B-295_J119007-1_UDS_Level_2_Report_Final_Report.pdf
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- Attached to
- Low Observable Paint Booth Facilities Maintenance Federal contract opportunity
- Solicitation number
- FA4819-17-R-4006
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UDS Level 2 Report (Final)
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Other files for this federal contract opportunity
| File | Type | Posted |
|---|---|---|
| FA4819-17-R-4006_0005.pdf | ||
| PWS_LO_MX_Rev_2,_dtd_3_Mar_2017.pdf | ||
| QA_24_Feb_2017.docx | DOCX document | |
| FA4819-17-R-4006_0004.pdf | ||
| FA4819-17-R-4006_0003.pdf | ||
| FA4819-17-R-4006_0002.pdf | ||
| PWS_LO_MX_Rev_1_dtd_6_Feb2017.pdf | ||
| Combined_Questions_from_Site_Visit_13_Jan_2017.pdf | ||
| Attachment__4,_Financial_Questionnaire.pdf | ||
| Attachment___5_PPQ.pdf | ||
| Attachment___2,_Hourly_Rate_per_Skill_Set.pdf | ||
| Attachment__3,_Site_Visit.pdf | ||
| Attachment__1,_PWS_LO_MX_23_Nov_2016.pdf | ||
| FA4819-17-R-4006_Solicitation.pdf |
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Client Sample Results TestAmerica Job ID: 400-119007-1Client: Bhate Environmental
SDG: WASTE CHARACTERIZATIONProject/Site: Tyndall AFB
Lab Sample ID: 400-119007-2Client Sample ID: LO/CRF-NBAY 1ST STAGE TOP Matrix: SolidDate Collected: 03/16/16 10:00
Date Received: 03/17/16 09:23
Method: 8270C - Semivolatile Organic Compounds (GC/MS)
PQL MDL
Benzoic acid 11 U 32 11 mg/Kg 03/24/16 17:37 04/03/16 16:15 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
11 0.64 mg/Kg 03/24/16 17:37 04/03/16 16:15 1Acenaphthene 0.64 U
11 0.64 mg/Kg 03/24/16 17:37 04/03/16 16:15 1Acenaphthylene 0.64 U
11 0.64 mg/Kg 03/24/16 17:37 04/03/16 16:15 1Anthracene 0.64 U
32 3.2 mg/Kg 03/24/16 17:37 04/03/16 16:15 1Benzidine 3.2 U
11 1.1 mg/Kg 03/24/16 17:37 04/03/16 16:15 14-Chloro-3-methylphenol 1.1 U
11 1.9 mg/Kg 03/24/16 17:37 04/03/16 16:15 14,6-Dinitro-2-methylphenol 1.9 U
11 4.8 mg/Kg 03/24/16 17:37 04/03/16 16:15 14-Nitrophenol 4.8 U
11 1.1 mg/Kg 03/24/16 17:37 04/03/16 16:15 14-Bromophenyl phenyl ether 1.1 U
11 2.6 mg/Kg 03/24/16 17:37 04/03/16 16:15 14-Chloroaniline 2.6 U
11 1.1 mg/Kg 03/24/16 17:37 04/03/16 16:15 14-Chlorophenyl phenyl ether 1.1 U
11 1.8 mg/Kg 03/24/16 17:37 04/03/16 16:15 14-Nitroaniline 1.8 U
11 1.1 mg/Kg 03/24/16 17:37 04/03/16 16:15 12-Chlorophenol 1.1 U
11 1.1 mg/Kg 03/24/16 17:37 04/03/16 16:15 12,4-Dichlorophenol 1.1 U
11 1.1 mg/Kg 03/24/16 17:37 04/03/16 16:15 12,6-Dichlorophenol 1.1 U
11 1.1 mg/Kg 03/24/16 17:37 04/03/16 16:15 12,4-Dimethylphenol 1.1 U
32 9.3 mg/Kg 03/24/16 17:37 04/03/16 16:15 12,4-Dinitrophenol 9.3 U
11 1.1 mg/Kg 03/24/16 17:37 04/03/16 16:15 12-Methylphenol 1.1 U
11 1.1 mg/Kg 03/24/16 17:37 04/03/16 16:15 12-Nitrophenol 1.1 U
21 2.1 mg/Kg 03/24/16 17:37 04/03/16 16:15 1Pentachlorophenol 2.1 U
11 1.1 mg/Kg 03/24/16 17:37 04/03/16 16:15 1Phenol 1.1 U
21 1.1 mg/Kg 03/24/16 17:37 04/03/16 16:15 13 & 4 Methylphenol 1.1 U
11 1.1 mg/Kg 03/24/16 17:37 04/03/16 16:15 12,4,5-Trichlorophenol 1.1 U
11 1.1 mg/Kg 03/24/16 17:37 04/03/16 16:15 12,4,6-Trichlorophenol 1.1 U
11 0.64 mg/Kg 03/24/16 17:37 04/03/16 16:15 1Benzo[a]anthracene 0.64 U
11 0.64 mg/Kg 03/24/16 17:37 04/03/16 16:15 1Benzo[a]pyrene 0.64 U
11 0.80 mg/Kg 03/24/16 17:37 04/03/16 16:15 1Benzo[b]fluoranthene 0.80 U
11 0.96 mg/Kg 03/24/16 17:37 04/03/16 16:15 1Benzo[g,h,i]perylene 0.96 U
11 0.70 mg/Kg 03/24/16 17:37 04/03/16 16:15 1Benzo[k]fluoranthene 0.70 U
11 1.6 mg/Kg 03/24/16 17:37 04/03/16 16:15 1Benzyl alcohol 1.6 U
11 1.1 mg/Kg 03/24/16 17:37 04/03/16 16:15 1Butyl benzyl phthalate 5.3 I
11 1.1 mg/Kg 03/24/16 17:37 04/03/16 16:15 1Bis(2-chloroethoxy)methane 1.1 U
11 1.1 mg/Kg 03/24/16 17:37 04/03/16 16:15 1Bis(2-chloroethyl)ether 1.1 U
11 1.1 mg/Kg 03/24/16 17:37 04/03/16 16:15 1Bis(2-ethylhexyl) phthalate 7.5 I
11 0.70 mg/Kg 03/24/16 17:37 04/03/16 16:15 1Chrysene 0.70 U
11 0.80 mg/Kg 03/24/16 17:37 04/03/16 16:15 1Dibenz(a,h)anthracene 0.80 U
11 1.1 mg/Kg 03/24/16 17:37 04/03/16 16:15 1Dibenzofuran 1.1 U
11 1.1 mg/Kg 03/24/16 17:37 04/03/16 16:15 1Di-n-butyl phthalate 1.1 U
11 1.1 mg/Kg 03/24/16 17:37 04/03/16 16:15 1Di-n-octyl phthalate 1.1 U
11 0.80 mg/Kg 03/24/16 17:37 04/03/16 16:15 1Fluoranthene 0.80 U
11 0.64 mg/Kg 03/24/16 17:37 04/03/16 16:15 1Fluorene 0.64 U
11 3.2 mg/Kg 03/24/16 17:37 04/03/16 16:15 1Hexachlorobenzene 3.2 U
11 1.1 mg/Kg 03/24/16 17:37 04/03/16 16:15 1Hexachlorobutadiene 1.1 U
11 2.1 mg/Kg 03/24/16 17:37 04/03/16 16:15 1Hexachlorocyclopentadiene 2.1 U
11 3.2 mg/Kg 03/24/16 17:37 04/03/16 16:15 1Hexachloroethane 3.2 U
11 0.80 mg/Kg 03/24/16 17:37 04/03/16 16:15 1Indeno[1,2,3-cd]pyrene 0.80 U
11 1.1 mg/Kg 03/24/16 17:37 04/03/16 16:15 1Isophorone 1.1 U
11 0.70 mg/Kg 03/24/16 17:37 04/03/16 16:15 1Naphthalene 0.70 U
11 2.1 mg/Kg 03/24/16 17:37 04/03/16 16:15 1N-Nitrosodi-n-butylamine 2.1 U
TestAmerica Pensacola
Page 8 of 59 4/7/2016
SDG: WASTE CHARACTERIZATIONProject/Site: Tyndall AFB
Lab Sample ID: 400-119007-2Client Sample ID: LO/CRF-NBAY 1ST STAGE TOP Matrix: SolidDate Collected: 03/16/16 10:00
Date Received: 03/17/16 09:23
Method: 8270C - Semivolatile Organic Compounds (GC/MS) (Continued)
PQL MDL
N-Nitrosodimethylamine 2.1 U 11 2.1 mg/Kg 03/24/16 17:37 04/03/16 16:15 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
11 1.1 mg/Kg 03/24/16 17:37 04/03/16 16:15 1N-Nitrosodiphenylamine 1.1 U
11 3.5 mg/Kg 03/24/16 17:37 04/03/16 16:15 1N-Nitrosodi-n-propylamine 3.5 U
11 0.64 mg/Kg 03/24/16 17:37 04/03/16 16:15 1Phenanthrene 0.64 U
11 0.80 mg/Kg 03/24/16 17:37 04/03/16 16:15 1Pyrene 0.80 U
11 1.1 mg/Kg 03/24/16 17:37 04/03/16 16:15 11,2-Dichlorobenzene 1.1 U
11 1.1 mg/Kg 03/24/16 17:37 04/03/16 16:15 11,3-Dichlorobenzene 1.1 U
11 1.1 mg/Kg 03/24/16 17:37 04/03/16 16:15 11,4-Dichlorobenzene 1.1 U
11 1.1 mg/Kg 03/24/16 17:37 04/03/16 16:15 12-Chloronaphthalene 1.1 U
11 5.0 mg/Kg 03/24/16 17:37 04/03/16 16:15 13,3'-Dichlorobenzidine 5.0 U
11 1.1 mg/Kg 03/24/16 17:37 04/03/16 16:15 1Diethyl phthalate 1.1 U
11 1.1 mg/Kg 03/24/16 17:37 04/03/16 16:15 1Dimethyl phthalate 1.1 U
11 1.1 mg/Kg 03/24/16 17:37 04/03/16 16:15 12,4-Dinitrotoluene 1.1 U
11 1.1 mg/Kg 03/24/16 17:37 04/03/16 16:15 12,6-Dinitrotoluene 1.1 U
11 0.64 mg/Kg 03/24/16 17:37 04/03/16 16:15 11-Methylnaphthalene 0.64 U
11 0.58 mg/Kg 03/24/16 17:37 04/03/16 16:15 12-Methylnaphthalene 0.58 U
11 1.1 mg/Kg 03/24/16 17:37 04/03/16 16:15 12-Nitroaniline 1.1 U
11 1.3 mg/Kg 03/24/16 17:37 04/03/16 16:15 13-Nitroaniline 1.3 U
11 1.1 mg/Kg 03/24/16 17:37 04/03/16 16:15 1Nitrobenzene 1.1 U
11 1.1 mg/Kg 03/24/16 17:37 04/03/16 16:15 11,2,4-Trichlorobenzene 1.1 U
11 1.1 mg/Kg 03/24/16 17:37 04/03/16 16:15 1bis (2-chloroisopropyl) ether 1.1 U
11 1.1 mg/Kg 03/24/16 17:37 04/03/16 16:15 11,2-Diphenylhydrazine (as
Azobenzene)
1.1 U
2,4,6-Tribromophenol 64 32 - 133 03/24/16 17:37 04/03/16 16:15 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
2-Fluorobiphenyl 77 03/24/16 17:37 04/03/16 16:15 144 - 120
2-Fluorophenol 46 03/24/16 17:37 04/03/16 16:15 125 - 120
Nitrobenzene-d5 65 03/24/16 17:37 04/03/16 16:15 127 - 120
Phenol-d5 56 03/24/16 17:37 04/03/16 16:15 137 - 120
Terphenyl-d14 90 03/24/16 17:37 04/03/16 16:15 136 - 134
Method: 6010B - Metals (ICP) - TCLP
PQL MDL
Arsenic 0.020 U 0.025 0.020 mg/L 04/01/16 09:41 04/01/16 16:46 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
5.0 0.050 mg/L 04/01/16 09:41 04/01/16 16:46 1Barium 0.26 I
0.050 0.010 mg/L 04/01/16 09:41 04/01/16 16:46 1Chromium 0.99
0.025 0.010 mg/L 04/01/16 09:41 04/01/16 16:46 1Lead 0.013 I
0.10 0.020 mg/L 04/01/16 09:41 04/01/16 16:46 1Selenium 0.020 U
0.025 0.010 mg/L 04/01/16 09:41 04/01/16 16:46 1Silver 0.24
Method: 6010B - Metals (ICP) - TCLP - DL
PQL MDL
Cadmium 0.025 U 0.13 0.025 mg/L 04/01/16 09:41 04/03/16 14:10 5
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
Method: 7470A - Mercury (CVAA) - TCLP
PQL MDL
Mercury 0.00056 U 0.0016 0.00056 mg/L 03/31/16 13:32 04/01/16 13:07 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
TestAmerica Pensacola
Page 9 of 59 4/7/2016
SDG: WASTE CHARACTERIZATIONProject/Site: Tyndall AFB
Lab Sample ID: 400-119007-3Client Sample ID: LO/CRF-NBAY 2ND STAGE BOTTOM Matrix: SolidDate Collected: 03/16/16 10:05
Date Received: 03/17/16 09:23
Method: 8270C - Semivolatile Organic Compounds (GC/MS)
PQL MDL
Benzoic acid 130 U 380 130 mg/Kg 03/24/16 17:37 04/03/16 16:52 20
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
130 7.6 mg/Kg 03/24/16 17:37 04/03/16 16:52 20Acenaphthene 7.6 U
130 7.6 mg/Kg 03/24/16 17:37 04/03/16 16:52 20Acenaphthylene 7.6 U
130 7.6 mg/Kg 03/24/16 17:37 04/03/16 16:52 20Anthracene 7.6 U
380 38 mg/Kg 03/24/16 17:37 04/03/16 16:52 20Benzidine 38 U
130 13 mg/Kg 03/24/16 17:37 04/03/16 16:52 204-Chloro-3-methylphenol 13 U
130 23 mg/Kg 03/24/16 17:37 04/03/16 16:52 204,6-Dinitro-2-methylphenol 23 U
130 57 mg/Kg 03/24/16 17:37 04/03/16 16:52 204-Nitrophenol 57 U
130 13 mg/Kg 03/24/16 17:37 04/03/16 16:52 204-Bromophenyl phenyl ether 13 U
130 30 mg/Kg 03/24/16 17:37 04/03/16 16:52 204-Chloroaniline 30 U
130 13 mg/Kg 03/24/16 17:37 04/03/16 16:52 204-Chlorophenyl phenyl ether 13 U
130 21 mg/Kg 03/24/16 17:37 04/03/16 16:52 204-Nitroaniline 21 U
130 13 mg/Kg 03/24/16 17:37 04/03/16 16:52 202-Chlorophenol 13 U
130 13 mg/Kg 03/24/16 17:37 04/03/16 16:52 202,4-Dichlorophenol 13 U
130 13 mg/Kg 03/24/16 17:37 04/03/16 16:52 202,6-Dichlorophenol 13 U
130 13 mg/Kg 03/24/16 17:37 04/03/16 16:52 202,4-Dimethylphenol 13 U
380 110 mg/Kg 03/24/16 17:37 04/03/16 16:52 202,4-Dinitrophenol 110 U
130 13 mg/Kg 03/24/16 17:37 04/03/16 16:52 202-Methylphenol 13 U
130 13 mg/Kg 03/24/16 17:37 04/03/16 16:52 202-Nitrophenol 13 U
250 25 mg/Kg 03/24/16 17:37 04/03/16 16:52 20Pentachlorophenol 25 U
130 13 mg/Kg 03/24/16 17:37 04/03/16 16:52 20Phenol 13 U
250 13 mg/Kg 03/24/16 17:37 04/03/16 16:52 203 & 4 Methylphenol 13 U
130 13 mg/Kg 03/24/16 17:37 04/03/16 16:52 202,4,5-Trichlorophenol 13 U
130 13 mg/Kg 03/24/16 17:37 04/03/16 16:52 202,4,6-Trichlorophenol 13 U
130 7.6 mg/Kg 03/24/16 17:37 04/03/16 16:52 20Benzo[a]anthracene 7.6 U
130 7.6 mg/Kg 03/24/16 17:37 04/03/16 16:52 20Benzo[a]pyrene 7.6 U
130 9.5 mg/Kg 03/24/16 17:37 04/03/16 16:52 20Benzo[b]fluoranthene 9.5 U
130 11 mg/Kg 03/24/16 17:37 04/03/16 16:52 20Benzo[g,h,i]perylene 11 U
130 8.4 mg/Kg 03/24/16 17:37 04/03/16 16:52 20Benzo[k]fluoranthene 8.4 U
130 19 mg/Kg 03/24/16 17:37 04/03/16 16:52 20Benzyl alcohol 19 U
130 13 mg/Kg 03/24/16 17:37 04/03/16 16:52 20Butyl benzyl phthalate 13 U
130 13 mg/Kg 03/24/16 17:37 04/03/16 16:52 20Bis(2-chloroethoxy)methane 13 U
130 13 mg/Kg 03/24/16 17:37 04/03/16 16:52 20Bis(2-chloroethyl)ether 13 U
130 13 mg/Kg 03/24/16 17:37 04/03/16 16:52 20Bis(2-ethylhexyl) phthalate 13 U
130 8.4 mg/Kg 03/24/16 17:37 04/03/16 16:52 20Chrysene 8.4 U
130 9.5 mg/Kg 03/24/16 17:37 04/03/16 16:52 20Dibenz(a,h)anthracene 9.5 U
130 13 mg/Kg 03/24/16 17:37 04/03/16 16:52 20Dibenzofuran 13 U
130 13 mg/Kg 03/24/16 17:37 04/03/16 16:52 20Di-n-butyl phthalate 13 U
130 13 mg/Kg 03/24/16 17:37 04/03/16 16:52 20Di-n-octyl phthalate 13 U
130 9.5 mg/Kg 03/24/16 17:37 04/03/16 16:52 20Fluoranthene 9.5 U
130 7.6 mg/Kg 03/24/16 17:37 04/03/16 16:52 20Fluorene 7.6 U
130 38 mg/Kg 03/24/16 17:37 04/03/16 16:52 20Hexachlorobenzene 38 U
130 13 mg/Kg 03/24/16 17:37 04/03/16 16:52 20Hexachlorobutadiene 13 U
130 25 mg/Kg 03/24/16 17:37 04/03/16 16:52 20Hexachlorocyclopentadiene 25 U
130 38 mg/Kg 03/24/16 17:37 04/03/16 16:52 20Hexachloroethane 38 U
130 9.5 mg/Kg 03/24/16 17:37 04/03/16 16:52 20Indeno[1,2,3-cd]pyrene 9.5 U
130 13 mg/Kg 03/24/16 17:37 04/03/16 16:52 20Isophorone 13 U
130 8.4 mg/Kg 03/24/16 17:37 04/03/16 16:52 20Naphthalene 8.4 U
130 25 mg/Kg 03/24/16 17:37 04/03/16 16:52 20N-Nitrosodi-n-butylamine 25 U
TestAmerica Pensacola
Page 10 of 59 4/7/2016
SDG: WASTE CHARACTERIZATIONProject/Site: Tyndall AFB
Lab Sample ID: 400-119007-3Client Sample ID: LO/CRF-NBAY 2ND STAGE BOTTOM Matrix: SolidDate Collected: 03/16/16 10:05
Date Received: 03/17/16 09:23
Method: 8270C - Semivolatile Organic Compounds (GC/MS) (Continued)
PQL MDL
N-Nitrosodimethylamine 25 U 130 25 mg/Kg 03/24/16 17:37 04/03/16 16:52 20
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
130 13 mg/Kg 03/24/16 17:37 04/03/16 16:52 20N-Nitrosodiphenylamine 13 U
130 42 mg/Kg 03/24/16 17:37 04/03/16 16:52 20N-Nitrosodi-n-propylamine 42 U
130 7.6 mg/Kg 03/24/16 17:37 04/03/16 16:52 20Phenanthrene 7.6 U
130 9.5 mg/Kg 03/24/16 17:37 04/03/16 16:52 20Pyrene 9.5 U
130 13 mg/Kg 03/24/16 17:37 04/03/16 16:52 201,2-Dichlorobenzene 13 U
130 13 mg/Kg 03/24/16 17:37 04/03/16 16:52 201,3-Dichlorobenzene 13 U
130 13 mg/Kg 03/24/16 17:37 04/03/16 16:52 201,4-Dichlorobenzene 13 U
130 13 mg/Kg 03/24/16 17:37 04/03/16 16:52 202-Chloronaphthalene 13 U
130 59 mg/Kg 03/24/16 17:37 04/03/16 16:52 203,3'-Dichlorobenzidine 59 U
130 13 mg/Kg 03/24/16 17:37 04/03/16 16:52 20Diethyl phthalate 13 U
130 13 mg/Kg 03/24/16 17:37 04/03/16 16:52 20Dimethyl phthalate 13 U
130 13 mg/Kg 03/24/16 17:37 04/03/16 16:52 202,4-Dinitrotoluene 13 U
130 13 mg/Kg 03/24/16 17:37 04/03/16 16:52 202,6-Dinitrotoluene 13 U
130 7.6 mg/Kg 03/24/16 17:37 04/03/16 16:52 201-Methylnaphthalene 7.6 U
130 6.9 mg/Kg 03/24/16 17:37 04/03/16 16:52 202-Methylnaphthalene 6.9 U
130 13 mg/Kg 03/24/16 17:37 04/03/16 16:52 202-Nitroaniline 13 U
130 15 mg/Kg 03/24/16 17:37 04/03/16 16:52 203-Nitroaniline 15 U
130 13 mg/Kg 03/24/16 17:37 04/03/16 16:52 20Nitrobenzene 13 U
130 13 mg/Kg 03/24/16 17:37 04/03/16 16:52 201,2,4-Trichlorobenzene 13 U
130 13 mg/Kg 03/24/16 17:37 04/03/16 16:52 20bis (2-chloroisopropyl) ether 13 U
130 13 mg/Kg 03/24/16 17:37 04/03/16 16:52 201,2-Diphenylhydrazine (as
Azobenzene)
13 U
2,4,6-Tribromophenol 0 J1 32 - 133 03/24/16 17:37 04/03/16 16:52 20
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
2-Fluorobiphenyl 0 J1 03/24/16 17:37 04/03/16 16:52 2044 - 120
2-Fluorophenol 12 J1 03/24/16 17:37 04/03/16 16:52 2025 - 120
Nitrobenzene-d5 20 J1 03/24/16 17:37 04/03/16 16:52 2027 - 120
Phenol-d5 15 J1 03/24/16 17:37 04/03/16 16:52 2037 - 120
Terphenyl-d14 39 03/24/16 17:37 04/03/16 16:52 2036 - 134
Method: 6010B - Metals (ICP) - TCLP
PQL MDL
Arsenic 0.020 U 0.025 0.020 mg/L 04/01/16 09:41 04/01/16 16:49 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
5.0 0.050 mg/L 04/01/16 09:41 04/01/16 16:49 1Barium 0.15 I
0.025 0.0050 mg/L 04/01/16 09:41 04/01/16 16:49 1Cadmium 0.0050 U
0.050 0.010 mg/L 04/01/16 09:41 04/01/16 16:49 1Chromium 0.29
0.025 0.010 mg/L 04/01/16 09:41 04/01/16 16:49 1Lead 0.010 U
0.10 0.020 mg/L 04/01/16 09:41 04/01/16 16:49 1Selenium 0.020 U
0.025 0.010 mg/L 04/01/16 09:41 04/01/16 16:49 1Silver 0.099
Method: 7470A - Mercury (CVAA) - TCLP
PQL MDL
Mercury 0.00056 U 0.0016 0.00056 mg/L 03/31/16 13:32 04/01/16 13:17 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
TestAmerica Pensacola
Page 11 of 59 4/7/2016
SDG: WASTE CHARACTERIZATIONProject/Site: Tyndall AFB
Lab Sample ID: 400-119007-4Client Sample ID: LO/CRF-NBAY 3RD STAGE BOTTOM Matrix: SolidDate Collected: 03/16/16 10:10
Date Received: 03/17/16 09:23
Method: 8270C - Semivolatile Organic Compounds (GC/MS)
PQL MDL
Benzoic acid 12 U 35 12 mg/Kg 03/24/16 17:37 04/03/16 17:29 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
12 0.71 mg/Kg 03/24/16 17:37 04/03/16 17:29 1Acenaphthene 0.71 U
12 0.71 mg/Kg 03/24/16 17:37 04/03/16 17:29 1Acenaphthylene 0.71 U
12 0.71 mg/Kg 03/24/16 17:37 04/03/16 17:29 1Anthracene 0.71 U
35 3.5 mg/Kg 03/24/16 17:37 04/03/16 17:29 1Benzidine 3.5 U
12 1.2 mg/Kg 03/24/16 17:37 04/03/16 17:29 14-Chloro-3-methylphenol 1.2 U
12 2.1 mg/Kg 03/24/16 17:37 04/03/16 17:29 14,6-Dinitro-2-methylphenol 2.1 U
12 5.3 mg/Kg 03/24/16 17:37 04/03/16 17:29 14-Nitrophenol 5.3 U
12 1.2 mg/Kg 03/24/16 17:37 04/03/16 17:29 14-Bromophenyl phenyl ether 1.2 U
12 2.8 mg/Kg 03/24/16 17:37 04/03/16 17:29 14-Chloroaniline 2.8 U
12 1.2 mg/Kg 03/24/16 17:37 04/03/16 17:29 14-Chlorophenyl phenyl ether 1.2 U
12 2.0 mg/Kg 03/24/16 17:37 04/03/16 17:29 14-Nitroaniline 2.0 U
12 1.2 mg/Kg 03/24/16 17:37 04/03/16 17:29 12-Chlorophenol 1.2 U
12 1.2 mg/Kg 03/24/16 17:37 04/03/16 17:29 12,4-Dichlorophenol 1.2 U
12 1.2 mg/Kg 03/24/16 17:37 04/03/16 17:29 12,6-Dichlorophenol 1.2 U
12 1.2 mg/Kg 03/24/16 17:37 04/03/16 17:29 12,4-Dimethylphenol 1.2 U
35 10 mg/Kg 03/24/16 17:37 04/03/16 17:29 12,4-Dinitrophenol 10 U
12 1.2 mg/Kg 03/24/16 17:37 04/03/16 17:29 12-Methylphenol 1.2 U
12 1.2 mg/Kg 03/24/16 17:37 04/03/16 17:29 12-Nitrophenol 1.2 U
23 2.3 mg/Kg 03/24/16 17:37 04/03/16 17:29 1Pentachlorophenol 2.3 U
12 1.2 mg/Kg 03/24/16 17:37 04/03/16 17:29 1Phenol 1.2 U
23 1.2 mg/Kg 03/24/16 17:37 04/03/16 17:29 13 & 4 Methylphenol 1.2 U
12 1.2 mg/Kg 03/24/16 17:37 04/03/16 17:29 12,4,5-Trichlorophenol 1.2 U
12 1.2 mg/Kg 03/24/16 17:37 04/03/16 17:29 12,4,6-Trichlorophenol 1.2 U
12 0.71 mg/Kg 03/24/16 17:37 04/03/16 17:29 1Benzo[a]anthracene 0.71 U
12 0.71 mg/Kg 03/24/16 17:37 04/03/16 17:29 1Benzo[a]pyrene 0.71 U
12 0.89 mg/Kg 03/24/16 17:37 04/03/16 17:29 1Benzo[b]fluoranthene 0.89 U
12 1.1 mg/Kg 03/24/16 17:37 04/03/16 17:29 1Benzo[g,h,i]perylene 1.1 U
12 0.78 mg/Kg 03/24/16 17:37 04/03/16 17:29 1Benzo[k]fluoranthene 0.78 U
12 1.8 mg/Kg 03/24/16 17:37 04/03/16 17:29 1Benzyl alcohol 1.8 U
12 1.2 mg/Kg 03/24/16 17:37 04/03/16 17:29 1Butyl benzyl phthalate 1.2 U
12 1.2 mg/Kg 03/24/16 17:37 04/03/16 17:29 1Bis(2-chloroethoxy)methane 1.2 U
12 1.2 mg/Kg 03/24/16 17:37 04/03/16 17:29 1Bis(2-chloroethyl)ether 1.2 U
12 1.2 mg/Kg 03/24/16 17:37 04/03/16 17:29 1Bis(2-ethylhexyl) phthalate 1.2 U
12 0.78 mg/Kg 03/24/16 17:37 04/03/16 17:29 1Chrysene 0.78 U
12 0.89 mg/Kg 03/24/16 17:37 04/03/16 17:29 1Dibenz(a,h)anthracene 0.89 U
12 1.2 mg/Kg 03/24/16 17:37 04/03/16 17:29 1Dibenzofuran 1.2 U
12 1.2 mg/Kg 03/24/16 17:37 04/03/16 17:29 1Di-n-butyl phthalate 1.2 U
12 1.2 mg/Kg 03/24/16 17:37 04/03/16 17:29 1Di-n-octyl phthalate 1.2 U
12 0.89 mg/Kg 03/24/16 17:37 04/03/16 17:29 1Fluoranthene 0.89 U
12 0.71 mg/Kg 03/24/16 17:37 04/03/16 17:29 1Fluorene 0.71 U
12 3.5 mg/Kg 03/24/16 17:37 04/03/16 17:29 1Hexachlorobenzene 3.5 U
12 1.2 mg/Kg 03/24/16 17:37 04/03/16 17:29 1Hexachlorobutadiene 1.2 U
12 2.3 mg/Kg 03/24/16 17:37 04/03/16 17:29 1Hexachlorocyclopentadiene 2.3 U
12 3.5 mg/Kg 03/24/16 17:37 04/03/16 17:29 1Hexachloroethane 3.5 U
12 0.89 mg/Kg 03/24/16 17:37 04/03/16 17:29 1Indeno[1,2,3-cd]pyrene 0.89 U
12 1.2 mg/Kg 03/24/16 17:37 04/03/16 17:29 1Isophorone 1.2 U
12 0.78 mg/Kg 03/24/16 17:37 04/03/16 17:29 1Naphthalene 0.78 U
12 2.3 mg/Kg 03/24/16 17:37 04/03/16 17:29 1N-Nitrosodi-n-butylamine 2.3 U
TestAmerica Pensacola
Page 12 of 59 4/7/2016
SDG: WASTE CHARACTERIZATIONProject/Site: Tyndall AFB
Lab Sample ID: 400-119007-4Client Sample ID: LO/CRF-NBAY 3RD STAGE BOTTOM Matrix: SolidDate Collected: 03/16/16 10:10
Date Received: 03/17/16 09:23
Method: 8270C - Semivolatile Organic Compounds (GC/MS) (Continued)
PQL MDL
N-Nitrosodimethylamine 2.3 U 12 2.3 mg/Kg 03/24/16 17:37 04/03/16 17:29 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
12 1.2 mg/Kg 03/24/16 17:37 04/03/16 17:29 1N-Nitrosodiphenylamine 1.2 U
12 3.9 mg/Kg 03/24/16 17:37 04/03/16 17:29 1N-Nitrosodi-n-propylamine 3.9 U
12 0.71 mg/Kg 03/24/16 17:37 04/03/16 17:29 1Phenanthrene 0.71 U
12 0.89 mg/Kg 03/24/16 17:37 04/03/16 17:29 1Pyrene 0.89 U
12 1.2 mg/Kg 03/24/16 17:37 04/03/16 17:29 11,2-Dichlorobenzene 1.2 U
12 1.2 mg/Kg 03/24/16 17:37 04/03/16 17:29 11,3-Dichlorobenzene 1.2 U
12 1.2 mg/Kg 03/24/16 17:37 04/03/16 17:29 11,4-Dichlorobenzene 1.2 U
12 1.2 mg/Kg 03/24/16 17:37 04/03/16 17:29 12-Chloronaphthalene 1.2 U
12 5.5 mg/Kg 03/24/16 17:37 04/03/16 17:29 13,3'-Dichlorobenzidine 5.5 U
12 1.2 mg/Kg 03/24/16 17:37 04/03/16 17:29 1Diethyl phthalate 1.2 U
12 1.2 mg/Kg 03/24/16 17:37 04/03/16 17:29 1Dimethyl phthalate 1.2 U
12 1.2 mg/Kg 03/24/16 17:37 04/03/16 17:29 12,4-Dinitrotoluene 1.2 U
12 1.2 mg/Kg 03/24/16 17:37 04/03/16 17:29 12,6-Dinitrotoluene 1.2 U
12 0.71 mg/Kg 03/24/16 17:37 04/03/16 17:29 11-Methylnaphthalene 0.71 U
12 0.64 mg/Kg 03/24/16 17:37 04/03/16 17:29 12-Methylnaphthalene 0.64 U
12 1.2 mg/Kg 03/24/16 17:37 04/03/16 17:29 12-Nitroaniline 1.2 U
12 1.4 mg/Kg 03/24/16 17:37 04/03/16 17:29 13-Nitroaniline 1.4 U
12 1.2 mg/Kg 03/24/16 17:37 04/03/16 17:29 1Nitrobenzene 1.2 U
12 1.2 mg/Kg 03/24/16 17:37 04/03/16 17:29 11,2,4-Trichlorobenzene 1.2 U
12 1.2 mg/Kg 03/24/16 17:37 04/03/16 17:29 1bis (2-chloroisopropyl) ether 1.2 U
12 1.2 mg/Kg 03/24/16 17:37 04/03/16 17:29 11,2-Diphenylhydrazine (as
Azobenzene)
1.2 U
2,4,6-Tribromophenol 0 J1 32 - 133 03/24/16 17:37 04/03/16 17:29 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
2-Fluorobiphenyl 0 J1 03/24/16 17:37 04/03/16 17:29 144 - 120
2-Fluorophenol 1 J1 03/24/16 17:37 04/03/16 17:29 125 - 120
Nitrobenzene-d5 2 J1 03/24/16 17:37 04/03/16 17:29 127 - 120
Phenol-d5 1 J1 03/24/16 17:37 04/03/16 17:29 137 - 120
Terphenyl-d14 3 J1 03/24/16 17:37 04/03/16 17:29 136 - 134
Method: 6010B - Metals (ICP) - TCLP
PQL MDL
Arsenic 0.020 U 0.025 0.020 mg/L 04/01/16 09:41 04/01/16 17:16 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
5.0 0.050 mg/L 04/01/16 09:41 04/01/16 17:16 1Barium 0.15 I
0.025 0.0050 mg/L 04/01/16 09:41 04/01/16 17:16 1Cadmium 0.0050 U
0.050 0.010 mg/L 04/01/16 09:41 04/01/16 17:16 1Chromium 0.15
0.025 0.010 mg/L 04/01/16 09:41 04/01/16 17:16 1Lead 0.012 I
0.10 0.020 mg/L 04/01/16 09:41 04/01/16 17:16 1Selenium 0.020 U
0.025 0.010 mg/L 04/01/16 09:41 04/01/16 17:16 1Silver 0.070
Method: 7470A - Mercury (CVAA) - TCLP
PQL MDL
Mercury 0.00056 U 0.0016 0.00056 mg/L 03/31/16 13:32 04/01/16 13:18 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
TestAmerica Pensacola
Page 13 of 59 4/7/2016
SDG: WASTE CHARACTERIZATIONProject/Site: Tyndall AFB
Lab Sample ID: 400-119007-5Client Sample ID: LO/CRF-SBAY 1ST STAGE TOP Matrix: SolidDate Collected: 03/16/16 10:15
Date Received: 03/17/16 09:23
Method: 8270C - Semivolatile Organic Compounds (GC/MS)
PQL MDL
Benzoic acid 14 U 38 14 mg/Kg 03/24/16 17:37 04/03/16 18:06 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
13 0.77 mg/Kg 03/24/16 17:37 04/03/16 18:06 1Acenaphthene 0.77 U
13 0.77 mg/Kg 03/24/16 17:37 04/03/16 18:06 1Acenaphthylene 0.77 U
13 0.77 mg/Kg 03/24/16 17:37 04/03/16 18:06 1Anthracene 0.77 U
38 3.8 mg/Kg 03/24/16 17:37 04/03/16 18:06 1Benzidine 3.8 U
13 1.3 mg/Kg 03/24/16 17:37 04/03/16 18:06 14-Chloro-3-methylphenol 1.3 U
13 2.3 mg/Kg 03/24/16 17:37 04/03/16 18:06 14,6-Dinitro-2-methylphenol 2.3 U
13 5.8 mg/Kg 03/24/16 17:37 04/03/16 18:06 14-Nitrophenol 6.7 I
13 1.3 mg/Kg 03/24/16 17:37 04/03/16 18:06 14-Bromophenyl phenyl ether 1.3 U
13 3.1 mg/Kg 03/24/16 17:37 04/03/16 18:06 14-Chloroaniline 3.1 U
13 1.3 mg/Kg 03/24/16 17:37 04/03/16 18:06 14-Chlorophenyl phenyl ether 1.3 U
13 2.1 mg/Kg 03/24/16 17:37 04/03/16 18:06 14-Nitroaniline 2.1 U
13 1.3 mg/Kg 03/24/16 17:37 04/03/16 18:06 12-Chlorophenol 1.3 U
13 1.3 mg/Kg 03/24/16 17:37 04/03/16 18:06 12,4-Dichlorophenol 1.3 U
13 1.3 mg/Kg 03/24/16 17:37 04/03/16 18:06 12,6-Dichlorophenol 1.3 U
13 1.3 mg/Kg 03/24/16 17:37 04/03/16 18:06 12,4-Dimethylphenol 1.3 U
38 11 mg/Kg 03/24/16 17:37 04/03/16 18:06 12,4-Dinitrophenol 11 U
13 1.3 mg/Kg 03/24/16 17:37 04/03/16 18:06 12-Methylphenol 1.3 U
13 1.3 mg/Kg 03/24/16 17:37 04/03/16 18:06 12-Nitrophenol 1.3 U
26 2.6 mg/Kg 03/24/16 17:37 04/03/16 18:06 1Pentachlorophenol 2.6 U
13 1.3 mg/Kg 03/24/16 17:37 04/03/16 18:06 1Phenol 2.2 I
26 1.3 mg/Kg 03/24/16 17:37 04/03/16 18:06 13 & 4 Methylphenol 1.3 U
13 1.3 mg/Kg 03/24/16 17:37 04/03/16 18:06 12,4,5-Trichlorophenol 1.3 U
13 1.3 mg/Kg 03/24/16 17:37 04/03/16 18:06 12,4,6-Trichlorophenol 1.3 U
13 0.77 mg/Kg 03/24/16 17:37 04/03/16 18:06 1Benzo[a]anthracene 0.77 U
13 0.77 mg/Kg 03/24/16 17:37 04/03/16 18:06 1Benzo[a]pyrene 0.77 U
13 0.97 mg/Kg 03/24/16 17:37 04/03/16 18:06 1Benzo[b]fluoranthene 0.97 U
13 1.2 mg/Kg 03/24/16 17:37 04/03/16 18:06 1Benzo[g,h,i]perylene 1.2 U
13 0.85 mg/Kg 03/24/16 17:37 04/03/16 18:06 1Benzo[k]fluoranthene 0.85 U
13 1.9 mg/Kg 03/24/16 17:37 04/03/16 18:06 1Benzyl alcohol 1.9 U
13 1.3 mg/Kg 03/24/16 17:37 04/03/16 18:06 1Butyl benzyl phthalate 3.0 I
13 1.3 mg/Kg 03/24/16 17:37 04/03/16 18:06 1Bis(2-chloroethoxy)methane 1.3 U
13 1.3 mg/Kg 03/24/16 17:37 04/03/16 18:06 1Bis(2-chloroethyl)ether 1.3 U
13 1.3 mg/Kg 03/24/16 17:37 04/03/16 18:06 1Bis(2-ethylhexyl) phthalate 3.0 I
13 0.85 mg/Kg 03/24/16 17:37 04/03/16 18:06 1Chrysene 0.85 U
13 0.97 mg/Kg 03/24/16 17:37 04/03/16 18:06 1Dibenz(a,h)anthracene 0.97 U
13 1.3 mg/Kg 03/24/16 17:37 04/03/16 18:06 1Dibenzofuran 1.3 U
13 1.3 mg/Kg 03/24/16 17:37 04/03/16 18:06 1Di-n-butyl phthalate 1.3 U
13 1.3 mg/Kg 03/24/16 17:37 04/03/16 18:06 1Di-n-octyl phthalate 1.3 U
13 0.97 mg/Kg 03/24/16 17:37 04/03/16 18:06 1Fluoranthene 0.97 U
13 0.77 mg/Kg 03/24/16 17:37 04/03/16 18:06 1Fluorene 0.77 U
13 3.9 mg/Kg 03/24/16 17:37 04/03/16 18:06 1Hexachlorobenzene 3.9 U
13 1.3 mg/Kg 03/24/16 17:37 04/03/16 18:06 1Hexachlorobutadiene 1.3 U
13 2.6 mg/Kg 03/24/16 17:37 04/03/16 18:06 1Hexachlorocyclopentadiene 2.6 U
13 3.9 mg/Kg 03/24/16 17:37 04/03/16 18:06 1Hexachloroethane 3.9 U
13 0.97 mg/Kg 03/24/16 17:37 04/03/16 18:06 1Indeno[1,2,3-cd]pyrene 0.97 U
13 1.3 mg/Kg 03/24/16 17:37 04/03/16 18:06 1Isophorone 1.3 U
13 0.85 mg/Kg 03/24/16 17:37 04/03/16 18:06 1Naphthalene 0.85 U
13 2.6 mg/Kg 03/24/16 17:37 04/03/16 18:06 1N-Nitrosodi-n-butylamine 2.6 U
TestAmerica Pensacola
Page 14 of 59 4/7/2016
SDG: WASTE CHARACTERIZATIONProject/Site: Tyndall AFB
Lab Sample ID: 400-119007-5Client Sample ID: LO/CRF-SBAY 1ST STAGE TOP Matrix: SolidDate Collected: 03/16/16 10:15
Date Received: 03/17/16 09:23
Method: 8270C - Semivolatile Organic Compounds (GC/MS) (Continued)
PQL MDL
N-Nitrosodimethylamine 2.6 U 13 2.6 mg/Kg 03/24/16 17:37 04/03/16 18:06 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
13 1.3 mg/Kg 03/24/16 17:37 04/03/16 18:06 1N-Nitrosodiphenylamine 1.3 U
13 4.3 mg/Kg 03/24/16 17:37 04/03/16 18:06 1N-Nitrosodi-n-propylamine 4.3 U
13 0.77 mg/Kg 03/24/16 17:37 04/03/16 18:06 1Phenanthrene 0.77 U
13 0.97 mg/Kg 03/24/16 17:37 04/03/16 18:06 1Pyrene 0.97 U
13 1.3 mg/Kg 03/24/16 17:37 04/03/16 18:06 11,2-Dichlorobenzene 1.3 U
13 1.3 mg/Kg 03/24/16 17:37 04/03/16 18:06 11,3-Dichlorobenzene 1.3 U
13 1.3 mg/Kg 03/24/16 17:37 04/03/16 18:06 11,4-Dichlorobenzene 1.3 U
13 1.3 mg/Kg 03/24/16 17:37 04/03/16 18:06 12-Chloronaphthalene 1.3 U
13 6.0 mg/Kg 03/24/16 17:37 04/03/16 18:06 13,3'-Dichlorobenzidine 6.0 U
13 1.3 mg/Kg 03/24/16 17:37 04/03/16 18:06 1Diethyl phthalate 5.1 I
13 1.3 mg/Kg 03/24/16 17:37 04/03/16 18:06 1Dimethyl phthalate 1.3 U
13 1.3 mg/Kg 03/24/16 17:37 04/03/16 18:06 12,4-Dinitrotoluene 1.3 U
13 1.3 mg/Kg 03/24/16 17:37 04/03/16 18:06 12,6-Dinitrotoluene 1.3 U
13 0.77 mg/Kg 03/24/16 17:37 04/03/16 18:06 11-Methylnaphthalene 0.77 U
13 0.70 mg/Kg 03/24/16 17:37 04/03/16 18:06 12-Methylnaphthalene 0.70 U
13 1.3 mg/Kg 03/24/16 17:37 04/03/16 18:06 12-Nitroaniline 1.3 U
13 1.5 mg/Kg 03/24/16 17:37 04/03/16 18:06 13-Nitroaniline 1.5 U
13 1.3 mg/Kg 03/24/16 17:37 04/03/16 18:06 1Nitrobenzene 1.3 U
13 1.3 mg/Kg 03/24/16 17:37 04/03/16 18:06 11,2,4-Trichlorobenzene 1.3 U
13 1.3 mg/Kg 03/24/16 17:37 04/03/16 18:06 1bis (2-chloroisopropyl) ether 1.3 U
13 1.3 mg/Kg 03/24/16 17:37 04/03/16 18:06 11,2-Diphenylhydrazine (as
Azobenzene)
1.3 U
2,4,6-Tribromophenol 67 32 - 133 03/24/16 17:37 04/03/16 18:06 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
2-Fluorobiphenyl 70 03/24/16 17:37 04/03/16 18:06 144 - 120
2-Fluorophenol 41 03/24/16 17:37 04/03/16 18:06 125 - 120
Nitrobenzene-d5 58 03/24/16 17:37 04/03/16 18:06 127 - 120
Phenol-d5 52 03/24/16 17:37 04/03/16 18:06 137 - 120
Terphenyl-d14 94 03/24/16 17:37 04/03/16 18:06 136 - 134
Method: 6010B - Metals (ICP) - TCLP
PQL MDL
Arsenic 0.020 U 0.025 0.020 mg/L 04/01/16 09:41 04/01/16 17:19 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
5.0 0.050 mg/L 04/01/16 09:41 04/01/16 17:19 1Barium 0.12 I
0.050 0.010 mg/L 04/01/16 09:41 04/01/16 17:19 1Chromium 0.20
0.025 0.010 mg/L 04/01/16 09:41 04/01/16 17:19 1Lead 0.010 U
0.10 0.020 mg/L 04/01/16 09:41 04/01/16 17:19 1Selenium 0.020 U
0.025 0.010 mg/L 04/01/16 09:41 04/01/16 17:19 1Silver 0.18
Method: 6010B - Metals (ICP) - TCLP - DL
PQL MDL
Cadmium 0.025 U 0.13 0.025 mg/L 04/01/16 09:41 04/03/16 14:14 5
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
Method: 7470A - Mercury (CVAA) - TCLP
PQL MDL
Mercury 0.00078 I 0.0016 0.00056 mg/L 03/31/16 13:32 04/01/16 13:20 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
TestAmerica Pensacola
Page 15 of 59 4/7/2016
SDG: WASTE CHARACTERIZATIONProject/Site: Tyndall AFB
Lab Sample ID: 400-119007-6Client Sample ID: LO/CRF-SBAY 2ND STAGE BOTTOM Matrix: SolidDate Collected: 03/16/16 10:20
Date Received: 03/17/16 09:23
Method: 8270C - Semivolatile Organic Compounds (GC/MS)
PQL MDL
Benzoic acid 290 U 830 290 mg/Kg 03/24/16 17:37 04/03/16 18:43 20
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
280 17 mg/Kg 03/24/16 17:37 04/03/16 18:43 20Acenaphthene 17 U
280 17 mg/Kg 03/24/16 17:37 04/03/16 18:43 20Acenaphthylene 17 U
280 17 mg/Kg 03/24/16 17:37 04/03/16 18:43 20Anthracene 17 U
830 83 mg/Kg 03/24/16 17:37 04/03/16 18:43 20Benzidine 83 U
280 28 mg/Kg 03/24/16 17:37 04/03/16 18:43 204-Chloro-3-methylphenol 28 U
280 50 mg/Kg 03/24/16 17:37 04/03/16 18:43 204,6-Dinitro-2-methylphenol 50 U
280 130 mg/Kg 03/24/16 17:37 04/03/16 18:43 204-Nitrophenol 130 U
280 28 mg/Kg 03/24/16 17:37 04/03/16 18:43 204-Bromophenyl phenyl ether 28 U
280 67 mg/Kg 03/24/16 17:37 04/03/16 18:43 204-Chloroaniline 67 U
280 28 mg/Kg 03/24/16 17:37 04/03/16 18:43 204-Chlorophenyl phenyl ether 28 U
280 46 mg/Kg 03/24/16 17:37 04/03/16 18:43 204-Nitroaniline 46 U
280 28 mg/Kg 03/24/16 17:37 04/03/16 18:43 202-Chlorophenol 28 U
280 28 mg/Kg 03/24/16 17:37 04/03/16 18:43 202,4-Dichlorophenol 28 U
280 28 mg/Kg 03/24/16 17:37 04/03/16 18:43 202,6-Dichlorophenol 28 U
280 28 mg/Kg 03/24/16 17:37 04/03/16 18:43 202,4-Dimethylphenol 28 U
830 240 mg/Kg 03/24/16 17:37 04/03/16 18:43 202,4-Dinitrophenol 240 U
280 28 mg/Kg 03/24/16 17:37 04/03/16 18:43 202-Methylphenol 28 U
280 28 mg/Kg 03/24/16 17:37 04/03/16 18:43 202-Nitrophenol 28 U
550 55 mg/Kg 03/24/16 17:37 04/03/16 18:43 20Pentachlorophenol 55 U
280 28 mg/Kg 03/24/16 17:37 04/03/16 18:43 20Phenol 28 U
550 28 mg/Kg 03/24/16 17:37 04/03/16 18:43 203 & 4 Methylphenol 28 U
280 28 mg/Kg 03/24/16 17:37 04/03/16 18:43 202,4,5-Trichlorophenol 28 U
280 28 mg/Kg 03/24/16 17:37 04/03/16 18:43 202,4,6-Trichlorophenol 28 U
280 17 mg/Kg 03/24/16 17:37 04/03/16 18:43 20Benzo[a]anthracene 17 U
280 17 mg/Kg 03/24/16 17:37 04/03/16 18:43 20Benzo[a]pyrene 17 U
280 21 mg/Kg 03/24/16 17:37 04/03/16 18:43 20Benzo[b]fluoranthene 21 U
280 25 mg/Kg 03/24/16 17:37 04/03/16 18:43 20Benzo[g,h,i]perylene 25 U
280 18 mg/Kg 03/24/16 17:37 04/03/16 18:43 20Benzo[k]fluoranthene 18 U
280 42 mg/Kg 03/24/16 17:37 04/03/16 18:43 20Benzyl alcohol 42 U
280 28 mg/Kg 03/24/16 17:37 04/03/16 18:43 20Butyl benzyl phthalate 28 U
280 28 mg/Kg 03/24/16 17:37 04/03/16 18:43 20Bis(2-chloroethoxy)methane 28 U
280 28 mg/Kg 03/24/16 17:37 04/03/16 18:43 20Bis(2-chloroethyl)ether 28 U
280 28 mg/Kg 03/24/16 17:37 04/03/16 18:43 20Bis(2-ethylhexyl) phthalate 28 U
280 18 mg/Kg 03/24/16 17:37 04/03/16 18:43 20Chrysene 18 U
280 21 mg/Kg 03/24/16 17:37 04/03/16 18:43 20Dibenz(a,h)anthracene 21 U
280 28 mg/Kg 03/24/16 17:37 04/03/16 18:43 20Dibenzofuran 28 U
280 28 mg/Kg 03/24/16 17:37 04/03/16 18:43 20Di-n-butyl phthalate 28 U
280 28 mg/Kg 03/24/16 17:37 04/03/16 18:43 20Di-n-octyl phthalate 28 U
280 21 mg/Kg 03/24/16 17:37 04/03/16 18:43 20Fluoranthene 21 U
280 17 mg/Kg 03/24/16 17:37 04/03/16 18:43 20Fluorene 17 U
280 84 mg/Kg 03/24/16 17:37 04/03/16 18:43 20Hexachlorobenzene 84 U
280 28 mg/Kg 03/24/16 17:37 04/03/16 18:43 20Hexachlorobutadiene 28 U
280 55 mg/Kg 03/24/16 17:37 04/03/16 18:43 20Hexachlorocyclopentadiene 55 U
280 84 mg/Kg 03/24/16 17:37 04/03/16 18:43 20Hexachloroethane 84 U
280 21 mg/Kg 03/24/16 17:37 04/03/16 18:43 20Indeno[1,2,3-cd]pyrene 21 U
280 28 mg/Kg 03/24/16 17:37 04/03/16 18:43 20Isophorone 28 U
280 18 mg/Kg 03/24/16 17:37 04/03/16 18:43 20Naphthalene 18 U
280 55 mg/Kg 03/24/16 17:37 04/03/16 18:43 20N-Nitrosodi-n-butylamine 55 U
TestAmerica Pensacola
Page 16 of 59 4/7/2016
SDG: WASTE CHARACTERIZATIONProject/Site: Tyndall AFB
Lab Sample ID: 400-119007-6Client Sample ID: LO/CRF-SBAY 2ND STAGE BOTTOM Matrix: SolidDate Collected: 03/16/16 10:20
Date Received: 03/17/16 09:23
Method: 8270C - Semivolatile Organic Compounds (GC/MS) (Continued)
PQL MDL
N-Nitrosodimethylamine 55 U 280 55 mg/Kg 03/24/16 17:37 04/03/16 18:43 20
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
280 28 mg/Kg 03/24/16 17:37 04/03/16 18:43 20N-Nitrosodiphenylamine 28 U
280 92 mg/Kg 03/24/16 17:37 04/03/16 18:43 20N-Nitrosodi-n-propylamine 92 U
280 17 mg/Kg 03/24/16 17:37 04/03/16 18:43 20Phenanthrene 17 U
280 21 mg/Kg 03/24/16 17:37 04/03/16 18:43 20Pyrene 21 U
280 28 mg/Kg 03/24/16 17:37 04/03/16 18:43 201,2-Dichlorobenzene 28 U
280 28 mg/Kg 03/24/16 17:37 04/03/16 18:43 201,3-Dichlorobenzene 28 U
280 28 mg/Kg 03/24/16 17:37 04/03/16 18:43 201,4-Dichlorobenzene 28 U
280 28 mg/Kg 03/24/16 17:37 04/03/16 18:43 202-Chloronaphthalene 28 U
280 130 mg/Kg 03/24/16 17:37 04/03/16 18:43 203,3'-Dichlorobenzidine 130 U
280 28 mg/Kg 03/24/16 17:37 04/03/16 18:43 20Diethyl phthalate 28 U
280 28 mg/Kg 03/24/16 17:37 04/03/16 18:43 20Dimethyl phthalate 28 U
280 28 mg/Kg 03/24/16 17:37 04/03/16 18:43 202,4-Dinitrotoluene 28 U
280 28 mg/Kg 03/24/16 17:37 04/03/16 18:43 202,6-Dinitrotoluene 28 U
280 17 mg/Kg 03/24/16 17:37 04/03/16 18:43 201-Methylnaphthalene 17 U
280 15 mg/Kg 03/24/16 17:37 04/03/16 18:43 202-Methylnaphthalene 15 U
280 28 mg/Kg 03/24/16 17:37 04/03/16 18:43 202-Nitroaniline 28 U
280 34 mg/Kg 03/24/16 17:37 04/03/16 18:43 203-Nitroaniline 34 U
280 28 mg/Kg 03/24/16 17:37 04/03/16 18:43 20Nitrobenzene 28 U
280 28 mg/Kg 03/24/16 17:37 04/03/16 18:43 201,2,4-Trichlorobenzene 28 U
280 28 mg/Kg 03/24/16 17:37 04/03/16 18:43 20bis (2-chloroisopropyl) ether 28 U
280 28 mg/Kg 03/24/16 17:37 04/03/16 18:43 201,2-Diphenylhydrazine (as
Azobenzene)
28 U
2,4,6-Tribromophenol 0 J1 32 - 133 03/24/16 17:37 04/03/16 18:43 20
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
2-Fluorobiphenyl 0 J1 03/24/16 17:37 04/03/16 18:43 2044 - 120
2-Fluorophenol 24 J1 03/24/16 17:37 04/03/16 18:43 2025 - 120
Nitrobenzene-d5 39 03/24/16 17:37 04/03/16 18:43 2027 - 120
Phenol-d5 30 J1 03/24/16 17:37 04/03/16 18:43 2037 - 120
Terphenyl-d14 64 03/24/16 17:37 04/03/16 18:43 2036 - 134
Method: 6010B - Metals (ICP) - TCLP
PQL MDL
Arsenic 0.020 U 0.025 0.020 mg/L 04/01/16 09:41 04/01/16 17:23 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
5.0 0.050 mg/L 04/01/16 09:41 04/01/16 17:23 1Barium 0.15 I
0.025 0.0050 mg/L 04/01/16 09:41 04/01/16 17:23 1Cadmium 0.0050 U
0.050 0.010 mg/L 04/01/16 09:41 04/01/16 17:23 1Chromium 0.57
0.025 0.010 mg/L 04/01/16 09:41 04/01/16 17:23 1Lead 0.010 U
0.10 0.020 mg/L 04/01/16 09:41 04/01/16 17:23 1Selenium 0.020 U
0.025 0.010 mg/L 04/01/16 09:41 04/01/16 17:23 1Silver 0.13
Method: 7470A - Mercury (CVAA) - TCLP
PQL MDL
Mercury 0.00056 U 0.0016 0.00056 mg/L 03/31/16 13:32 04/01/16 13:21 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
TestAmerica Pensacola
Page 17 of 59 4/7/2016
SDG: WASTE CHARACTERIZATIONProject/Site: Tyndall AFB
Lab Sample ID: 400-119007-7Client Sample ID: LO/CRF-SBAY 3RD STAGE BOTTOM Matrix: SolidDate Collected: 03/16/16 10:30
Date Received: 03/17/16 09:23
Method: 8270C - Semivolatile Organic Compounds (GC/MS)
PQL MDL
Benzoic acid 260 U 750 260 mg/Kg 03/24/16 17:37 04/03/16 15:38 20
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
250 15 mg/Kg 03/24/16 17:37 04/03/16 15:38 20Acenaphthene 15 U
250 15 mg/Kg 03/24/16 17:37 04/03/16 15:38 20Acenaphthylene 15 U
250 15 mg/Kg 03/24/16 17:37 04/03/16 15:38 20Anthracene 15 U
750 75 mg/Kg 03/24/16 17:37 04/03/16 15:38 20Benzidine 75 U
250 25 mg/Kg 03/24/16 17:37 04/03/16 15:38 204-Chloro-3-methylphenol 25 U
250 45 mg/Kg 03/24/16 17:37 04/03/16 15:38 204,6-Dinitro-2-methylphenol 45 U
250 110 mg/Kg 03/24/16 17:37 04/03/16 15:38 204-Nitrophenol 110 U
250 25 mg/Kg 03/24/16 17:37 04/03/16 15:38 204-Bromophenyl phenyl ether 25 U
250 60 mg/Kg 03/24/16 17:37 04/03/16 15:38 204-Chloroaniline 60 U
250 25 mg/Kg 03/24/16 17:37 04/03/16 15:38 204-Chlorophenyl phenyl ether 25 U
250 41 mg/Kg 03/24/16 17:37 04/03/16 15:38 204-Nitroaniline 41 U
250 25 mg/Kg 03/24/16 17:37 04/03/16 15:38 202-Chlorophenol 25 U
250 25 mg/Kg 03/24/16 17:37 04/03/16 15:38 202,4-Dichlorophenol 25 U
250 25 mg/Kg 03/24/16 17:37 04/03/16 15:38 202,6-Dichlorophenol 25 U
250 25 mg/Kg 03/24/16 17:37 04/03/16 15:38 202,4-Dimethylphenol 25 U
750 220 mg/Kg 03/24/16 17:37 04/03/16 15:38 202,4-Dinitrophenol 220 U
250 25 mg/Kg 03/24/16 17:37 04/03/16 15:38 202-Methylphenol 25 U
250 25 mg/Kg 03/24/16 17:37 04/03/16 15:38 202-Nitrophenol 25 U
500 50 mg/Kg 03/24/16 17:37 04/03/16 15:38 20Pentachlorophenol 50 U
250 25 mg/Kg 03/24/16 17:37 04/03/16 15:38 20Phenol 25 U
500 25 mg/Kg 03/24/16 17:37 04/03/16 15:38 203 & 4 Methylphenol 25 U
250 25 mg/Kg 03/24/16 17:37 04/03/16 15:38 202,4,5-Trichlorophenol 25 U
250 25 mg/Kg 03/24/16 17:37 04/03/16 15:38 202,4,6-Trichlorophenol 25 U
250 15 mg/Kg 03/24/16 17:37 04/03/16 15:38 20Benzo[a]anthracene 15 U
250 15 mg/Kg 03/24/16 17:37 04/03/16 15:38 20Benzo[a]pyrene 15 U
250 19 mg/Kg 03/24/16 17:37 04/03/16 15:38 20Benzo[b]fluoranthene 19 U
250 23 mg/Kg 03/24/16 17:37 04/03/16 15:38 20Benzo[g,h,i]perylene 23 U
250 17 mg/Kg 03/24/16 17:37 04/03/16 15:38 20Benzo[k]fluoranthene 17 U
250 38 mg/Kg 03/24/16 17:37 04/03/16 15:38 20Benzyl alcohol 38 U
250 25 mg/Kg 03/24/16 17:37 04/03/16 15:38 20Butyl benzyl phthalate 25 U
250 25 mg/Kg 03/24/16 17:37 04/03/16 15:38 20Bis(2-chloroethoxy)methane 25 U
250 25 mg/Kg 03/24/16 17:37 04/03/16 15:38 20Bis(2-chloroethyl)ether 25 U
250 25 mg/Kg 03/24/16 17:37 04/03/16 15:38 20Bis(2-ethylhexyl) phthalate 25 U
250 17 mg/Kg 03/24/16 17:37 04/03/16 15:38 20Chrysene 17 U
250 19 mg/Kg 03/24/16 17:37 04/03/16 15:38 20Dibenz(a,h)anthracene 19 U
250 25 mg/Kg 03/24/16 17:37 04/03/16 15:38 20Dibenzofuran 25 U
250 25 mg/Kg 03/24/16 17:37 04/03/16 15:38 20Di-n-butyl phthalate 25 U
250 25 mg/Kg 03/24/16 17:37 04/03/16 15:38 20Di-n-octyl phthalate 25 U
250 19 mg/Kg 03/24/16 17:37 04/03/16 15:38 20Fluoranthene 19 U
250 15 mg/Kg 03/24/16 17:37 04/03/16 15:38 20Fluorene 15 U
250 75 mg/Kg 03/24/16 17:37 04/03/16 15:38 20Hexachlorobenzene 75 U
250 25 mg/Kg 03/24/16 17:37 04/03/16 15:38 20Hexachlorobutadiene 25 U
250 50 mg/Kg 03/24/16 17:37 04/03/16 15:38 20Hexachlorocyclopentadiene 50 U
250 75 mg/Kg 03/24/16 17:37 04/03/16 15:38 20Hexachloroethane 75 U
250 19 mg/Kg 03/24/16 17:37 04/03/16 15:38 20Indeno[1,2,3-cd]pyrene 19 U
250 25 mg/Kg 03/24/16 17:37 04/03/16 15:38 20Isophorone 25 U
250 17 mg/Kg 03/24/16 17:37 04/03/16 15:38 20Naphthalene 17 U
250 50 mg/Kg 03/24/16 17:37 04/03/16 15:38 20N-Nitrosodi-n-butylamine 50 U
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Page 18 of 59 4/7/2016
SDG: WASTE CHARACTERIZATIONProject/Site: Tyndall AFB
Lab Sample ID: 400-119007-7Client Sample ID: LO/CRF-SBAY 3RD STAGE BOTTOM Matrix: SolidDate Collected: 03/16/16 10:30
Date Received: 03/17/16 09:23
Method: 8270C - Semivolatile Organic Compounds (GC/MS) (Continued)
PQL MDL
N-Nitrosodimethylamine 50 U 250 50 mg/Kg 03/24/16 17:37 04/03/16 15:38 20
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
250 25 mg/Kg 03/24/16 17:37 04/03/16 15:38 20N-Nitrosodiphenylamine 25 U
250 83 mg/Kg 03/24/16 17:37 04/03/16 15:38 20N-Nitrosodi-n-propylamine 83 U
250 15 mg/Kg 03/24/16 17:37 04/03/16 15:38 20Phenanthrene 15 U
250 19 mg/Kg 03/24/16 17:37 04/03/16 15:38 20Pyrene 19 U
250 25 mg/Kg 03/24/16 17:37 04/03/16 15:38 201,2-Dichlorobenzene 25 U
250 25 mg/Kg 03/24/16 17:37 04/03/16 15:38 201,3-Dichlorobenzene 25 U
250 25 mg/Kg 03/24/16 17:37 04/03/16 15:38 201,4-Dichlorobenzene 25 U
250 25 mg/Kg 03/24/16 17:37 04/03/16 15:38 202-Chloronaphthalene 25 U
250 120 mg/Kg 03/24/16 17:37 04/03/16 15:38 203,3'-Dichlorobenzidine 120 U
250 25 mg/Kg 03/24/16 17:37 04/03/16 15:38 20Diethyl phthalate 25 U
250 25 mg/Kg 03/24/16 17:37 04/03/16 15:38 20Dimethyl phthalate 25 U
250 25 mg/Kg 03/24/16 17:37 04/03/16 15:38 202,4-Dinitrotoluene 25 U
250 25 mg/Kg 03/24/16 17:37 04/03/16 15:38 202,6-Dinitrotoluene 25 U
250 15 mg/Kg 03/24/16 17:37 04/03/16 15:38 201-Methylnaphthalene 15 U
250 14 mg/Kg 03/24/16 17:37 04/03/16 15:38 202-Methylnaphthalene 14 U
250 25 mg/Kg 03/24/16 17:37 04/03/16 15:38 202-Nitroaniline 25 U
250 30 mg/Kg 03/24/16 17:37 04/03/16 15:38 203-Nitroaniline 30 U
250 25 mg/Kg 03/24/16 17:37 04/03/16 15:38 20Nitrobenzene 25 U
250 25 mg/Kg 03/24/16 17:37 04/03/16 15:38 201,2,4-Trichlorobenzene 25 U
250 25 mg/Kg 03/24/16 17:37 04/03/16 15:38 20bis (2-chloroisopropyl) ether 25 U
250 25 mg/Kg 03/24/16 17:37 04/03/16 15:38 201,2-Diphenylhydrazine (as
Azobenzene)
25 U
2,4,6-Tribromophenol 188 J1 32 - 133 03/24/16 17:37 04/03/16 15:38 20
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
2-Fluorobiphenyl 30 J1 03/24/16 17:37 04/03/16 15:38 2044 - 120
2-Fluorophenol 53 03/24/16 17:37 04/03/16 15:38 2025 - 120
Nitrobenzene-d5 89 03/24/16 17:37 04/03/16 15:38 2027 - 120
Phenol-d5 85 03/24/16 17:37 04/03/16 15:38 2037 - 120
Terphenyl-d14 163 J1 03/24/16 17:37 04/03/16 15:38 2036 - 134
Method: 6010B - Metals (ICP) - TCLP
PQL MDL
Arsenic 0.020 U 0.025 0.020 mg/L 04/01/16 09:41 04/01/16 17:26 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
5.0 0.050 mg/L 04/01/16 09:41 04/01/16 17:26 1Barium 0.20 I
0.025 0.0050 mg/L 04/01/16 09:41 04/01/16 17:26 1Cadmium 0.0050 U
0.050 0.010 mg/L 04/01/16 09:41 04/01/16 17:26 1Chromium 0.71
0.025 0.010 mg/L 04/01/16 09:41 04/01/16 17:26 1Lead 0.023 I
0.10 0.020 mg/L 04/01/16 09:41 04/01/16 17:26 1Selenium 0.034 I
0.025 0.010 mg/L 04/01/16 09:41 04/01/16 17:26 1Silver 0.15
Method: 7470A - Mercury (CVAA) - TCLP
PQL MDL
Mercury 0.00056 U 0.0016 0.00056 mg/L 03/31/16 13:32 04/01/16 13:22 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
TestAmerica Pensacola
Page 19 of 59 4/7/2016
| 1. Cover Page |
| 2. Table of Contents |
| 3. Case Narrative |
| 4. Method Summary |
| 5. Sample Summary |
| 6. Client Sample Results |
| 7. Definitions |
| 8. Chronicle |
| 9. QC Association |
| 10. QC Sample Results |
| 11. Chain of Custody |
| 12. Receipt Checklists |
| 13. Certification Summary |
File details come from the government source that posted it. Updated .