr Blvd

Lansing, MI 48906

Flint Bishop Airport Landfill / 2341-7650-81

2341-7650-81

Brian Kuberski Reported: 11/19/2025 15:21

Metiri Group - Holt - 1914 Holloway Dr, Holt, MI 48842

Sample Results

(Continued)

Sample:

25K0043-01 (Water) Sampled: 11/04/25 16:00

Vent #1 (Continued)

Analyte Result PQL

Date

Analyzed Method/Qual Units DF

Prep

Batch

TCLP Volatiles - Prep EPA 1311/5030B (Continued)

1,1-Dichloroethene ND 0.14 EPA 8260D11/14/25 BEK023720mg/L 1

1,2-Dichloroethane ND 0.10 EPA 8260D11/14/25 BEK023720mg/L 2

1,4-Dichlorobenzene ND 1.5 EPA 8260D11/14/25 BEK023720mg/L 3

2-Butanone ND 40 EPA 8260D11/14/25 BEK023720mg/L 4

Benzene ND 0.10 EPA 8260D11/14/25 BEK023720mg/L 5

Carbon Tetrachloride ND 0.10 EPA 8260D11/14/25 BEK023720mg/L 6

Chlorobenzene ND 20 EPA 8260D11/14/25 BEK023720mg/L 7

Chloroform ND 1.2 EPA 8260D11/14/25 BEK023720mg/L 8

Tetrachloroethene ND 0.14 EPA 8260D11/14/25 BEK023720mg/L 9

Trichloroethene ND 0.10 EPA 8260D11/14/25 BEK023720mg/L 10

Vinyl Chloride ND 0.040 EPA 8260D11/14/25 BEK023720mg/L 11 F+, L+, V+

Surrogate: Dibromofluoromethane(S) 97% 80-120 EPA 8260D11/14/25 20

Surrogate: Toluene-d8(S) 104% 80-120 EPA 8260D11/14/25 20

Surrogate: 1,2-Dichloroethane-d4(S) 104% 80-120 EPA 8260D11/14/25 20

Surrogate: 4-Bromofluorobenzene(S) 103% 80-120 EPA 8260D11/14/25 20

Analyte Result PQL

Date

Analyzed Method/Qual Units DF

Prep

Batch

Per- and Polyfluoroalkyl Substances (EPA 1633)

PFBA ND 3.2 EPA 163311/15/25 BEK02391ng/L 1

PFPeA 65 1.6 EPA 163311/15/25 BEK02391ng/L 2

PFHxA 120 0.80 EPA 163311/15/25 BEK02391ng/L 3

PFHpA 56 0.80 EPA 163311/15/25 BEK02391ng/L 4

PFOA 150 0.80 EPA 163311/15/25 BEK02391ng/L 5

PFNA 14 0.80 EPA 163311/15/25 BEK02391ng/L 6 V+

PFDA ND 0.80 EPA 163311/15/25 BEK02391ng/L 7

PFUnA ND 0.80 EPA 163311/15/25 BEK02391ng/L 8

PFDoA ND 0.80 EPA 163311/15/25 BEK02391ng/L 9

PFTrDA ND 0.80 EPA 163311/15/25 BEK02391ng/L 10

PFTeDA ND 0.80 EPA 163311/15/25 BEK02391ng/L 11

PFBS 35 0.80 EPA 163311/15/25 BEK02391ng/L 12

PFPeS 20 0.80 EPA 163311/15/25 BEK02391ng/L 13

PFHxS 56 0.80 EPA 163311/15/25 BEK02391ng/L 14

PFHpS 5.5 0.80 EPA 163311/15/25 BEK02391ng/L 15

The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.

No duplication of this report is allowed, except in its entirety.

Page 10 of 88 25K0043_1 HoltGeneralFormat 11 19 25 1521 11/19/25 15:22:11

Project Manager:

EGLE - State Overflow

3350 N Martin Luther King Jr Blvd

Lansing, MI 48906

Flint Bishop Airport Landfill / 2341-7650-81

2341-7650-81

Brian Kuberski Reported: 11/19/2025 15:21

Metiri Group - Holt - 1914 Holloway Dr, Holt, MI 48842

Sample Results

(Continued)

Sample:

25K0043-01 (Water) Sampled: 11/04/25 16:00

Vent #1 (Continued)

Analyte Result PQL

Date

Analyzed Method/Qual Units DF

Prep

Batch

Per- and Polyfluoroalkyl Substances (EPA 1633) (Continued)

PFOS 110 0.80 EPA 163311/15/25 BEK02391ng/L 16

PFNS ND 0.80 EPA 163311/15/25 BEK02391ng/L 17

PFDS ND 0.80 EPA 163311/15/25 BEK02391ng/L 18

PFDoS ND 0.80 EPA 163311/15/25 BEK02391ng/L 19

4:2FTS ND 3.2 EPA 163311/15/25 BEK02391ng/L 20 EIS+

6:2FTS ND 3.2 EPA 163311/15/25 BEK02391ng/L 21 EIS+, V+

8:2FTS ND 3.2 EPA 163311/15/25 BEK02391ng/L 22

PFOSA ND 0.80 EPA 163311/15/25 BEK02391ng/L 23

NMeFOSA ND 0.80 EPA 163311/15/25 BEK02391ng/L 24

NEtFOSA ND 0.80 EPA 163311/15/25 BEK02391ng/L 25

NMeFOSAA 2.5 0.80 EPA 163311/15/25 BEK02391ng/L 26

NEtFOSAA 51 0.80 EPA 163311/15/25 BEK02391ng/L 27

NMeFOSE ND 8.0 EPA 163311/15/25 BEK02391ng/L 28

NEtFOSE 21 8.0 EPA 163311/15/25 BEK02391ng/L 29

HFPO-DA ND 3.2 EPA 163311/15/25 BEK02391ng/L 30

ADONA ND 3.2 EPA 163311/15/25 BEK02391ng/L 31

PFEESA ND 1.6 EPA 163311/15/25 BEK02391ng/L 32

PFMPA 13 1.6 EPA 163311/15/25 BEK02391ng/L 33

PFMBA 2.8 1.6 EPA 163311/15/25 BEK02391ng/L 34

NFDHA ND 1.6 EPA 163311/15/25 BEK02391ng/L 35

9Cl-PF3ONS ND 3.2 EPA 163311/15/25 BEK02391ng/L 36

11Cl-PF3OUDS ND 3.2 EPA 163311/15/25 BEK02391ng/L 37

3:3FTCA 27 4.0 EPA 163311/15/25 BEK02391ng/L 38

5:3FTCA 72 20 EPA 163311/15/25 BEK02391ng/L 39

7:3FTCA ND 20 EPA 163311/15/25 BEK02391ng/L 40

PFOS (Estimated Linear) 0.0 EPA 163311/15/25 BEK02391ng/L 41

PFOS (Estimated Branched) 0.0 EPA 163311/15/25 BEK02391ng/L 42

PFHxS (Estimated Linear) 0.0 EPA 163311/15/25 BEK02391ng/L 43

PFHxS (Estimated Branched) 0.0 EPA 163311/15/25 BEK02391ng/L 44

Extracted Internal Standards (EIS): 13C4-PFBA 35% 5-130 EPA 163311/15/25 1

Extracted Internal Standards (EIS): 13C5-PFPEA 51% 40-130 EPA 163311/15/25 1

Extracted Internal Standards (EIS): 13C5-PFHXA 54% 40-130 EPA 163311/15/25 1

Extracted Internal Standards (EIS): 13C4-PFHPA 75% 40-130 EPA 163311/15/25 1

The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.

No duplication of this report is allowed, except in its entirety.

Page 11 of 88 25K0043_1 HoltGeneralFormat 11 19 25 1521 11/19/25 15:22:11

Project Manager:

EGLE - State Overflow

3350 N Martin Luther King Jr Blvd

Lansing, MI 48906

Flint Bishop Airport Landfill / 2341-7650-81

2341-7650-81

Brian Kuberski Reported: 11/19/2025 15:21

Metiri Group - Holt - 1914 Holloway Dr, Holt, MI 48842

Sample Results

(Continued)

Sample:

25K0043-01 (Water) Sampled: 11/04/25 16:00

Vent #1 (Continued)

Analyte Result PQL

Date

Analyzed Method/Qual Units DF

Prep

Batch

Per- and Polyfluoroalkyl Substances (EPA 1633) (Continued)

Extracted Internal Standards (EIS): 13C8-PFOA 63% 40-130 EPA 163311/15/25 1

Extracted Internal Standards (EIS): 13C9-PFNA 57% 40-130 EPA 163311/15/25 1

Extracted Internal Standards (EIS): 13C6-PFDA 74% 40-130 EPA 163311/15/25 1

Extracted Internal Standards (EIS): 13C7-PFUnA 55% 30-130 EPA 163311/15/25 1

Extracted Internal Standards (EIS): 13C2-PFDOA 44% 10-130 EPA 163311/15/25 1

Extracted Internal Standards (EIS): 13C2-PFTEDA 36% 10-130 EPA 163311/15/25 1

Extracted Internal Standards (EIS): 13C3-PFBS 40% 40-135 EPA 163311/15/25 1

Extracted Internal Standards (EIS): 13C3-PFHXS 44% 40-130 EPA 163311/15/25 1

Extracted Internal Standards (EIS): 13C8-PFOS 45% 40-130 EPA 163311/15/25 1

Extracted Internal Standards (EIS): 13C2-4:2FTS 219% 40-200 EPA 163311/15/25EIS+ 1

Extracted Internal Standards (EIS): 13C2-6:2FTS 236% 40-200 EPA 163311/15/25EIS+ 1

Extracted Internal Standards (EIS): 13C2-8:2FTS 160% 40-300 EPA 163311/15/25 1

Extracted Internal Standards (EIS): 13C8-PFOSA 126% 40-130 EPA 163311/15/25 1

Extracted Internal Standards (EIS): D3-NMEFOSA 38% 10-130 EPA 163311/15/25 1

Extracted Internal Standards (EIS): D5-NETFOSA 33% 10-130 EPA 163311/15/25 1

Extracted Internal Standards (EIS): D3-NMEFOSAA 86% 40-170 EPA 163311/15/25 1

Extracted Internal Standards (EIS): D5-NETFOSAA 68% 25-135 EPA 163311/15/25 1

Extracted Internal Standards (EIS): D7-NMEFOSE 78% 10-130 EPA 163311/15/25 1

Extracted Internal Standards (EIS): D9-NETFOSE 72% 10-130 EPA 163311/15/25 1

Extracted Internal Standards (EIS): 13C3-HFPO-DA 69% 40-130 EPA 163311/15/25 1

Analyte Result PQL

Date

Analyzed Method/Qual Units DF

Prep

Batch

TCLP (EPA 1311) Per- and Polyfluoroalkyl Substances

PFBA 110 1.7 EPA 163311/15/25 BEK02391ng/L� 1

PFPeA 34 0.85 EPA 163311/15/25 BEK02391ng/L� 2

PFHxA 120 0.43 EPA 163311/15/25 BEK02391ng/L� 3

PFHpA 52 0.43 EPA 163311/15/25 BEK02391ng/L� 4 EIS+

PFOA 140 0.43 EPA 163311/15/25 BEK02391ng/L� 5 E

PFNA 12 0.43 EPA 163311/15/25 BEK02391ng/L� 6 V+

PFDA ND 0.43 EPA 163311/15/25 BEK02391ng/L� 7

PFUnA ND 0.43 EPA 163311/15/25 BEK02391ng/L� 8

PFDoA ND 0.43 EPA 163311/15/25 BEK02391ng/L� 9

PFTrDA ND 0.43 EPA 163311/15/25 BEK02391ng/L� 10

PFTeDA ND 0.43 EPA 163311/15/25 BEK02391ng/L� 11

PFBS 39 0.43 EPA 163311/15/25 BEK02391ng/L� 12

PFPeS 15 0.43 EPA 163311/15/25 BEK02391ng/L� 13

PFHxS 54 0.43 EPA 163311/15/25 BEK02391ng/L� 14

PFHpS 4.6 0.43 EPA 163311/15/25 BEK02391ng/L� 15

PFOS 100 0.43 EPA 163311/15/25 BEK02391ng/L� 16

The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.

No duplication of this report is allowed, except in its entirety.

Page 12 of 88 25K0043_1 HoltGeneralFormat 11 19 25 1521 11/19/25 15:22:11

Project Manager:

EGLE - State Overflow

3350 N Martin Luther King Jr Blvd

Lansing, MI 48906

Flint Bishop Airport Landfill / 2341-7650-81

2341-7650-81

Brian Kuberski Reported: 11/19/2025 15:21

Metiri Group - Holt - 1914 Holloway Dr, Holt, MI 48842

Sample Results

(Continued)

Sample:

25K0043-01 (Water) Sampled: 11/04/25 16:00

Vent #1 (Continued)

Analyte Result PQL

Date

Analyzed Method/Qual Units DF

Prep

Batch

TCLP (EPA 1311) Per- and Polyfluoroalkyl Substances (Continued)

PFNS ND 0.43 EPA 163311/15/25 BEK02391ng/L� 17

PFDS ND 0.43 EPA 163311/15/25 BEK02391ng/L� 18

PFDoS ND 0.43 EPA 163311/15/25 BEK02391ng/L� 19

4:2FTS ND 1.7 EPA 163311/15/25 BEK02391ng/L� 20

6:2FTS ND 1.7 EPA 163311/15/25 BEK02391ng/L� 21 EIS+, V+

8:2FTS ND 1.7 EPA 163311/15/25 BEK02391ng/L� 22 EIS+

PFOSA ND 0.43 EPA 163311/15/25 BEK02391ng/L� 23

NMeFOSA ND 0.43 EPA 163311/15/25 BEK02391ng/L� 24

NEtFOSA ND 0.43 EPA 163311/15/25 BEK02391ng/L� 25

NMeFOSAA 1.7 0.43 EPA 163311/15/25 BEK02391ng/L� 26 EIS+

NEtFOSAA 38 0.43 EPA 163311/15/25 BEK02391ng/L� 27 EIS+

NMeFOSE ND 4.3 EPA 163311/15/25 BEK02391ng/L� 28

NEtFOSE 6.7 4.3 EPA 163311/15/25 BEK02391ng/L� 29

HFPO-DA ND 1.7 EPA 163311/15/25 BEK02391ng/L� 30

ADONA ND 1.7 EPA 163311/15/25 BEK02391ng/L� 31

PFEESA ND 0.85 EPA 163311/15/25 BEK02391ng/L� 32

PFMPA 5.8 0.85 EPA 163311/15/25 BEK02391ng/L� 33

PFMBA 3.8 0.85 EPA 163311/15/25 BEK02391ng/L� 34

NFDHA ND 0.85 EPA 163311/15/25 BEK02391ng/L� 35

9Cl-PF3ONS ND 1.7 EPA 163311/15/25 BEK02391ng/L� 36

11Cl-PF3OUDS ND 1.7 EPA 163311/15/25 BEK02391ng/L� 37

3:3FTCA ND 2.1 EPA 163311/15/25 BEK02391ng/L� 38

5:3FTCA 53 11 EPA 163311/15/25 BEK02391ng/L� 39

7:3FTCA ND 11 EPA 163311/15/25 BEK02391ng/L� 40

Surrogate: 13C4-PFBA 15% 10-130 EPA 163311/15/25 1

Surrogate: 13C5-PFPEA 62% 40-130 EPA 163311/15/25 1

Surrogate: 13C5-PFHXA 96% 40-130 EPA 163311/15/25 1

Surrogate: 13C4-PFHPA 147% 40-130 EPA 163311/15/25EIS+ 1

Surrogate: 13C8-PFOA 112% 40-130 EPA 163311/15/25 1

Surrogate: 13C9-PFNA 102% 40-130 EPA 163311/15/25 1

Surrogate: 13C6-PFDA 116% 40-130 EPA 163311/15/25 1

Surrogate: 13C7-PFUnA 98% 30-130 EPA 163311/15/25 1

Surrogate: 13C2-PFDOA 88% 10-130 EPA 163311/15/25 1

Surrogate: 13C2-PFTEDA 46% 10-130 EPA 163311/15/25 1

Surrogate: 13C3-PFBS 76% 40-135 EPA 163311/15/25 1

The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.

No duplication of this report is allowed, except in its entirety.

Page 13 of 88 25K0043_1 HoltGeneralFormat 11 19 25 1521 11/19/25 15:22:11

Project Manager:

EGLE - State Overflow

3350 N Martin Luther King Jr Blvd

Lansing, MI 48906

Flint Bishop Airport Landfill / 2341-7650-81

2341-7650-81

Brian Kuberski Reported: 11/19/2025 15:21

Metiri Group - Holt - 1914 Holloway Dr, Holt, MI 48842

Sample Results

(Continued)

Sample:

25K0043-01 (Water) Sampled: 11/04/25 16:00

Vent #1 (Continued)

Analyte Result PQL

Date

Analyzed Method/Qual Units DF

Prep

Batch

TCLP (EPA 1311) Per- and Polyfluoroalkyl Substances (Continued)

Surrogate: 13C3-PFHXS 120% 40-130 EPA 163311/15/25 1

Surrogate: 13C8-PFOS 114% 40-130 EPA 163311/15/25 1

Surrogate: 13C2-4:2FTS 187% 40-200 EPA 163311/15/25 1

Surrogate: 13C2-6:2FTS 318% 40-200 EPA 163311/15/25EIS+ 1

Surrogate: 13C2-8:2FTS 377% 40-300 EPA 163311/15/25EIS+ 1

Surrogate: 13C8-PFOSA 120% 40-130 EPA 163311/15/25 1

Surrogate: D3-NMEFOSA 58% 10-130 EPA 163311/15/25 1

Surrogate: D5-NETFOSA 54% 10-130 EPA 163311/15/25 1

Surrogate: D3-NMEFOSAA 192% 40-170 EPA 163311/15/25EIS+ 1

Surrogate: D5-NETFOSAA 209% 25-135 EPA 163311/15/25EIS+ 1

Surrogate: D7-NMEFOSE 79% 10-130 EPA 163311/15/25 1

Surrogate: D9-NETFOSE 75% 10-130 EPA 163311/15/25 1

Surrogate: 13C3-HFPO-DA 125% 40-130 EPA 163311/15/25 1

Analyte Result PQL

Date

Analyzed Method/Qual Units DF

Prep

Batch

Metals

Mercury 0.057 0.025 EPA 7470A11/11/25 BEK01531ug/L 1

Analyte Result PQL

Date

Analyzed Method/Qual Units DF

Prep

Batch

TCLP Metals - Prep EPA 1311

Mercury ND 0.050 EPA 7470A11/11/25 BEK01531mg/L 1

Analyte Result PQL

Date

Analyzed Method/Qual Units DF

Prep

Batch

Wet Chemistry

PH 6.9 1.0 EPA 9040C11/07/25 BEK00961N/A 1 H

Temperature C 23 1.0 EPA 9040C11/07/25 BEK00961 2 H

Cyanide, Reactive ND 5.0 ASTM

D7511-12

11/06/25 BEK00791ug/kg� 1

IGNITABILITY >207 SW-846 101011/07/25 BEK01001Deg F 1

Sulfide, Reactive ND 6.6 HACH 813111/07/25 BEK01101mg/L� 1

Analyte Result PQL

Date

Analyzed Method/Qual Units DF

Prep

Batch

TCLP Extraction

Tumble Date 11/6/25 EPA 131111/06/25 BEK00861[blank]� 1

The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.

No duplication of this report is allowed, except in its entirety.

Page 14 of 88 25K0043_1 HoltGeneralFormat 11 19 25 1521 11/19/25 15:22:11

Project Manager:

EGLE - State Overflow

3350 N Martin Luther King Jr Blvd

Lansing, MI 48906

Flint Bishop Airport Landfill / 2341-7650-81

2341-7650-81

Brian Kuberski Reported: 11/19/2025 15:21

Metiri Group - Holt - 1914 Holloway Dr, Holt, MI 48842

Sample Results

(Continued)

Sample:

25K0043-02 (Water) Sampled: 11/04/25 17:00

Comp-01

Analyte Result PQL

Date

Analyzed Method/Qual Units DF

Prep

Batch

TCLP Semivolatiles - Prep EPA 1311/3510C

2,4,5-Trichlorophenol ND 0.10 EPA 8270E11/13/25 BEK02081mg/L 1

2,4,6-Trichlorophenol ND 0.10 EPA 8270E11/13/25 BEK02081mg/L 2

2,4-Dinitrotoluene ND 0.025 EPA 8270E11/13/25 BEK02081mg/L 3

2-Methylphenol ND 0.10 EPA 8270E11/13/25 BEK02081mg/L 4

3&4-Methylphenol ND 0.10 EPA 8270E11/13/25 BEK02081mg/L 5

Hexachlorobenzene ND 0.025 EPA 8270E11/13/25 BEK02081mg/L 6

Hexachlorobutadiene ND 0.10 EPA 8270E11/13/25 BEK02081mg/L 7

Hexachloroethane ND 0.10 EPA 8270E11/13/25 BEK02081mg/L 8

Nitrobenzene ND 0.10 EPA 8270E11/13/25 BEK02081mg/L� 9

Pentachlorophenol ND 0.10 EPA 8270E11/13/25 BEK02081mg/L 10

Pyridine ND 0.10 EPA 8270E11/13/25 BEK02081mg/L 11 B, L-

Surrogate: 1-Fluoronaphthalene(S) 76.1% 46-114 EPA 8270E11/13/25 1

Surrogate: 2,4,6-Tribromophenol(S) 110% 25-118 EPA 8270E11/13/25 1

Surrogate: 2-Fluorobiphenyl(S) 86.5% 49-115 EPA 8270E11/13/25 1

Surrogate: 2-Fluorophenol(S) 75.6% 31-112 EPA 8270E11/13/25 1

Surrogate: 4-Terphenyl-d14(S) 99.4% 48-117 EPA 8270E11/13/25 1

Surrogate: Phenol-d6(S) 63.6% 32-113 EPA 8270E11/13/25 1

Analyte Result PQL

Date

Analyzed Method/Qual Units DF

Prep

Batch

TCLP Volatiles - Prep EPA 1311/5030B

Tumble Date 11/11/25 EPA 8260C

TCLP

11/11/25 BEK01511[blank] 1

1,1-Dichloroethene ND 0.14 EPA 8260D11/14/25 BEK023720mg/L 1

1,2-Dichloroethane ND 0.10 EPA 8260D11/14/25 BEK023720mg/L 2

1,4-Dichlorobenzene ND 1.5 EPA 8260D11/14/25 BEK023720mg/L 3

2-Butanone ND 40 EPA 8260D11/14/25 BEK023720mg/L 4

Benzene ND 0.10 EPA 8260D11/14/25 BEK023720mg/L 5

Carbon Tetrachloride ND 0.10 EPA 8260D11/14/25 BEK023720mg/L 6

Chlorobenzene ND 20 EPA 8260D11/14/25 BEK023720mg/L 7

Chloroform ND 1.2 EPA 8260D11/14/25 BEK023720mg/L 8

Tetrachloroethene ND 0.14 EPA 8260D11/14/25 BEK023720mg/L 9

Trichloroethene ND 0.10 EPA 8260D11/14/25 BEK023720mg/L 10

Vinyl Chloride ND 0.040 EPA 8260D11/14/25 BEK023720mg/L 11 F+, L+, V+

The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.

No duplication of this report is allowed, except in its entirety.

Page 15 of 88 25K0043_1 HoltGeneralFormat 11 19 25 1521 11/19/25 15:22:11

Project Manager:

EGLE - State Overflow

3350 N Martin Luther King Jr Blvd

Lansing, MI 48906

Flint Bishop Airport Landfill / 2341-7650-81

2341-7650-81

Brian Kuberski Reported: 11/19/2025 15:21

Metiri Group - Holt - 1914 Holloway Dr, Holt, MI 48842

Sample Results

(Continued)

Sample:

25K0043-02 (Water) Sampled: 11/04/25 17:00

Comp-01 (Continued)

Analyte Result PQL

Date

Analyzed Method/Qual Units DF

Prep

Batch

TCLP Volatiles - Prep EPA 1311/5030B (Continued)

Surrogate: Dibromofluoromethane(S) 99% 80-120 EPA 8260D11/14/25 20

Surrogate: Toluene-d8(S) 103% 80-120 EPA 8260D11/14/25 20

Surrogate: 1,2-Dichloroethane-d4(S) 106% 80-120 EPA 8260D11/14/25 20

Surrogate: 4-Bromofluorobenzene(S) 104% 80-120 EPA 8260D11/14/25 20

Analyte Result PQL

Date

Analyzed Method/Qual Units DF

Prep

Batch

TCLP (EPA 1311) Per- and Polyfluoroalkyl Substances

PFBA ND 1.7 EPA 163311/15/25 BEK02391ng/L� 1

PFPeA 17 0.83 EPA 163311/15/25 BEK02391ng/L� 2

PFHxA 49 0.42 EPA 163311/15/25 BEK02391ng/L� 3

PFHpA 23 0.42 EPA 163311/15/25 BEK02391ng/L� 4 EIS+

PFOA 81 0.42 EPA 163311/15/25 BEK02391ng/L� 5

PFNA 23 0.42 EPA 163311/15/25 BEK02391ng/L� 6 V+

PFDA 1.1 0.42 EPA 163311/15/25 BEK02391ng/L� 7

PFUnA ND 0.42 EPA 163311/15/25 BEK02391ng/L� 8

PFDoA ND 0.42 EPA 163311/15/25 BEK02391ng/L� 9

PFTrDA ND 0.42 EPA 163311/15/25 BEK02391ng/L� 10

PFTeDA ND 0.42 EPA 163311/15/25 BEK02391ng/L� 11

PFBS 29 0.42 EPA 163311/15/25 BEK02391ng/L� 12

PFPeS 22 0.42 EPA 163311/15/25 BEK02391ng/L� 13

PFHxS 95 0.42 EPA 163311/15/25 BEK02391ng/L� 14

PFHpS 5.1 0.42 EPA 163311/15/25 BEK02391ng/L� 15

PFOS 170 4.2 EPA 163311/15/25 BEK023910ng/L� 16

PFNS ND 0.42 EPA 163311/15/25 BEK02391ng/L� 17

PFDS ND 0.42 EPA 163311/15/25 BEK02391ng/L� 18

PFDoS ND 0.42 EPA 163311/15/25 BEK02391ng/L� 19

4:2FTS ND 1.7 EPA 163311/15/25 BEK02391ng/L� 20 EIS+

6:2FTS ND 17 EPA 163311/15/25 BEK023910ng/L� 21 V+

8:2FTS ND 17 EPA 163311/15/25 BEK023910ng/L� 22

PFOSA 0.43 0.42 EPA 163311/15/25 BEK02391ng/L� 23

NMeFOSA ND 0.42 EPA 163311/15/25 BEK02391ng/L� 24

NEtFOSA ND 0.42 EPA 163311/15/25 BEK02391ng/L� 25

NMeFOSAA 2.4 0.42 EPA 163311/15/25 BEK02391ng/L� 26 EIS+

NEtFOSAA 26 0.42 EPA 163311/15/25 BEK02391ng/L� 27 EIS+

The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.

No duplication of this report is allowed, except in its entirety.

Page 16 of 88 25K0043_1 HoltGeneralFormat 11 19 25 1521 11/19/25 15:22:11

Project Manager:

EGLE - State Overflow

3350 N Martin Luther King Jr Blvd

Lansing, MI 48906

Flint Bishop Airport Landfill / 2341-7650-81

2341-7650-81

Brian Kuberski Reported: 11/19/2025 15:21

Metiri Group - Holt - 1914 Holloway Dr, Holt, MI 48842

Sample Results

(Continued)

Sample:

25K0043-02 (Water) Sampled: 11/04/25 17:00

Comp-01 (Continued)

Analyte Result PQL

Date

Analyzed Method/Qual Units DF

Prep

Batch

TCLP (EPA 1311) Per- and Polyfluoroalkyl Substances (Continued)

NMeFOSE ND 4.2 EPA 163311/15/25 BEK02391ng/L� 28

NEtFOSE ND 4.2 EPA 163311/15/25 BEK02391ng/L� 29

HFPO-DA ND 1.7 EPA 163311/15/25 BEK02391ng/L� 30

ADONA ND 1.7 EPA 163311/15/25 BEK02391ng/L� 31

PFEESA ND 0.83 EPA 163311/15/25 BEK02391ng/L� 32

PFMPA ND 0.83 EPA 163311/15/25 BEK02391ng/L� 33

PFMBA ND 0.83 EPA 163311/15/25 BEK02391ng/L� 34

NFDHA ND 0.83 EPA 163311/15/25 BEK02391ng/L� 35

9Cl-PF3ONS ND 1.7 EPA 163311/15/25 BEK02391ng/L� 36

11Cl-PF3OUDS ND 1.7 EPA 163311/15/25 BEK02391ng/L� 37

3:3FTCA 7.6 2.1 EPA 163311/15/25 BEK02391ng/L� 38

5:3FTCA 17 10 EPA 163311/15/25 BEK02391ng/L� 39

7:3FTCA ND 10 EPA 163311/15/25 BEK02391ng/L� 40

Surrogate: 13C4-PFBA 38% 10-130 EPA 163311/15/25 1

Surrogate: 13C5-PFPEA 72% 40-130 EPA 163311/15/25 1

Surrogate: 13C5-PFHXA 95% 40-130 EPA 163311/15/25 1

Surrogate: 13C4-PFHPA 133% 40-130 EPA 163311/15/25EIS+ 1

Surrogate: 13C8-PFOA 107% 40-130 EPA 163311/15/25 1

Surrogate: 13C9-PFNA 105% 40-130 EPA 163311/15/25 1

Surrogate: 13C6-PFDA 121% 40-130 EPA 163311/15/25 1

Surrogate: 13C7-PFUnA 98% 30-130 EPA 163311/15/25 1

Surrogate: 13C2-PFDOA 95% 10-130 EPA 163311/15/25 1

Surrogate: 13C2-PFTEDA 83% 10-130 EPA 163311/15/25 1

Surrogate: 13C3-PFBS 101% 40-135 EPA 163311/15/25 1

Surrogate: 13C3-PFHXS 113% 40-130 EPA 163311/15/25 1

Surrogate: 13C8-PFOS 115% 40-130 EPA 163311/15/25 1

Surrogate: 13C8-PFOS 121% 40-130 EPA 163311/15/25 10

Surrogate: 13C2-4:2FTS 252% 40-200 EPA 163311/15/25EIS+ 1

Surrogate: 13C2-6:2FTS 124% 40-200 EPA 163311/15/25 10

Surrogate: 13C2-8:2FTS 114% 40-300 EPA 163311/15/25 10

Surrogate: 13C8-PFOSA 120% 40-130 EPA 163311/15/25 1

Surrogate: D3-NMEFOSA 58% 10-130 EPA 163311/15/25 1

Surrogate: D5-NETFOSA 59% 10-130 EPA 163311/15/25 1

Surrogate: D3-NMEFOSAA 213% 40-170 EPA 163311/15/25EIS+ 1

Surrogate: D5-NETFOSAA 206% 25-135 EPA 163311/15/25EIS+ 1

Surrogate: D7-NMEFOSE 97% 10-130 EPA 163311/15/25 1

Surrogate: D9-NETFOSE 90% 10-130 EPA 163311/15/25 1

Surrogate: 13C3-HFPO-DA 102% 40-130 EPA 163311/15/25 1

Analyte Result PQL

Date

Analyzed Method/Qual Units DF

Prep

Batch

The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.

No duplication of this report is allowed, except in its entirety.

Page 17 of 88 25K0043_1 HoltGeneralFormat 11 19 25 1521 11/19/25 15:22:11

Project Manager:

EGLE - State Overflow

3350 N Martin Luther King Jr Blvd

Lansing, MI 48906

Flint Bishop Airport Landfill / 2341-7650-81

2341-7650-81

Brian Kuberski Reported: 11/19/2025 15:21

Metiri Group - Holt - 1914 Holloway Dr, Holt, MI 48842

Sample Results

(Continued)

Sample:

25K0043-02 (Water) Sampled: 11/04/25 17:00

Comp-01 (Continued)

Analyte Result PQL

Date

Analyzed Method/Qual Units DF

Prep

Batch

TCLP Metals - Prep EPA 1311

Mercury ND 0.050 EPA 7470A11/11/25 BEK01531mg/L 1

Analyte Result PQL

Date

Analyzed Method/Qual Units DF

Prep

Batch

Wet Chemistry

PH 6.8 1.0 EPA 9040C11/07/25 BEK00961N/A 1 H

Temperature C 23 1.0 EPA 9040C11/07/25 BEK00961 2 H

Cyanide, Reactive ND 5.0 ASTM

D7511-12

11/06/25 BEK00791ug/kg� 1

IGNITABILITY >207 SW-846 101011/11/25 BEK01001Deg F 1

Sulfide, Reactive ND 6.6 HACH 813111/07/25 BEK01101mg/L� 1

Analyte Result PQL

Date

Analyzed Method/Qual Units DF

Prep

Batch

TCLP Extraction

Tumble Date 11/6/25 EPA 131111/06/25 BEK00861[blank]� 1

The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.

No duplication of this report is allowed, except in its entirety.

Page 18 of 88 25K0043_1 HoltGeneralFormat 11 19 25 1521 11/19/25 15:22:11

Project Manager:

EGLE - State Overflow

3350 N Martin Luther King Jr Blvd

Lansing, MI 48906

Flint Bishop Airport Landfill / 2341-7650-81

2341-7650-81

Brian Kuberski Reported: 11/19/2025 15:21

Metiri Group - Holt - 1914 Holloway Dr, Holt, MI 48842

Sample Results

Data Analyzed by: Trace Analytical Laboratories, Inc.

Sample:

25K0043-01 (Water) Sampled: 11/04/25 16:00

Vent #1

Analyte Result PQL

Date

Analyzed Method/Qual Units DF

Prep

Batch

Metals, Total

Silver ND 0.0010 EPA 6020B11/13/25 T1759251mg/L� 1

Arsenic ND 0.0050 EPA 6020B11/13/25 T1759251mg/L� 1

Barium ND 0.10 EPA 6020B11/13/25 T1759251mg/L� 1

Cadmium ND 0.0010 EPA 6020B11/13/25 T1759251mg/L� 1

Chromium ND 0.010 EPA 6020B11/13/25 T1759251mg/L� 1

Copper ND 0.0040 EPA 6020B11/13/25 T1759251mg/L� 1

Lead ND 0.0030 EPA 6020B11/13/25 T1759251mg/L� 1

Selenium ND 0.0050 EPA 6020B11/13/25 T1759251mg/L� 1

Zinc ND 0.050 EPA 6020B11/13/25 T1759251mg/L� 1

Analyte Result PQL

Date

Analyzed Method/Qual Units DF

Prep

Batch

Metals, TCLP

Silver ND 0.10 EPA 6010D11/11/25 T1758621mg/L� 1

Arsenic ND 0.30 EPA 6010D11/11/25 T1758621mg/L� 1

Barium ND 1.0 EPA 6010D11/11/25 T1758621mg/L� 1

Cadmium ND 0.10 EPA 6010D11/11/25 T1758621mg/L� 1

Chromium ND 0.50 EPA 6010D11/11/25 T1758621mg/L� 1

Lead ND 0.50 EPA 6010D11/11/25 T1758621mg/L� 1

Selenium ND 0.60 EPA 6010D11/11/25 T1758621mg/L� 1

The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.

No duplication of this report is allowed, except in its entirety.

Page 19 of 88 25K0043_1 HoltGeneralFormat 11 19 25 1521 11/19/25 15:22:11

Project Manager:

EGLE - State Overflow

3350 N Martin Luther King Jr Blvd

Lansing, MI 48906

Flint Bishop Airport Landfill / 2341-7650-81

2341-7650-81

Brian Kuberski Reported: 11/19/2025 15:21

Metiri Group - Holt - 1914 Holloway Dr, Holt, MI 48842

Sample Results

(Continued)

Data Analyzed by: Trace Analytical Laboratories, Inc.

Sample:

25K0043-02 (Water) Sampled: 11/04/25 17:00

Comp-01

Analyte Result PQL

Date

Analyzed Method/Qual Units DF

Prep

Batch

Metals, TCLP

Silver ND 0.10 EPA 6010D11/11/25 T1758621mg/L� 1

Arsenic ND 0.30 EPA 6010D11/11/25 T1758621mg/L� 1

Barium ND 1.0 EPA 6010D11/11/25 T1758621mg/L� 1

Cadmium ND 0.10 EPA 6010D11/11/25 T1758621mg/L� 1

Chromium ND 0.50 EPA 6010D11/11/25 T1758621mg/L� 1

Lead ND 0.50 EPA 6010D11/11/25 T1758621mg/L� 1

Selenium ND 0.60 EPA 6010D11/11/25 T1758621mg/L� 1

The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.

No duplication of this report is allowed, except in its entirety.

Page 20 of 88 25K0043_1 HoltGeneralFormat 11 19 25 1521 11/19/25 15:22:11

Project Manager:

EGLE - State Overflow

3350 N Martin Luther King Jr Blvd

Lansing, MI 48906

Flint Bishop Airport Landfill / 2341-7650-81

2341-7650-81

Brian Kuberski Reported: 11/19/2025 15:21

Metiri Group - Holt - 1914 Holloway Dr, Holt, MI 48842

EPA 8260D

PREPARATION BATCH SUMMARY

Laboratory:

Client:

Batch Matrix:Batch: Preparation:

Metiri Group - Holt

EGLE - State Overflow

BEK0073 Water EPA 5030B

SAMPLE NAME LAB SAMPLE ID DATE PREPARED INITIAL VOL./WEIGHT

FINAL VOL.

Vent #1 25K0043-01 11/06/25 20:26 42.0000 42

Blank BEK0073-BLK1 11/06/25 11:43 42.0000 42

LCS BEK0073-BS1 11/06/25 09:58 100.0000 100

LCS Dup BEK0073-BSD1 11/06/25 10:24 100.0000 100

The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.

No duplication of this report is allowed, except in its entirety.

Page 21 of 88 25K0043_1 HoltGeneralFormat 11 19 25 1521 11/19/25 15:22:11

Project Manager:

EGLE - State Overflow

3350 N Martin Luther King Jr Blvd

Lansing, MI 48906

Flint Bishop Airport Landfill / 2341-7650-81

2341-7650-81

Brian Kuberski Reported: 11/19/2025 15:21

Metiri Group - Holt - 1914 Holloway Dr, Holt, MI 48842

ASTM D7511-12

PREPARATION BATCH SUMMARY

Laboratory:

Client:

Batch Matrix:Batch: Preparation:

Metiri Group - Holt

EGLE - State Overflow

BEK0079 Water Wet Chem No Prep

SAMPLE NAME LAB SAMPLE ID DATE PREPARED INITIAL VOL./WEIGHT

FINAL VOL.

Vent #1 25K0043-01 11/06/25 09:16 10.0000 10

Comp-01 25K0043-02 11/06/25 09:16 10.0000 10

Blank BEK0079-BLK1 11/06/25 09:16 10.0000 10

LCS BEK0079-BS1 11/06/25 09:16 10.0000 10

LCS Dup BEK0079-BSD1 11/06/25 09:16 10.0000 10

The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.

No duplication of this report is allowed, except in its entirety.

Page 22 of 88 25K0043_1 HoltGeneralFormat 11 19 25 1521 11/19/25 15:22:11

Project Manager:

EGLE - State Overflow

3350 N Martin Luther King Jr Blvd

Lansing, MI 48906

Flint Bishop Airport Landfill / 2341-7650-81

2341-7650-81

Brian Kuberski Reported: 11/19/2025 15:21

Metiri Group - Holt - 1914 Holloway Dr, Holt, MI 48842

EPA 1311

PREPARATION BATCH SUMMARY

Laboratory:

Client:

Batch Matrix:Batch: Preparation:

Metiri Group - Holt

EGLE - State Overflow

BEK0086 Water EPA 1311 Bottle Prep

SAMPLE NAME LAB SAMPLE ID DATE PREPARED INITIAL VOL./WEIGHT

FINAL VOL.

Vent #1 25K0043-01 11/06/25 12:14 100.0000 2,000

Comp-01 25K0043-02 11/06/25 12:14 100.0000 2,000

The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.

No duplication of this report is allowed, except in its entirety.

Page 23 of 88 25K0043_1 HoltGeneralFormat 11 19 25 1521 11/19/25 15:22:11

Project Manager:

EGLE - State Overflow

3350 N Martin Luther King Jr Blvd

Lansing, MI 48906

Flint Bishop Airport Landfill / 2341-7650-81

2341-7650-81

Brian Kuberski Reported: 11/19/2025 15:21

Metiri Group - Holt - 1914 Holloway Dr, Holt, MI 48842

EPA 9040C

PREPARATION BATCH SUMMARY

Laboratory:

Client:

Batch Matrix:Batch: Preparation:

Metiri Group - Holt

EGLE - State Overflow

BEK0096 Water Wet Chem No Prep

SAMPLE NAME LAB SAMPLE ID DATE PREPARED INITIAL VOL./WEIGHT

FINAL VOL.

Vent #1 25K0043-01 11/07/25 08:23 10.0000 10

Comp-01 25K0043-02 11/07/25 08:23 10.0000 10

Vent #1 BEK0096-DUP1 11/07/25 08:23 10.0000 10

The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.

No duplication of this report is allowed, except in its entirety.

Page 24 of 88 25K0043_1 HoltGeneralFormat 11 19 25 1521 11/19/25 15:22:11

Project Manager:

EGLE - State Overflow

3350 N Martin Luther King Jr Blvd

Lansing, MI 48906

Flint Bishop Airport Landfill / 2341-7650-81

2341-7650-81

Brian Kuberski Reported: 11/19/2025 15:21

Metiri Group - Holt - 1914 Holloway Dr, Holt, MI 48842

SW-846 1010

PREPARATION BATCH SUMMARY

Laboratory:

Client:

Batch Matrix:Batch: Preparation:

Metiri Group - Holt

EGLE - State Overflow

BEK0100 Water Wet Chem No Prep

SAMPLE NAME LAB SAMPLE ID DATE PREPARED INITIAL VOL./WEIGHT

FINAL VOL.

Vent #1 25K0043-01 11/07/25 08:56 70.0000 70

Comp-01 25K0043-02 11/07/25 08:56 70.0000 70

LCS BEK0100-BS1 11/07/25 08:56 70.0000 70

Comp-01 BEK0100-DUP1 11/07/25 08:56 70.0000 70

The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.

No duplication of this report is allowed, except in its entirety.

Page 25 of 88 25K0043_1 HoltGeneralFormat 11 19 25 1521 11/19/25 15:22:11

Project Manager:

EGLE - State Overflow

3350 N Martin Luther King Jr Blvd

Lansing, MI 48906

Flint Bishop Airport Landfill / 2341-7650-81

2341-7650-81

Brian Kuberski Reported: 11/19/2025 15:21

Metiri Group - Holt - 1914 Holloway Dr, Holt, MI 48842

HACH 8131

PREPARATION BATCH SUMMARY

Laboratory:

Client:

Batch Matrix:Batch: Preparation:

Metiri Group - Holt

EGLE - State Overflow

BEK0110 Water Wet Chem No Prep

SAMPLE NAME LAB SAMPLE ID DATE PREPARED INITIAL VOL./WEIGHT

FINAL VOL.

Vent #1 25K0043-01 11/07/25 10:39 25.0000 25

Comp-01 25K0043-02 11/07/25 10:39 25.0000 25

Blank BEK0110-BLK1 11/07/25 10:39 50.0000 50

LCS BEK0110-BS1 11/07/25 10:39 50.0000 50

LCS Dup BEK0110-BSD1 11/07/25 10:39 50.0000 50

Vent #1 BEK0110-MS1 11/07/25 10:39 5.0000 25

Vent #1 BEK0110-MSD1 11/07/25 10:39 5.0000 25

The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.

No duplication of this report is allowed, except in its entirety.

Page 26 of 88 25K0043_1 HoltGeneralFormat 11 19 25 1521 11/19/25 15:22:11

Project Manager:

EGLE - State Overflow

3350 N Martin Luther King Jr Blvd

Lansing, MI 48906

Flint Bishop Airport Landfill / 2341-7650-81

2341-7650-81

Brian Kuberski Reported: 11/19/2025 15:21

Metiri Group - Holt - 1914 Holloway Dr, Holt, MI 48842

EPA 8260C TCLP

PREPARATION BATCH SUMMARY

Laboratory:

Client:

Batch Matrix:Batch: Preparation:

Metiri Group - Holt

EGLE - State Overflow

BEK0119 Solid EPA 1311 ZHE

SAMPLE NAME LAB SAMPLE ID DATE PREPARED INITIAL VOL./WEIGHT

FINAL VOL.

Vent #1 25K0043-01 11/07/25 13:50 400.0000 400

Blank BEK0119-BLK1 11/07/25 13:50 400.0000 400

The contents of this report apply to the sample(s) analyzed in accordance with the chain of custody document.

No duplication of this report is allowed, except in its entirety.

Page 27 of 88 25K0043_1 HoltGeneralFormat 11 19 25 1521 11/19/25 15:22:11

Project Manager:

EGLE - State Overflow

3350 N Martin Luther King Jr Blvd

Lansing, MI 48906

Flint Bishop Airport Landfill / 2341-7650-81

2341-7650-81

Brian Kuberski Reported: 11/19/2025 15:21

Metiri Group - Holt - 1914 Holloway Dr, Holt, MI 48842

EPA 8151A

PREPARATION BATCH SUMMARY

Laboratory:

Client:

Batch Matrix:Batch: Preparation:

Metiri Group - Holt

EGLE - State Overflow

BEK0143 Water EPA 8151A

SAMPLE NAME LAB SAMPLE ID DATE PREPARED INITIAL VOL./WEIGHT

FINAL VOL.

Vent #1 25K0043-01…

This is the start of the file's text. The full file is on GovTribe.

File details come from the government source that posted it. Updated Jul 10, 2026.