Attachment - AL-Oxide TCLP 2022.pdf

07/25/22

Technical Report for

HazTrain, Inc.

Joint Base McGuire Dix, Lakehurst,NJ Haz Waste

SGS Job Number: JD48247

Sampling Date: 07/13/22

Report to:

Haz Train 3460 Rockefeller Court Waldrof, MD 20602 timczysz@haztrain.com

ATTN: Tim Czysz

Total number of pages in report:

Certifications: NJ(12129), NY(10983), CA, CT, FL, IL, IN, KS, KY, LA, MA, MD, ME, MN, NC, OH VAP (CL0056), AK (UST-103), AZ (AZ0786), PA(68-00408), RI, SC, TX, UT, VA, WV

This report shall not be reproduced, except in its entirety, without the written approval of SGS.

Test results relate only to samples analyzed.

SGS North America Inc. • 2235 Route 130 • Dayton, NJ 08810 • tel: 732-329-0200 • fax: 732-329-3499

Test results contained within this data package meet the requirements of the National Environmental Laboratory Accreditation Program and/or state specific certification programs as applicable.

Client Service contact: Jadon Schiller 732-329-0200

David Chastain General Manager

Dayton, NJ 07/25/22 e-Hardcopy 2.0 Automated Report

SGS is the sole authority for authorizing edits or modifications to this document.

Unauthorized modification of this report is strictly prohibited.

Review standard terms at: http://www.sgs.com/en/terms-and-conditions

The results set forth herein are provided by SGS North America Inc.

Please share your ideas about how we can serve you better at:

EHS.US.CustomerCare@sgs.com

JD48247

mailto:EHS.US.CustomerCare@sgs.com?subject=Customer care improvement idea (report JD48247)

Table of Contents -1-

Sections:

Section 1: Sample Summary Section 2: Case Narrative/Conformance Summary Section 3: Summary of Hits Section 4: Sample Results

4.1: JD48247-1: ALUMINUM OXIDE

Section 5: Misc. Forms

5.1: Chain of Custody 5.2: Sample Tracking Chronicle 5.3: Internal Chain of Custody

Section 6: Metals Analysis - QC Data Summaries 6.1: Inst QC MA52735: Hg 6.2: Inst QC MA52760: As,Ba,Cd,Cr,Pb,Se,Ag 6.3: Prep QC MP34146: Hg 6.4: Prep QC MP34149: As,Ba,Cd,Cr,Pb,Se,Ag

SGS North America Inc.

Sample Summary

HazTrain, Inc.

Job No: JD48247

Joint Base McGuire Dix, Lakehurst,NJ Haz Waste

Sample Collected Matrix Client Number Date Time By Received Code Type Sample ID

JD48247-1 07/13/22 10:10 HH 07/13/22 SO Soil ALUMINUM OXIDE

Soil samples reported on a dry weight basis unless otherwise indicated on result page.

On 07/13/2022, 1 Sample(s), 0 Trip Blank(s) and 0 Field Blank(s) were received at SGS North America Inc. at a maximum corrected temperature of 3.9 C. Samples were intact and chemically preserved, unless noted below. A SGS North America Inc. Job Number of JD48247 was assigned to the project. Laboratory sample ID, client sample ID and dates of sample collection are detailed in the report’s Results Summary Section.

Specified quality control criteria were achieved for this job except as noted below. For more information, please refer to the analytical results and QC summary pages.

Client: HazTrain, Inc.

Site: Joint Base McGuire Dix, Lakehurst,NJ Haz Waste

Job No JD48247

Report Date 7/25/2022 9:33:18 AM

CASE NARRATIVE / CONFORMANCE SUMMARY

Compounds qualified as out of range in the continuing calibration summary report are acceptable as per method requirements when there is a high bias but the sample result is non-detect.

Metals Analysis By Method SW846 6010D Matrix: LEACHATE Batch ID: MP34149

All samples were digested within the recommended method holding time.

All method blanks for this batch meet method specific criteria.

Sample(s) JD48265-1MS, JD48265-1MSD, JD48265-1SDL were used as the QC samples for metals.

RPD(s) for Serial Dilution for Arsenic, Cadmium, Chromium, Lead, Silver are outside control limits for sample MP34149- SD1. Percent difference acceptable due to low initial sample concentration (< 50 times IDL).

Metals Analysis By Method SW846 7470A Matrix: LEACHATE Batch ID: MP34146

All samples were digested within the recommended method holding time.

All method blanks for this batch meet method specific criteria.

Sample(s) JD48265-1MS, JD48265-1MSD were used as the QC samples for metals.

SGS North America Inc. certifies that data reported for samples received, listed on the associated custody chain or analytical task order, were produced to specifications meeting the Quality System precision, accuracy and completeness objectives except as noted.

Estimated non-standard method measurement uncertainty data is available on request, based on quality control bias and implicit for standard methods. Acceptable uncertainty requires tested parameter quality control data to meet method criteria.

SGS North America Inc. is not responsible for data quality assumptions if partial reports are used and recommends that this report be used in its entirety. Data release is authorized by SGS North America Inc indicated via signature on the report cover

Monday, July 25, 2022 Page 1 of 1

Summary of Hits Page 1 of 1 Job Number: JD48247 Account: HazTrain, Inc.

Project: Joint Base McGuire Dix, Lakehurst,NJ Haz Waste Collected: 07/13/22

Lab Sample ID Client Sample ID Result/ Analyte Qual RL MDL Units Method

JD48247-1 ALUMINUM OXIDE

Barium 0.91 0.20 mg/l SW846 6010D Cadmium 0.0095 0.0040 mg/l SW846 6010D Chromium 1.1 0.010 mg/l SW846 6010D Mercury 0.00022 0.00020 mg/l SW846 7470A

Sample Results

Report of Analysis

Dayton, NJ Section 4

Report of Analysis Page 1 of 1

Client Sample ID: ALUMINUM OXIDE Lab Sample ID: JD48247-1 Date Sampled: 07/13/22 Matrix: SO - Soil Date Received: 07/13/22

Percent Solids: n/a Project: Joint Base McGuire Dix, Lakehurst,NJ Haz Waste

Metals Analysis, TCLP Leachate SW846 1311

Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method

Arsenic <0.10 D004 5.0 0.10 mg/l 1 07/21/22 07/22/22 ND SW846 6010D 2 SW846 3010A 4

Barium 0.91 D005 100 0.20 mg/l 1 07/21/22 07/22/22 ND SW846 6010D 2 SW846 3010A 4

Cadmium 0.0095 D006 1.0 0.0040 mg/l 1 07/21/22 07/22/22 ND SW846 6010D 2 SW846 3010A 4

Chromium 1.1 D007 5.0 0.010 mg/l 1 07/21/22 07/22/22 ND SW846 6010D 2 SW846 3010A 4

Lead <0.10 D008 5.0 0.10 mg/l 1 07/21/22 07/22/22 ND SW846 6010D 2 SW846 3010A 4

Mercury 0.00022 D009 0.20 0.00020mg/l 1 07/19/22 07/19/22 LM SW846 7470A 1 SW846 7470A 3

Selenium <0.10 D010 1.0 0.10 mg/l 1 07/21/22 07/22/22 ND SW846 6010D 2 SW846 3010A 4

Silver <0.010 D011 5.0 0.010 mg/l 1 07/21/22 07/22/22 ND SW846 6010D 2 SW846 3010A 4

(1) Instrument QC Batch: MA52735

(2) Instrument QC Batch: MA52760

(3) Prep QC Batch: MP34146

(4) Prep QC Batch: MP34149

RL = Reporting Limit MCL = Maximum Contamination Level (40 CFR 261 7/1/11)

JD48247

4.1

Misc. Forms

Custody Documents and Other Forms

Includes the following where applicable:

• Chain of Custody

• Sample Tracking Chronicle

• Internal Chain of Custody

Dayton, NJ Section 5 r

( SG$ CHAIN OF CUST00Y Page_of_

So 0 merica nc. - on

FED-EX Tracking # l~'R'f; T<:.-n-:\-1\17-S'Z, 2235 Route 130, Dayton, NJ 08810 TEL. 732-329-0200 FAX: 732-329-3499/3480 SGS Quote# SGSJo"'1JQ -'-18-< ~ f--EHSA-QAC-0023-04-FORM-Standard COC www.sas.com/ehsusa

SGS N rth A Dayt

Client I Reporting Information Prolect Information Reauested Analvsis Matrix Codes Company Name:

PrJ,~~ef /3u>e h~ f ... ,,s7 J B,#1 /J L )fc. Cv,-< tJrd' DW - Drinking Water GW - Ground Water eit:c; Street - WW-Water

{(,,- ~'17 -- SW - Surface Water Billlna Information fW different from Report to)

SO-Soil

City Stat#J Zip City State Company Name SL- Sludge

.1/711 " SEO-Sediment hheLtf1 ·

01-0il

71/:a;r 4r;:~ Project# Street Address LIQ - Other Liquid

~ AIR-Air SOL - Other Solid

Phone# ?Cl? {"J 5 >16'-( Client Purchase Order# City State Zip --...I WP-Wipe

FB - Field Blank

Sam7;;;

mefj l/o/l'Ji/o/ Phone# Project Manager Attention:

EB-Equipment Blank RB - Rinse Blank TB - Trip Blank

Collection Number of preserved Bottles pH Check {Lab Use Only) w

Source w :c "'

SGS

:c 0 0 0 Sampled Grab(G) Chlorinated 0 z s: 0 (.)

Sample# Field ID I Point of Collection MEOH/DI Vial# Date Time by Comp(C) (YIN) Matrix #oflfttles (3 ~ z ~ 0 15 w z LABUSl!ONLY :c z :c z ::; w

I 11 lu '11 'A J/'YI P".:t-,J.t 7/n/22 tC!o HH Gi > v )( OS"'J I

I

Turn Around Time (Business Days) Deliverable Comments I Soecial Instructions

Approved By (SGS PM): I Data: D Commercial ""A"" (Level 1) D NY ASP Category A D DOD-QSMS

D 1 O Business Days "' D Commercial ""B"" (Level 2) I D NY ASP Category B toltial ."9&W~ ~~Ir D 5 Business Days D NJ Reduced (Level 3) D MA MCP Criteria ___

D 3 Business Days• D Full Tier I (Leval 4) D CT RCP Criteria ___

D 2 Business Days• D Commercial "C" D State Forms ~·V~--~

D 1 Business Day• c NJ DKQP D EDD Format

D Other Commercial "A"= Results only; Commercial "B" =Results+ QC Summary All data available via Lablink •Approval needed for 1-3 B\lalnus Day TAT Commetclal "C'" = Results + QC Summary+ Partial Raw data htto://www.sas.com/en/terms-and-conditions

.)., \: Sample Custody must be documented below each time samples chanae possession, lncludlna courier delivery . ,_ / ,.,,- I -

17Rl~ Data/Time:

~ f2J 7.;3.zz /o;Jr ;·n~ ~ 1- -I)· z.Z D•tj' YJ Received By:

~ l"f'/tJ/J z /oiS 2 . v Relinquished by: Date/Time: Received By: Rellnqulshed By: Date/Time: Received By:

3 3 4 4 Rellnqulshed by: Date/Time: RocolvedBy: Custody Seal # u Intact Therm ID: ~~Cooler Temp. ·c

5 5 D Not intact I Absent D See Sample Receipt Summa

JD48247: Chain of Custody

JD48247

5.1

Job Number: JD48247 Client: HAZ TRAIN

Date / Time Received: 7/13/2022 3:45:00 PM Delivery Method:

Project: JOINT BASE MCGUIRE DIX, LAKEHURST,

4. No. Coolers: 1

Airbill #'s:

Cooler Security

1. Custody Seals Present:

Y or N

2. Custody Seals Intact:

3. COC Present:

4. Smpl Dates/Time OK

2. Cooler temp verification:

Cooler Temperature Y or N

1. Temp criteria achieved:

3. Cooler media:

IR Gun

Ice (Bag)

Quality Control Preservation Y or N N/A

1. Trip Blank present / cooler:

2. Trip Blank listed on COC:

3. Samples preserved properly:

4. VOCs headspace free:

Sample Integrity - Documentation Y or N

1. Sample labels present on bottles:

2. Container labeling complete:

3. Sample container label / COC agree:

Sample Integrity - Condition Y or N

1. Sample recvd within HT:

3. Condition of sample:

2. All containers accounted for:

Sample Integrity - Instructions

1. Analysis requested is clear:

2. Bottles received for unspecified tests

3. Sufficient volume recvd for analysis:

4. Compositing instructions clear:

5. Filtering instructions clear:

Intact

Y or N

Comments

Y or N N/A

Cooler Temps (Raw Measured) °C:

Cooler Temps (Corrected) °C:

Cooler 1: (4.2);

Cooler 1: (3.9);

SM089-03

Rev. Date 12/7/17

SGS Sample Receipt Summary

Test Strip Lot #s: pH 1-12: 231619 pH 12+: 203117A Other: (Specify)

JD48247: Chain of Custody

JD48247

5.1

Internal Sample Tracking Chronicle

HazTrain, Inc.

Job No: JD48247

Joint Base McGuire Dix, Lakehurst,NJ Haz Waste

Sample Number Method Analyzed By Prepped By Test Codes

JD48247-1 Collected: 13-JUL-22 10:10 By: HH Received: 13-JUL-22 By: JP

ALUMINUM OXIDE

JD48247-1 SW846 7470A 19-JUL-22 14:22 LM 19-JUL-22 LM EHG

JD48247-1 SW846 6010D 22-JUL-22 15:59 ND 21-JUL-22 SF EAG,EAS,EBA,ECD,ECR,EPB,ESE

JD48247

5.2

SGS Internal Chain of Custody Page 1 of 1 Job Number: JD48247 Account: HAZTMDW HazTrain, Inc.

Project: Joint Base McGuire Dix, Lakehurst,NJ Haz Waste Received: 07/13/22

Sample.Bottle Transfer Transfer Number FROM TO Date/Time Reason

JD48247-1.1 Rania Salters Secured Storage 07/13/22 22:21 Return to Storage JD48247-1.1 Secured Storage Todd Shoemaker 07/14/22 13:43 Retrieve from Storage JD48247-1.1 Todd Shoemaker Secured Staging Area 07/14/22 13:43 Return to Storage JD48247-1.1 Secured Staging Area Noah Fite 07/14/22 15:23 Retrieve from Storage JD48247-1.1 Noah Fite Secured Storage 07/14/22 17:47 Return to Storage

JD48247-1.1.1 Noah Fite TCLP 07/14/22 15:23 Leachate from JD48247-1.1 JD48247-1.1.1 TCLP Noah Fite 07/15/22 09:06 Leachate from JD48247-1.1 JD48247-1.1.1 Noah Fite Secured Storage 07/15/22 09:06 Return to Storage

JD48247

5.3

Metals Analysis

QC Data Summaries

Includes the following where applicable:

• Instrument Runlogs

• Initial and Continuing Calibration Blanks

• Initial and Continuing Calibration Checks

• High and Low Check Standards

• Interfering Element Check Standards

• Method Blank Summaries

• Matrix Spike and Duplicate Summaries

• Blank Spike and Lab Control Sample Summaries

• Serial Dilution Summaries

Dayton, NJ Section 6

SGS Instrument Runlog Inorganics Analyses

Login Number: JD48247 Account: HAZTMDW - HazTrain, Inc.

Project: Joint Base McGuire Dix, Lakehurst,NJ Haz Waste

File ID: H9071922W1.CSV Date Analyzed: 07/19/22 Methods: SW846 7470A Analyst: LM Run ID: MA52735 Parameters: Hg

Sample Dilution PS Time Description Factor Recov Comments

12:25 MA52735-STD1 1 b=1.5418e-004,c=-1.2836e-002,rho=0.9998229

12:26 MA52735-STD2 1 STDB

12:28 MA52735-STD3 1 STDC

12:29 MA52735-STD4 1 STDD

12:31 MA52735-STD5 1 STDE

12:33 MA52735-STD6 1 STDF

12:38 ZZZZZZ 1

12:39 MA52735-ICV1 1

12:41 MA52735-ICB1 1

12:43 MA52735-CCV1 1

12:44 MA52735-CCB1 1

12:46 MA52735-CRI1 1

12:47 MP34144-MB1 1

12:49 MP34144-B1 1

12:50 MP34144-S1 1

12:52 MP34144-S2 1

12:54 JD48207-1F 1 (sample used for QC only; not part of login JD48247)

12:56 ZZZZZZ 1

12:57 ZZZZZZ 1

12:59 MA52735-CCV2 1

13:01 MA52735-CCB2 1

13:02 ZZZZZZ 1

13:04 ZZZZZZ 1

13:05 ZZZZZZ 1

13:07 ZZZZZZ 1

13:08 ZZZZZZ 1

13:10 ZZZZZZ 1

13:11 ZZZZZZ 1

13:12 ZZZZZZ 1

13:14 MA52735-CCV3 1

13:15 MA52735-CCB3 1

13:17 ZZZZZZ 1

13:18 ZZZZZZ 1

JD48247

6.1

Login Number: JD48247 Account: HAZTMDW - HazTrain, Inc.

Project: Joint Base McGuire Dix, Lakehurst,NJ Haz Waste

File ID: H9071922W1.CSV Date Analyzed: 07/19/22 Methods: SW846 7470A Analyst: LM Run ID: MA52735 Parameters: Hg

Sample Dilution PS Time Description Factor Recov Comments

13:20 ZZZZZZ 1

13:21 ZZZZZZ 1

13:23 ZZZZZZ 1

13:24 ZZZZZZ 1

13:25 ZZZZZZ 1

13:27 ZZZZZZ 1

13:28 MA52735-CCV4 1

13:30 MA52735-CCB4 1

13:32 MP34145-MB1 1

13:33 MP34145-B1 1

13:34 MP34145-S1 1

13:36 MP34145-S2 1

13:38 JD48290-3 1 (sample used for QC only; not part of login JD48247)

13:40 ZZZZZZ 1

13:41 ZZZZZZ 1

13:44 MA52735-CCV5 1

13:46 MA52735-CCB5 1

13:48 ZZZZZZ 1

13:49 ZZZZZZ 1

13:50 ZZZZZZ 1

13:52 ZZZZZZ 1

13:54 ZZZZZZ 1

13:55 ZZZZZZ 1

13:57 ZZZZZZ 1

13:58 ZZZZZZ 1

13:59 ZZZZZZ 1

14:03 MA52735-CCV6 1

14:05 MA52735-CCB6 1

14:06 MP34146-MB1 1

14:08 MP34146-B1 1

14:09 MP34146-S1 1

14:11 MP34146-S2 1

14:13 JD48265-1 1 (sample used for QC only; not part of login JD48247)

JD48247

Login Number: JD48247 Account: HAZTMDW - HazTrain, Inc.

Project: Joint Base McGuire Dix, Lakehurst,NJ Haz Waste

File ID: H9071922W1.CSV Date Analyzed: 07/19/22 Methods: SW846 7470A Analyst: LM Run ID: MA52735 Parameters: Hg

Sample Dilution PS Time Description Factor Recov Comments

14:15 MA52735-CCV7 1

14:16 MA52735-CCB7 1

14:18 ZZZZZZ 1

14:19 ZZZZZZ 1

14:21 ZZZZZZ 1

14:22 JD48247-1 1

-----------> Last reportable sample/prep for job JD48247

14:23 MA52735-CCV8 1

14:25 MA52735-CCB8 1

-----------> Last reportable CCB for job JD48247

14:27 MP34147-MB1 1

14:28 MP34147-B1 1

14:30 MP34147-S1 1

14:32 MP34147-S2 1

14:33 JD48189-2 1 (sample used for QC only; not part of login JD48247)

14:35 ZZZZZZ 1

14:37 ZZZZZZ 1

14:38 ZZZZZZ 1

14:39 MA52735-CCV9 1

14:41 MA52735-CCB9 1

14:43 ZZZZZZ 1

14:44 ZZZZZZ 1

14:45 ZZZZZZ 1

14:47 ZZZZZZ 1

14:48 ZZZZZZ 1

14:49 ZZZZZZ 1

14:51 ZZZZZZ 1

14:52 ZZZZZZ 1

14:54 MA52735-CCV10 1

14:55 MA52735-CCB10 1

14:57 ZZZZZZ 1

14:59 ZZZZZZ 1

15:00 ZZZZZZ 1

15:01 ZZZZZZ 1

15:03 ZZZZZZ 1

JD48247

Login Number: JD48247 Account: HAZTMDW - HazTrain, Inc.

Project: Joint Base McGuire Dix, Lakehurst,NJ Haz Waste

File ID: H9071922W1.CSV Date Analyzed: 07/19/22 Methods: SW846 7470A Analyst: LM Run ID: MA52735 Parameters: Hg

Sample Dilution PS Time Description Factor Recov Comments

15:04 ZZZZZZ 1

15:05 ZZZZZZ 1

15:07 ZZZZZZ 1

15:08 MA52735-CCV11 1

15:10 MA52735-CCB11 1

15:20 ZZZZZZ 10

15:22 ZZZZZZ 5

15:24 MA52735-CCV12 1

15:26 MA52735-CCB12 1

Refer to raw data for calibration curve and standards.

JD48247

REPORTED ELEMENTS SUMMARY

Login Number: JD48247 Account: HAZTMDW - HazTrain, Inc.

Project: Joint Base McGuire Dix, Lakehurst,NJ Haz Waste

File ID: H9071922W1.CSV Date Analyzed: 07/19/22 Methods: SW846 7470A Analyst: LM Run ID: MA52735 Parameters: Hg

Sample Element: H Time Description Dilution g

12:38 ZZZZZZ 1

12:39 MA52735-ICV1 1 X

12:41 MA52735-ICB1 1 X

12:43 MA52735-CCV1 1 X

12:44 MA52735-CCB1 1 X

12:46 MA52735-CRI1 1 X

12:47 MP34144-MB1 1 X

12:49 MP34144-B1 1 X

12:50 MP34144-S1 1 X

12:52 MP34144-S2 1 X

12:54 JD48207-1F 1 X (a)

12:56 ZZZZZZ 1

12:57 ZZZZZZ 1

12:59 MA52735-CCV2 1 X

13:01 MA52735-CCB2 1 X

13:02 ZZZZZZ 1

13:04 ZZZZZZ 1

13:05 ZZZZZZ 1

13:07 ZZZZZZ 1

13:08 ZZZZZZ 1

13:10 ZZZZZZ 1

13:11 ZZZZZZ 1

13:12 ZZZZZZ 1

13:14 MA52735-CCV3 1 X

13:15 MA52735-CCB3 1 X

13:17 ZZZZZZ 1

13:18 ZZZZZZ 1

13:20 ZZZZZZ 1

13:21 ZZZZZZ 1

13:23 ZZZZZZ 1

13:24 ZZZZZZ 1

13:25 ZZZZZZ 1

13:27 ZZZZZZ 1

Element: H g

JD48247

6.1.1

Account: HAZTMDW - HazTrain, Inc.

Project: Joint Base McGuire Dix, Lakehurst,NJ Haz Waste

File ID: H9071922W1.CSV Date Analyzed: 07/19/22 Methods: SW846 7470A Analyst: LM Run ID: MA52735 Parameters: Hg

Sample Element: H Time Description Dilution g

13:28 MA52735-CCV4 1 X

13:30 MA52735-CCB4 1 X

13:32 MP34145-MB1 1 X

13:33 MP34145-B1 1 X

13:34 MP34145-S1 1 X

13:36 MP34145-S2 1 X

13:38 JD48290-3 1 X (a)

13:40 ZZZZZZ 1

13:41 ZZZZZZ 1

13:44 MA52735-CCV5 1 X

13:46 MA52735-CCB5 1 X

13:48 ZZZZZZ 1

13:49 ZZZZZZ 1

13:50 ZZZZZZ 1

13:52 ZZZZZZ 1

13:54 ZZZZZZ 1

13:55 ZZZZZZ 1

13:57 ZZZZZZ 1

13:58 ZZZZZZ 1

13:59 ZZZZZZ 1

14:03 MA52735-CCV6 1 X

14:05 MA52735-CCB6 1 X

14:06 MP34146-MB1 1 X

14:08 MP34146-B1 1 X

14:09 MP34146-S1 1 X

14:11 MP34146-S2 1 X

14:13 JD48265-1 1 X (a)

14:15 MA52735-CCV7 1 X

14:16 MA52735-CCB7 1 X

14:18 ZZZZZZ 1

14:19 ZZZZZZ 1

14:21 ZZZZZZ 1

14:22 JD48247-1 1 X

Element: H g

JD48247

Account: HAZTMDW - HazTrain, Inc.

Project: Joint Base McGuire Dix, Lakehurst,NJ Haz Waste

File ID: H9071922W1.CSV Date Analyzed: 07/19/22 Methods: SW846 7470A Analyst: LM Run ID: MA52735 Parameters: Hg

Sample Element: H Time Description Dilution g

14:23 MA52735-CCV8 1 X

14:25 MA52735-CCB8 1 X

14:27 MP34147-MB1 1 X

14:28 MP34147-B1 1 X

14:30 MP34147-S1 1 X

14:32 MP34147-S2 1 X

14:33 JD48189-2 1 X (a)

14:35 ZZZZZZ 1

14:37 ZZZZZZ 1

14:38 ZZZZZZ 1

14:39 MA52735-CCV9 1 X

14:41 MA52735-CCB9 1 X

14:43 ZZZZZZ 1

14:44 ZZZZZZ 1

14:45 ZZZZZZ 1

14:47 ZZZZZZ 1

14:48 ZZZZZZ 1

14:49 ZZZZZZ 1

14:51 ZZZZZZ 1

14:52 ZZZZZZ 1

14:54 MA52735-CCV10 1 X

14:55 MA52735-CCB10 1 X

14:57 ZZZZZZ 1

14:59 ZZZZZZ 1

15:00 ZZZZZZ 1

15:01 ZZZZZZ 1

15:03 ZZZZZZ 1

15:04 ZZZZZZ 1

15:05 ZZZZZZ 1

15:07 ZZZZZZ 1

15:08 MA52735-CCV11 1 X

15:10 MA52735-CCB11 1 X

15:20 ZZZZZZ 10

Element: H g

JD48247

Account: HAZTMDW - HazTrain, Inc.

Project: Joint Base McGuire Dix, Lakehurst,NJ Haz Waste

File ID: H9071922W1.CSV Date Analyzed: 07/19/22 Methods: SW846 7470A Analyst: LM Run ID: MA52735 Parameters: Hg

Sample Element: H Time Description Dilution g

15:22 ZZZZZZ 5

15:24 MA52735-CCV12 1 X

15:26 MA52735-CCB12 1 X

(a) Sample used for QC only; not part of login JD48247.

Element: H g

JD48247

BLANK RESULTS SUMMARY

Part 1 - Initial and Continuing Calibration Blanks

Login Number: JD48247 Account: HAZTMDW - HazTrain, Inc.

Project: Joint Base McGuire Dix, Lakehurst,NJ Haz Waste

File ID: H9071922W1.CSV Date Analyzed: 07/19/22 Methods: SW846 7470A QC Limits: result < RL Run ID: MA52735 Units: ug/l

Time: 12:41 12:44 13:01 13:15 Sample ID: ICB1 CCB1 CCB2 CCB3

Metal RL IDL raw final raw final raw final raw final

Mercury 0.20 .034 0.0171 <0.20 0.00610 <0.20 0.00410 <0.20 -0.00240 <0.20

(*) Outside of QC limits (anr) Analyte not requested

JD48247

6.1.2

Login Number: JD48247 Account: HAZTMDW - HazTrain, Inc.

Project: Joint Base McGuire Dix, Lakehurst,NJ Haz Waste

File ID: H9071922W1.CSV Date Analyzed: 07/19/22 Methods: SW846 7470A QC Limits: result < RL Run ID: MA52735 Units: ug/l

Time: 13:30 13:46 14:05 14:16 Sample ID: CCB4 CCB5 CCB6 CCB7

Metal RL IDL raw final raw final raw final raw final

Mercury 0.20 .034 -0.0107 <0.20 -0.0461 <0.20 0.0291 <0.20 0.0263 <0.20

(*) Outside of QC limits (anr) Analyte not requested

JD48247

Login Number: JD48247 Account: HAZTMDW - HazTrain, Inc.

Project: Joint Base McGuire Dix, Lakehurst,NJ Haz Waste

File ID: H9071922W1.CSV Date Analyzed: 07/19/22 Methods: SW846 7470A QC Limits: result < RL Run ID: MA52735 Units: ug/l

Time: 14:25 Sample ID: CCB8

Metal RL IDL raw final

Mercury 0.20 .034 0.0286 <0.20

(*) Outside of QC limits (anr) Analyte not requested

JD48247

CALIBRATION CHECK STANDARDS SUMMARY

Initial and Continuing Calibration Checks

Login Number: JD48247 Account: HAZTMDW - HazTrain, Inc.

Project: Joint Base McGuire Dix, Lakehurst,NJ Haz Waste

File ID: H9071922W1.CSV Date Analyzed: 07/19/22 Methods: SW846 7470A QC Limits: 90 to 110 % Recovery Run ID: MA52735 Units: ug/l

Time: 12:39 12:43 12:59 Sample ID: ICV ICV1 CCV CCV1 CCV CCV2

Metal True Results % Rec True Results % Rec True Results % Rec

Mercury 3 3.21 107.0 2.5 2.50 100.0 2.5 2.36 94.4

(*) Outside of QC limits (anr) Analyte not requested

JD48247

6.1.3

Login Number: JD48247 Account: HAZTMDW - HazTrain, Inc.

Project: Joint Base McGuire Dix, Lakehurst,NJ Haz Waste

File ID: H9071922W1.CSV Date Analyzed: 07/19/22 Methods: SW846 7470A QC Limits: 90 to 110 % Recovery Run ID: MA52735 Units: ug/l

Time: 13:14 13:28 13:44 Sample ID: CCV CCV3 CCV CCV4 CCV CCV5

Metal True Results % Rec True Results % Rec True Results % Rec

Mercury 2.5 2.35 94.0 2.5 2.35 94.0 2.5 2.29 91.6

(*) Outside of QC limits (anr) Analyte not requested

JD48247

Login Number: JD48247 Account: HAZTMDW - HazTrain, Inc.

Project: Joint Base McGuire Dix, Lakehurst,NJ Haz Waste

File ID: H9071922W1.CSV Date Analyzed: 07/19/22 Methods: SW846 7470A QC Limits: 90 to 110 % Recovery Run ID: MA52735 Units: ug/l

Time: 14:03 14:15 14:23 Sample ID: CCV CCV6 CCV CCV7 CCV CCV8

Metal True Results % Rec True Results % Rec True Results % Rec

Mercury 2.5 2.52 100.8 2.5 2.55 102.0 2.5 2.29 91.6

(*) Outside of QC limits (anr) Analyte not requested

JD48247

LOW CALIBRATION CHECK STANDARDS SUMMARY

Account: HAZTMDW - HazTrain, Inc.

Project: Joint Base McGuire Dix, Lakehurst,NJ Haz Waste

File ID: H9071922W1.CSV Date Analyzed: 07/19/22 Methods: SW846 7470A QC Limits: 70 to 130 % Recovery Run ID: MA52735 Units: ug/l

Time: 12:46 Sample ID: CRI CRIA CRI1

Metal True True Results % Rec

Mercury 0.20 0.208 104.0

(*) Outside of QC limits (anr) Analyte not requested

JD48247

6.1.4

Login Number: JD48247 Account: HAZTMDW - HazTrain, Inc.

Project: Joint Base McGuire Dix, Lakehurst,NJ Haz Waste

File ID: SF072222M1.ICP Date Analyzed: 07/22/22 Methods: EPA 200.7, SW846 6010D Analyst: ND Run ID: MA52760 Parameters: As,Ba,Cd,Cr,Pb,Se,Ag

Sample Dilution PS Time Description Factor Recov Comments

06:21 MA52760-STD1 1 STDA

06:26 MA52760-STD2 1 STDB

06:31 MA52760-ICV1 1

06:39 MA52760-ICB1 1

06:46 MA52760-ICCV1 1

06:55 MA52760-CCB1 1

07:00 MA52760-CRI1 1

07:05 MA52760-CRID1 1

07:10 MA52760-ICSA1 1

07:15 MA52760-ICSAB1 1

07:20 MA52760-HSTD1 1

07:25 MA52760-HSTD2 1

07:30 ZZZZZZ 1

07:35 ZZZZZZ 1

07:40 ZZZZZZ 1

07:46 MA52760-CCV1 1

07:50 MA52760-CCB2 1

07:56 ZZZZZZ 1

08:01 MP34180-B1 1

08:06 MP34180-S1 1

08:11 MP34180-S2 1

08:15 JD48560-1 1 (sample used for QC only; not part of login JD48247)

08:20 MP34180-SD1 5

08:26 ZZZZZZ 1

08:31 ZZZZZZ 1

08:36 ZZZZZZ 1

08:41 MA52760-CCV2 1

08:46 MA52760-CCB3 1

08:51 MP34180-MB1 1

08:56 MP34179-MB1 1

09:01 ZZZZZZ 1

09:07 ZZZZZZ 1

09:12 ZZZZZZ 1

JD48247

6.2

Login Number: JD48247 Account: HAZTMDW - HazTrain, Inc.

Project: Joint Base McGuire Dix, Lakehurst,NJ Haz Waste

File ID: SF072222M1.ICP Date Analyzed: 07/22/22 Methods: EPA 200.7, SW846 6010D Analyst: ND Run ID: MA52760 Parameters: As,Ba,Cd,Cr,Pb,Se,Ag

Sample Dilution PS Time Description Factor Recov Comments

09:17 ZZZZZZ 1

09:22 ZZZZZZ 1

09:27 ZZZZZZ 1

09:32 ZZZZZZ 1

09:37 MA52760-CCV3 1

09:42 MA52760-CCB4 1

09:47 ZZZZZZ 1

09:52 ZZZZZZ 1

09:57 ZZZZZZ 1

10:02 ZZZZZZ 1

10:08 ZZZZZZ 1

10:13 ZZZZZZ 1

10:18 ZZZZZZ 1

10:23 MP34179-B1 1

10:28 MP34179-S1 1

10:32 MA52760-CCV4 1

10:37 MA52760-CCB5 1

10:43 MP34179-S2 1

10:47 JD48319-3 1 (sample used for QC only; not part of login JD48247)

10:52 MP34179-SD1 5

10:58 ZZZZZZ 1

11:03 ZZZZZZ 1

11:08 MP34051-MB2 1

11:13 MP34051-B2 1

11:18 MP34051-S1 1

11:23 MP34051-S2 1

11:27 MA52760-CCV5 1

11:32 MA52760-CCB6 1

11:38 ZZZZZZ 1

11:43 JD48063-10 1 (sample used for QC only; not part of login JD48247)

11:48 MP34051-SD1 5

11:53 ZZZZZZ 1

11:58 ZZZZZZ 1

JD48247

Login Number: JD48247 Account: HAZTMDW - HazTrain, Inc.

Project: Joint Base McGuire Dix, Lakehurst,NJ Haz Waste

File ID: SF072222M1.ICP Date Analyzed: 07/22/22 Methods: EPA 200.7, SW846 6010D Analyst: ND Run ID: MA52760 Parameters: As,Ba,Cd,Cr,Pb,Se,Ag

Sample Dilution PS Time Description Factor Recov Comments

12:03 ZZZZZZ 1

12:08 ZZZZZZ 1

12:13 ZZZZZZ 1

12:18 ZZZZZZ 1

12:23 ZZZZZZ 1

12:28 MA52760-CCV6 1

12:33 MA52760-CCB7 1

12:38 ZZZZZZ 1

12:43 ZZZZZZ 1

12:48 ZZZZZZ 1

12:53 ZZZZZZ 1

12:58 ZZZZZZ 1

13:03 ZZZZZZ 1

13:08 ZZZZZZ 1

13:13 ZZZZZZ 1

13:18 ZZZZZZ 1

13:23 MA52760-CCV7 1

13:28 MA52760-CCB8 1

13:33 ZZZZZZ 1

13:38 ZZZZZZ 1

13:43 ZZZZZZ 1

13:48 ZZZZZZ 2

13:53 ZZZZZZ 2

13:58 ZZZZZZ 2

14:03 ZZZZZZ 2

14:08 ZZZZZZ 2

14:13 ZZZZZZ 2

14:18 ZZZZZZ 2

14:23 MA52760-CCV8 1

14:28 MA52760-CCB9 1

14:33 ZZZZZZ 2

14:38 ZZZZZZ 2

14:43 ZZZZZZ 2

JD48247

Login Number: JD48247 Account: HAZTMDW - HazTrain, Inc.

Project: Joint Base McGuire Dix, Lakehurst,NJ Haz Waste

File ID: SF072222M1.ICP Date Analyzed: 07/22/22 Methods: EPA 200.7, SW846 6010D Analyst: ND Run ID: MA52760 Parameters: As,Ba,Cd,Cr,Pb,Se,Ag

Sample Dilution PS Time Description Factor Recov Comments

14:48 ZZZZZZ 2

14:53 ZZZZZZ 2

14:58 ZZZZZZ 2

15:03 ZZZZZZ 2

15:08 MP34149-MB2 1

15:13 MP34149-LB2 1

15:19 MP34149-B2 1

15:24 MA52760-CCV9 1

15:28 MA52760-CCB10 1

15:34 MP34149-LS2 1

15:39 MP34149-S1 1

15:44 MP34149-S2 1

15:49 JD48265-1 1 (sample used for QC only; not part of login JD48247)

15:54 MP34149-SD1 5

15:59 JD48247-1 1

-----------> Last reportable sample/prep for job JD48247

16:04 ZZZZZZ 1

16:10 ZZZZZZ 5

16:15 ZZZZZZ 1

16:20 ZZZZZZ 1

16:25 MA52760-CCV10 1

16:30 MA52760-CCB11 1

-----------> Last reportable CCB for job JD48247

16:35 ZZZZZZ 1

16:41 ZZZZZZ 1

16:46 ZZZZZZ 1

16:51 MP33868-S2 10

16:56 MA52760-CCV11 1

17:01 MA52760-CCB12 1

Refer to raw data for calibration curve and standards.

JD48247

Account: HAZTMDW - HazTrain, Inc.

Project: Joint Base McGuire Dix, Lakehurst,NJ Haz Waste

File ID: SF072222M1.ICP Date Analyzed: 07/22/22 Methods: EPA 200.7, SW846 6010D Analyst: ND Run ID: MA52760 Parameters: As,Ba,Cd,Cr,Pb,Se,Ag

Sample Element: A B C C P S A Time Description Dilution s a d r b e g

06:31 MA52760-ICV1 1 X X X X X X X

06:39 MA52760-ICB1 1 X X X X X X X

06:46 MA52760-ICCV1 1 X X X X X X X

06:55 MA52760-CCB1 1 X X X X X X X

07:00 MA52760-CRI1 1 X X X X X X X

07:05 MA52760-CRID1 1 X X X X X X X

07:10 MA52760-ICSA1 1 X X X X X X X

07:15 MA52760-ICSAB1 1 X X X X X X X

07:20 MA52760-HSTD1 1 X X X X X X X

07:25 MA52760-HSTD2 1 X X X X X X X

07:30 ZZZZZZ 1

07:35 ZZZZZZ 1

07:40 ZZZZZZ 1

07:46 MA52760-CCV1 1 X X X X X X X

07:50 MA52760-CCB2 1 X X X X X X X

07:56 ZZZZZZ 1

08:01 MP34180-B1 1 X X X X X X X

08:06 MP34180-S1 1 X X X X X X X

08:11 MP34180-S2 1 X X X X X X X

08:15 JD48560-1 1 X X X X X X X (a)

08:20 MP34180-SD1 5 X X X X X X X

08:26 ZZZZZZ 1

08:31 ZZZZZZ 1

08:36 ZZZZZZ 1

08:41 MA52760-CCV2 1 X X X X X X X

08:46 MA52760-CCB3 1 X X X X X X X

08:51 MP34180-MB1 1 X X X X X X X

08:56 MP34179-MB1 1 X X X X X X X

09:01 ZZZZZZ 1

09:07 ZZZZZZ 1

09:12 ZZZZZZ 1

09:17 ZZZZZZ 1

09:22 ZZZZZZ 1

Element: A B C C P S A s a d r b e g

JD48247

6.2.1

Account: HAZTMDW - HazTrain, Inc.

Project: Joint Base McGuire Dix, Lakehurst,NJ Haz Waste

File ID: SF072222M1.ICP Date Analyzed: 07/22/22 Methods: EPA 200.7, SW846 6010D Analyst: ND Run ID: MA52760 Parameters: As,Ba,Cd,Cr,Pb,Se,Ag

Sample Element: A B C C P S A Time Description Dilution s a d r b e g

09:27 ZZZZZZ 1

09:32 ZZZZZZ 1

09:37 MA52760-CCV3 1 X X X X X X X

09:42 MA52760-CCB4 1 X X X X X X X

09:47 ZZZZZZ 1

09:52 ZZZZZZ 1

09:57 ZZZZZZ 1

10:02 ZZZZZZ 1

10:08 ZZZZZZ 1

10:13 ZZZZZZ 1

10:18 ZZZZZZ 1

10:23 MP34179-B1 1 X X X X X X X

10:28 MP34179-S1 1 X X X X X X X

10:32 MA52760-CCV4 1 X X X X X X X

10:37 MA52760-CCB5 1 X X X X X X X

10:43 MP34179-S2 1 X X X X X X X

10:47 JD48319-3 1 (a)

10:52 MP34179-SD1 5 X X X X X X X

10:58 ZZZZZZ 1

11:03 ZZZZZZ 1

11:08 MP34051-MB2 1 X X X X

11:13 MP34051-B2 1 X X X X

11:18 MP34051-S1 1 X X X X

11:23 MP34051-S2 1 X X X X

11:27 MA52760-CCV5 1 X X X X X X X

11:32 MA52760-CCB6 1 X X X X X X X

11:38 ZZZZZZ 1

11:43 JD48063-10 1 X X X X (a)

11:48 MP34051-SD1 5 X X X X

11:53 ZZZZZZ 1

11:58 ZZZZZZ 1

12:03 ZZZZZZ 1

12:08 ZZZZZZ 1

Element: A B C C P S A s a d r b e g

JD48247

Account: HAZTMDW - HazTrain, Inc.

Project: Joint Base McGuire Dix, Lakehurst,NJ Haz Waste

File ID: SF072222M1.ICP Date Analyzed: 07/22/22 Methods: EPA 200.7, SW846 6010D Analyst: ND Run ID: MA52760 Parameters: As,Ba,Cd,Cr,Pb,Se,Ag

Sample Element: A B C C P S A Time Description Dilution s a d r b e g

12:13 ZZZZZZ 1

12:18 ZZZZZZ 1

12:23 ZZZZZZ 1

12:28 MA52760-CCV6 1 X X X X X X X

12:33 MA52760-CCB7 1 X X X X X X X

12:38 ZZZZZZ 1

12:43 ZZZZZZ 1

12:48 ZZZZZZ 1

12:53 ZZZZZZ 1

12:58 ZZZZZZ 1

13:03 ZZZZZZ 1

13:08 ZZZZZZ 1

13:13 ZZZZZZ 1

13:18 ZZZZZZ 1

13:23 MA52760-CCV7 1 X X X X X X X

13:28 MA52760-CCB8 1 X X X X X X X

13:33 ZZZZZZ 1

13:38 ZZZZZZ 1

13:43 ZZZZZZ 1

13:48 ZZZZZZ 2

13:53 ZZZZZZ 2

13:58 ZZZZZZ 2

14:03 ZZZZZZ 2

14:08 ZZZZZZ 2

14:13 ZZZZZZ 2

14:18 ZZZZZZ 2

14:23 MA52760-CCV8 1 X X X X X X X

14:28 MA52760-CCB9 1 X X X X X X X

14:33 ZZZZZZ 2

14:38 ZZZZZZ 2

14:43 ZZZZZZ 2

14:48 ZZZZZZ 2

14:53 ZZZZZZ 2

Element: A B C C P S A s a d r b e g

JD48247

Account: HAZTMDW - HazTrain, Inc.

Project: Joint Base McGuire Dix, Lakehurst,NJ Haz Waste

File ID: SF072222M1.ICP Date Analyzed: 07/22/22 Methods: EPA 200.7, SW846 6010D Analyst: ND Run ID: MA52760 Parameters: As,Ba,Cd,Cr,Pb,Se,Ag

Sample Element: A B C C P S A Time Description Dilution s a d r b e g

14:58 ZZZZZZ 2

15:03 ZZZZZZ 2

15:08 MP34149-MB2 1 X X X X X X X

15:13 MP34149-LB2 1

15:19 MP34149-B2 1 X X X X X X X

15:24 MA52760-CCV9 1 X X X X X X X

15:28 MA52760-CCB10 1 X X X X X X X

15:34 MP34149-LS2 1 X X X X X X X

15:39 MP34149-S1 1 X X X X X X X

15:44 MP34149-S2 1 X X X X X X X

15:49 JD48265-1 1 X X X X X X X (a)

15:54 MP34149-SD1 5 X X X X X X X

15:59 JD48247-1 1 X X X X X X X

16:04 ZZZZZZ 1

16:10 ZZZZZZ 5

16:15 ZZZZZZ 1

16:20 ZZZZZZ 1

16:25 MA52760-CCV10 1 X X X X X X X

16:30 MA52760-CCB11 1 X X X X X X X

16:35 ZZZZZZ 1

16:41 ZZZZZZ 1

16:46 ZZZZZZ 1

16:51 MP33868-S2 10 X

16:56 MA52760-CCV11 1 X X X X X X X

17:01 MA52760-CCB12 1 X X X X X X X

(a) Sample used for QC only; not part of login JD48247.

Element: A B C C P S A s a d r b e g

JD48247

INTERNAL STANDARD SUMMARY

Account: HAZTMDW - HazTrain, Inc.

Project: Joint Base McGuire Dix, Lakehurst,NJ Haz Waste

File ID: SF072222M1.ICP Date Analyzed: 07/22/22 Methods: EPA 200.7, SW846 6010D Analyst: ND Run ID: MA52760 Parameters: As,Ba,Cd,Cr,Pb,Se,Ag

Sample Time Description Istd#1 Istd#2 Istd#3 Istd#4

06:21 MA52760-STD1 2292 R 73188 R 4510 R 5854 R

06:26 MA52760-STD2 2183 70252 4501 5706

06:31 MA52760-ICV1 2238 71258 4541 5761

06:39 MA52760-ICB1 2262 72310 4515 5796

06:46 MA52760-ICCV1 2208 70659 4504 5677

06:55 MA52760-CCB1 2277 73117 4509 5823

07:00 MA52760-CRI1 2253 72057 4449 5755

07:05 MA52760-CRID1 2265 72415 4477 5795

07:10 MA52760-ICSA1 2111 68162 4451 5504

07:15 MA52760-ICSAB1 2109 67991 4439 5546

07:20 MA52760-HSTD1 2240 72787 4512 5957

07:25 MA52760-HSTD2 2134 69315 4443 5513

07:30 ZZZZZZ 2251 72613 4559 5974

07:35 ZZZZZZ 2200 71989 4545 5720

07:40 ZZZZZZ 2273 73198 4542 5802

07:46 MA52760-CCV1 2224 71455 4494 5693

07:50 MA52760-CCB2 2266 73040 4511 5764

07:56 ZZZZZZ 2281 73470 4636 5812

08:01 MP34180-B1 2252 72662 4633 5757

08:06 MP34180-S1 2240 72411 4628 5701

08:11 MP34180-S2 2240 72048 4643 5709

08:15 JD48560-1 2247 72726 4627 5686

08:20 MP34180-SD1 2271 72945 4582 5781

08:26 ZZZZZZ 2265 73779 4606 5723

08:31 ZZZZZZ 2262 73685 4569 5749

08:36 ZZZZZZ 2278 73149 4606 5794

08:41 MA52760-CCV2 2220 71179 4552 5705

08:46 MA52760-CCB3 2253 72476 4542 5749

08:51 MP34180-MB1 2211 71745 4530 5657

08:56 MP34179-MB1 2285 73489 4637 5823

09:01 ZZZZZZ 2257 73324 4626 5725

09:07 ZZZZZZ 2276 73926 4591 5794

09:12 ZZZZZZ 2256 72466 4657 5758

JD48247

6.2.2

Account: HAZTMDW - HazTrain, Inc.

Project: Joint Base McGuire Dix, Lakehurst,NJ Haz Waste

File ID: SF072222M1.ICP Date Analyzed: 07/22/22 Methods: EPA 200.7, SW846 6010D Analyst: ND Run ID: MA52760 Parameters: As,Ba,Cd,Cr,Pb,Se,Ag

Sample Time Description Istd#1 Istd#2 Istd#3 Istd#4

09:17 ZZZZZZ 2271 73122 4569 5812

09:22 ZZZZZZ 2268 73788 4576 5788

09:27 ZZZZZZ 2284 74130 4507 5805

09:32 ZZZZZZ 2249 73076 4567 5706

09:37 MA52760-CCV3 2233 71970 4542 5720

09:42 MA52760-CCB4 2274 73315 4536 5804

09:47 ZZZZZZ 2261 73242 4615 5794

09:52 ZZZZZZ 2282 73941 4606 5815

09:57 ZZZZZZ 2277 74127 4585 5813

10:02 ZZZZZZ 2240 72494 4603 5710

10:08 ZZZZZZ 2270 73752 4592 5772

10:13 ZZZZZZ 2275 73501 4614 5775

10:18 ZZZZZZ 2279 74079 4611 5846

10:23 MP34179-B1 2257 72788 4598 5777

10:28 MP34179-S1 2202 71507 4568 5602

10:32 MA52760-CCV4 2226 71758 4507 5696

10:37 MA52760-CCB5 2245 71762 4549 5721

10:43 MP34179-S2 2183 70159 4541 5554

10:47 JD48319-3 2205 72258 4559 5597

10:52 MP34179-SD1 2228 71559 4533 5684

10:58 ZZZZZZ 2219 72880 4535 5625

11:03 ZZZZZZ 2267 72952 4591 5761

11:08 MP34051-MB2 2275 73398 4622 5781

11:13 MP34051-B2 2245 72795 4582 5731

11:18 MP34051-S1 2275 72564 4645 5739

11:23 MP34051-S2 2257 72416 4663 5718

11:27 MA52760-CCV5 2232 72140 4498 5708

11:32 MA52760-CCB6 2251 71990 4512 5733

11:38 ZZZZZZ 2254 71207 4465 5749

11:43 JD48063-10 2296 73411 4670 5742

11:48 MP34051-SD1 2289 73194 4549 5792

11:53 ZZZZZZ 2344 74778 4848 5733

11:58 ZZZZZZ 2338 74180 4820 5725

JD48247

Account: HAZTMDW - HazTrain, Inc.

Project: Joint Base McGuire Dix, Lakehurst,NJ Haz Waste

File ID: SF072222M1.ICP Date Analyzed: 07/22/22 Methods: EPA 200.7, SW846 6010D Analyst: ND Run ID: MA52760 Parameters: As,Ba,Cd,Cr,Pb,Se,Ag

Sample Time Description Istd#1 Istd#2 Istd#3 Istd#4

12:03 ZZZZZZ 2347 74989 4812 5797

12:08 ZZZZZZ 2363 75580 4793 5804

12:13 ZZZZZZ 2348 75569 4846 5759

12:18 ZZZZZZ 2348 74918 4850 5738

12:23 ZZZZZZ 2317 73263 4832 5720

12:28 MA52760-CCV6 2232 71266 4527 5687

12:33 MA52760-CCB7 2277 72067 4518 5777

12:38 ZZZZZZ 2342 75646 4830 5691

12:43 ZZZZZZ 2301 73098 4777 5682

12:48 ZZZZZZ 2267 72523 4683 5645

12:53 ZZZZZZ 2360 75536 4834 5751

12:58 ZZZZZZ 2306 73336 4798 5688

13:03 ZZZZZZ 2264 72684 4661 5636

13:08 ZZZZZZ 2351 75417 4800 5735

13:13 ZZZZZZ 2318 74429 4766 5731

13:18 ZZZZZZ 2343 75137 4799 5736

13:23 MA52760-CCV7 2222 70537 4442 5665

13:28 MA52760-CCB8 2262 71628 4563 5718

13:33 ZZZZZZ 2352 74604 4857 5737

13:38 ZZZZZZ 2338 74212 4821 5749

13:43 ZZZZZZ 2304 73354 4722 5719

13:48 ZZZZZZ 2346 74997 4703 5797

13:53 ZZZZZZ 2271 73077 4674 5641

13:58 ZZZZZZ 2291 72817 4663 5711

14:03 ZZZZZZ 2293 71644 4679 5690

14:08 ZZZZZZ 2325 74419 4701 5730

14:13 ZZZZZZ 2324 73948 4731 5738

14:18 ZZZZZZ 2310 73571 4687 5731

14:23 MA52760-CCV8 2238 71893 4526 5678

14:28 MA52760-CCB9 2249 70323 4522 5687

14:33 ZZZZZZ 2312 73244 4723 5708

14:38 ZZZZZZ 2333 74472 4735 5758

14:43 ZZZZZZ 2278 71997 4644 5672

JD48247

Account: HAZTMDW - HazTrain, Inc.

Project: Joint Base McGuire Dix, Lakehurst,NJ Haz Waste

File ID: SF072222M1.ICP Date Analyzed: 07/22/22 Methods: EPA 200.7, SW846 6010D Analyst: ND Run ID: MA52760 Parameters: As,Ba,Cd,Cr,Pb,Se,Ag

Sample Time Description Istd#1 Istd#2 Istd#3 Istd#4

14:48 ZZZZZZ 2288 72643 4680 5666

14:53 ZZZZZZ 2324 74094 4679 5778

14:58 ZZZZZZ 2287 73010 4707 5676

15:03 ZZZZZZ 2314 73577 4700 5713

15:08 MP34149-MB2 2309 73894 4583 5817

15:13 MP34149-LB2 2121 68852 4519 5184

15:19 MP34149-B2 2262 71053 4585 5734

15:24 MA52760-CCV9 2230 71173 4507 5657

15:28 MA52760-CCB10 2272 72446 4514 5736

15:34 MP34149-LS2 2121 68470 4480 5158

15:39 MP34149-S1 2151 67869 4535 5298

15:44 MP34149-S2 2138 68760 4525 5262

15:49 JD48265-1 2158 69430 4475 5244

15:54 MP34149-SD1 2223 70862 4496 5524

15:59 JD48247-1 2146 69948 4555 5601

16:04 ZZZZZZ 2062 67924 4434 5047

16:10 ZZZZZZ 2219 70290 4498 5513

16:15 ZZZZZZ 2145 68642 4521 5183

16:20 ZZZZZZ 2144 69565 4522 5213

16:25 MA52760-CCV10 2248 72270 4496 5701

16:30 MA52760-CCB11 2274 72521 4472 5738

16:35 ZZZZZZ 2144 69509 4496 5230

16:41 ZZZZZZ 2145 69665 4495 5233

16:46 ZZZZZZ 2123 68686 4494 5192

16:51 MP33868-S2 2199 71612 4481 5491

16:56 MA52760-CCV11 2234 70810 4492 5674

17:01 MA52760-CCB12 2267 71780 4506 5716

R = Reference for ISTD limits. ! = Outside limits.

LEGEND:

Istd# Parameter Limits _______ ________________________ __________ Istd#1 Yttrium (2243) 70-130 % Istd#2 Yttrium (3600) 70-130 % Istd#3 Yttrium (3710) 70-130 % Istd#4 Indium 70-130 %

JD48247

Login Number: JD48247 Account: HAZTMDW - HazTrain, Inc.

Project: Joint Base McGuire Dix, Lakehurst,NJ Haz Waste

File ID: SF072222M1.ICP Date Analyzed: 07/22/22 Methods: EPA 200.7, SW846 6010D QC Limits: result < RL Run ID: MA52760 Units: ug/l

Time: 06:39 06:55 07:50 08:46 Sample ID: ICB1 CCB1 CCB2 CCB3

Metal RL IDL raw final raw final raw final raw final

Aluminum 200 9.2 anr

Antimony 6.0 2.8 anr

Arsenic 3.0 2.6 -0.900 <3.0 -1.20 <3.0 0.500 <3.0 0.200 <3.0

Barium 200 .2 -0.300 <200 -0.300 <200 0.00 <200 -0.200 <200

Beryllium 1.0 .2 anr

Bismuth 20 2.5

Boron 100 1.8

Cadmium 3.0 .4 0.200 <3.0 0.200 <3.0 0.200 <3.0 0.100 <3.0

Calcium 5000 13 anr

Cerium 100

Chromium 10 .7 -0.200 <10 -0.300 <10 -0.100 <10 0.200 <10

Cobalt 50 .6 anr

Copper 10 .7 anr

Iron 100 3.3 anr

Lead 3.0 2 -0.800 <3.0 0.900 <3.0 0.900 <3.0 -0.500 <3.0

Lithium 50 1.5

Magnesium 5000 25 anr

Manganese 15 .1 anr

Molybdenum 20 .6

Nickel 10 .8 anr

Phosphorus 50 7

Potassium 10000 35 anr

Selenium 10 3.6 0.500 <10 -0.500 <10 1.00 <10 0.800 <10

Silicon 200 2.2

Silver 10 .6 0.600 <10 0.700 <10 0.500 <10 0.500 <10

Sodium 10000 14 anr

Strontium 10 .1

Sulfur 50 3.7

Thallium 10 5.2 anr

Tin 10 1.4

Titanium 10 .8

Tungsten 50 1.3

Vanadium 50 .5 anr

JD48247

6.2.3

Login Number: JD48247 Account: HAZTMDW - HazTrain, Inc.

Project: Joint Base McGuire Dix, Lakehurst,NJ Haz Waste

File ID: SF072222M1.ICP Date Analyzed: 07/22/22 Methods: EPA 200.7, SW846 6010D QC Limits: result < RL Run ID: MA52760 Units: ug/l

Time: 06:39 06:55 07:50 08:46 Sample ID: ICB1 CCB1 CCB2 CCB3

Metal RL IDL raw final raw final raw final raw final

Zinc 20 .3 anr

Zirconium 10 .5

(*) Outside of QC limits (anr) Analyte not requested

JD48247

Login Number: JD48247 Account: HAZTMDW - HazTrain, Inc.

Project: Joint Base McGuire Dix, Lakehurst,NJ Haz Waste

File ID: SF072222M1.ICP Date Analyzed: 07/22/22 Methods: EPA 200.7, SW846 6010D QC Limits: result < RL Run ID: MA52760 Units: ug/l

Time: 09:42 10:37 11:32 12:33 Sample ID: CCB4 CCB5 CCB6 CCB7

Metal RL IDL raw final raw final raw final raw final

Aluminum 200 9.2 anr

Antimony 6.0 2.8 anr

Arsenic 3.0 2.6 0.600 <3.0 0.100 <3.0 -0.300 <3.0 -0.400 <3.0

Barium 200 .2 -0.100 <200 0.00 <200 0.00 <200 -0.400 <200

Beryllium 1.0 .2 anr

Bismuth 20 2.5

Boron 100 1.8

Cadmium 3.0 .4 0.00 <3.0 0.00 <3.0 0.100 <3.0 0.200 <3.0

Calcium 5000 13 anr

Cerium 100

Chromium 10 .7 -0.200 <10 0.00 <10 0.100 <10 -0.100 <10

Cobalt 50 .6 anr

Copper 10 .7 anr

Iron 100 3.3 anr

Lead 3.0 2 -0.800 <3.0 0.300 <3.0 -0.900 <3.0 0.300 <3.0

Lithium 50 1.5

Magnesium 5000 25 anr

Manganese 15 .1 anr

Molybdenum 20 .6

Nickel 10 .8 anr

Phosphorus 50 7

Potassium 10000 35 anr

Selenium 10 3.6 0.800 <10 0.300 <10 2.30 <10 1.00 <10

Silicon 200 2.2

Silver 10 .6 0.200 <10 0.100 <10 0.400 <10 0.500 <10

Sodium 10000 14 anr

Strontium 10 .1

Sulfur 50 3.7

Thallium 10 5.2 anr

Tin 10 1.4

Titanium 10 .8

Tungsten 50 1.3

Vanadium 50 .5 anr

JD48247

Login Number: JD48247 Account: HAZTMDW - HazTrain, Inc.

Project: Joint Base McGuire Dix, Lakehurst,NJ Haz Waste

File ID: SF072222M1.ICP Date Analyzed: 07/22/22 Methods: EPA 200.7, SW846 6010D QC Limits: result < RL Run ID: MA52760 Units: ug/l

Time: 09:42 10:37 11:32 12:33 Sample ID: CCB4 CCB5 CCB6 CCB7

Metal RL IDL raw final raw final raw final raw final

Zinc 20 .3 anr

Zirconium 10 .5

(*) Outside of QC limits (anr) Analyte not requested

JD48247

Login Number: JD48247 Account: HAZTMDW - HazTrain, Inc.

Project: Joint Base McGuire Dix, Lakehurst,NJ Haz Waste

File ID: SF072222M1.ICP Date Analyzed: 07/22/22 Methods: EPA 200.7, SW846 6010D QC Limits: result < RL Run ID: MA52760 Units: ug/l

Time: 13:28 14:28 15:28 16:30 Sample ID: CCB8 CCB9 CCB10 CCB11

Metal RL IDL raw final raw final raw final raw final

Aluminum 200 9.2 anr

Antimony 6.0 2.8 anr

Arsenic 3.0 2.6 -0.600 <3.0 1.20 <3.0 0.100 <3.0 0.500 <3.0

Barium 200 .2 -0.400 <200 -0.300 <200 0.100 <200 -0.300 <200

Beryllium 1.0 .2 anr

Bismuth 20 2.5

Boron 100 1.8

Cadmium 3.0 .4 0.200 <3.0 -0.100 <3.0 0.00 <3.0 0.100 <3.0

Calcium 5000 13 anr

Cerium 100

Chromium 10 .7 -0.100 <10 -0.100 <10 -0.100 <10 0.00 <10

Cobalt 50 .6 anr

Copper 10 .7 anr

Iron 100 3.3 anr

Lead 3.0 2 -0.700 <3.0 0.00 <3.0 0.00 <3.0 -0.100 <3.0

Lithium 50 1.5

Magnesium 5000 25 anr

Manganese 15 .1 anr

Molybdenum 20 .6

Nickel 10 .8 anr

Phosphorus 50 7

Potassium 10000 35 anr

Selenium 10 3.6 -0.100 <10 -1.00 <10 2.70 <10 -0.300 <10

Silicon 200 2.2

Silver 10 .6 0.500 <10 0.200 <10 0.600 <10 0.300 <10

Sodium 10000 14 anr

Strontium 10 .1

Sulfur 50 3.7

Thallium 10 5.2 anr

Tin 10 1.4

Titanium 10 .8

Tungsten 50 1.3

Vanadium 50 .5 anr

JD48247

Login Number: JD48247 Account: HAZTMDW - HazTrain, Inc.

Project: Joint Base McGuire Dix, Lakehurst,NJ Haz Waste

File ID: SF072222M1.ICP Date Analyzed: 07/22/22 Methods: EPA 200.7, SW846 6010D QC Limits: result < RL Run ID: MA52760 Units: ug/l

Time: 13:28 14:28 15:28 16:30 Sample ID: CCB8 CCB9 CCB10 CCB11

Metal RL IDL raw final raw final raw final raw final

Zinc 20 .3 anr

Zirconium 10 .5

(*) Outside of QC limits (anr) Analyte not requested

JD48247

Initial Continuing Calibration Check

Login Number: JD48247 Account: HAZTMDW - HazTrain, Inc.

Project: Joint Base McGuire Dix, Lakehurst,NJ Haz Waste

File ID: SF072222M1.ICP Date Analyzed: 07/22/22 Methods: EPA 200.7, SW846 6010D QC Limits: to % Recovery Run ID: MA52760 Units: ug/l

Time: 06:46 Sample ID: ICCV ICCV1

Metal True Results % Rec

Aluminum anr

Antimony anr

Arsenic 2000 2010 100.5

Barium 2000 1990 99.5

Beryllium anr

Bismuth

Boron

Cadmium 2000 1990 99.5

Calcium anr

Cerium

Chromium 2000 2010 100.5

Cobalt anr

Copper anr

Iron anr

Lead 2000 2060 103.0

Lithium

Magnesium anr

Manganese anr

Molybdenum

Nickel anr

Phosphorus

Potassium anr

Selenium 2000 2000 100.0

Silicon

Silver 250 246 98.4

Sodium anr

Strontium

Sulfur

Thallium anr

Tin

Titanium

Tungsten

Vanadium anr

JD48247

6.2.4

Initial Continuing Calibration Check

Login Number: JD48247 Account: HAZTMDW - HazTrain, Inc.

Project: Joint Base McGuire Dix, Lakehurst,NJ Haz Waste

File ID: SF072222M1.ICP Date Analyzed: 07/22/22 Methods: EPA 200.7, SW846 6010D QC Limits: to % Recovery Run ID: MA52760 Units: ug/l

Time: 06:46 Sample ID: ICCV ICCV1

Metal True Results % Rec

Zinc anr

Zirconium

(*) Outside of QC limits (anr) Analyte not requested

JD48247

6.2.4

Login Number: JD48247 Account: HAZTMDW - HazTrain, Inc.

Project: Joint Base McGuire Dix, Lakehurst,NJ Haz Waste

File ID: SF072222M1.ICP Date Analyzed: 07/22/22 Methods: EPA 200.7, SW846 6010D QC Limits: 95 to 105 % Recovery Run ID: MA52760 Units: ug/l

Time: 06:31 07:46 08:41 Sample ID: ICV ICV1 CCV CCV1 CCV CCV2

Metal True Results % Rec True Results % Rec True Results % Rec

Aluminum anr

Antimony anr

Arsenic 2000 1980 99.0 2000 1980 99.0 2000 1980 99.0

Barium 2000 1960 98.0 2000 2020 101.0 2000 2010 100.5

Beryllium anr

Bismuth

Boron

Cadmium 2000 1950 97.5 2000 1980 99.0 2000 1980 99.0

Calcium anr

Cerium

Chromium 2000 1970 98.5 2000 2000 100.0 2000 2000 100.0

Cobalt anr

Copper anr

Iron anr

Lead 2000 2010 100.5 2000 2050 102.5 2000 2040 102.0

Lithium

Magnesium anr

Manganese anr

Molybdenum

Nickel anr

Phosphorus

Potassium anr

Selenium 2000 1940 97.0 2000 1970 98.5 2000 1970 98.5

Silicon

Silver 250 246 98.4 250 245 98.0 250 246 98.4

Sodium anr

Strontium

Sulfur

Thallium anr

Tin

Titanium

Tungsten

Vanadium anr

JD48247

6.2.5

Login Number: JD48247 Account: HAZTMDW - HazTrain, Inc.

Project: Joint Base McGuire Dix, Lakehurst,NJ Haz Waste

File ID: SF072222M1.ICP Date Analyzed: 07/22/22 Methods: EPA 200.7, SW846 6010D QC Limits: 95 to 105 % Recovery Run ID: MA52760 Units: ug/l

Time: 06:31 07:46 08:41 Sample ID: ICV ICV1 CCV CCV1 CCV CCV2

Metal True Results % Rec True Results % Rec True Results % Rec

Zinc anr

Zirconium

(*) Outside of QC limits (anr) Analyte not requested

JD48247

Login Number: JD48247 Account: HAZTMDW - HazTrain, Inc.

Project: Joint Base McGuire Dix, Lakehurst,NJ Haz Waste

File ID: SF072222M1.ICP Date Analyzed: 07/22/22 Methods: EPA 200.7, SW846 6010D QC Limits: 95 to 105 % Recovery Run ID: MA52760 Units: ug/l

Time: 09:37 10:32 11:27 Sample ID: CCV CCV3 CCV CCV4 CCV CCV5

Metal True Results % Rec True Results % Rec True Results % Rec

Aluminum anr

Antimony anr

Arsenic 2000 1980 99.0 2000 1980 99.0 2000 1980 99.0

Barium 2000 2000 100.0 2000 1990 99.5 2000 1990 99.5

Beryllium anr

Bismuth

Boron

Cadmium 2000 1980 99.0 2000 1970 98.5 2000 1970 98.5

Calcium anr

Cerium

Chromium 2000 1980 99.0 2000 1990 99.5 2000 1990 99.5

Cobalt anr

Copper anr

Iron anr

Lead 2000 2050 102.5 2000 2060 103.0 2000 2060 103.0

Lithium

Magnesium anr

Manganese anr

Molybdenum

Nickel anr

Phosphorus

Potassium anr

Selenium 2000 1960 98.0 2000 1970 98.5 2000 1970 98.5

Silicon

Silver 250 245 98.0 250 245 98.0 250 244 97.6

Sodium anr

Strontium

Sulfur

Thallium anr

Tin

Titanium

Tungsten

Vanadium anr

JD48247

Login Number: JD48247 Account: HAZTMDW - HazTrain, Inc.

Project: Joint Base McGuire Dix, Lakehurst,NJ Haz Waste

File ID: SF072222M1.ICP Date Analyzed: 07/22/22 Methods: EPA 200.7, SW846 6010D QC Limits: 95 to 105 % Recovery Run ID: MA52760 Units: ug/l

Time: 09:37 10:32 11:27 Sample ID: CCV CCV3 CCV CCV4 CCV CCV5

Metal True Results % Rec True Results % Rec True Results % Rec

Zinc anr

Zirconium

(*) Outside of QC limits (anr) Analyte not requested

JD48247

Login Number: JD48247 Account: HAZTMDW - HazTrain, Inc.

Project: Joint Base McGuire Dix, Lakehurst,NJ Haz Waste

File ID: SF072222M1.ICP Date Analyzed: 07/22/22 Methods: EPA 200.7, SW846 6010D QC Limits: 95 to 105 % Recovery Run ID: MA52760 Units: ug/l

Time: 12:28 13:23 14:23 Sample ID: CCV CCV6 CCV CCV7 CCV CCV8

Metal True Results % Rec True Results % Rec True Results % Rec

Aluminum anr

Antimony anr

Arsenic 2000 1970 98.5 2000 1980 99.0 2000 1970 98.5

Barium 2000 1990 99.5 2000 2020 101.0 2000 1980 99.0

Beryllium anr

Bismuth

Boron

Cadmium 2000 1970 98.5 2000 1950 97.5 2000 1940 97.0

Calcium anr

Cerium

Chromium 2000 2000 100.0 2000 1980 99.0 2000 1970 98.5

Cobalt anr

Copper anr

Iron anr

Lead 2000 2060 103.0 2000 2040 102.0 2000 2050 102.5

Lithium

Magnesium anr

Manganese anr

Molybdenum

Nickel anr

Phosphorus

Potassium anr

Selenium 2000 1960 98.0 2000 1950 97.5 2000 1940 97.0

Silicon

Silver 250 245 98.0 250 247 98.8 250 246 98.4

Sodium anr

Strontium

Sulfur

Thallium anr

Tin

Titanium

Tungsten

Vanadium anr

JD48247

Login Number: JD48247 Account: HAZTMDW - HazTrain, Inc.

Project: Joint Base McGuire Dix, Lakehurst,NJ Haz Waste

File ID: SF072222M1.ICP Date Analyzed: 07/22/22 Methods: EPA 200.7, SW846 6010D QC Limits: 95 to 105 % Recovery Run ID: MA52760 Units: ug/l

Time: 12:28 13:23 14:23 Sample ID: CCV CCV6 CCV CCV7 CCV CCV8

Metal True Results % Rec True Results % Rec True Results % Rec

Zinc anr

Zirconium

(*) Outside of QC limits (anr) Analyte not requested

JD48247

Login Number: JD48247 Account: HAZTMDW - HazTrain, Inc.

Project: Joint Base McGuire Dix, Lakehurst,NJ Haz Waste

File ID: SF072222M1.ICP Date Analyzed: 07/22/22 Methods: EPA 200.7, SW846 6010D QC Limits: 95 to 105 % Recovery Run ID: MA52760 Units: ug/l

Time: 15:24 16:25 Sample ID: CCV CCV9 CCV CCV10

Metal True Results % Rec True Results % Rec

Aluminum anr

Antimony anr

Arsenic 2000 1980 99.0 2000 1960 98.0

Barium 2000 1980 99.0 2000 1980 99.0

Beryllium anr

Bismuth

Boron

Cadmium 2000 1950 97.5 2000 1930 96.5

Calcium anr

Cerium

Chromium 2000 1980 99.0 2000 1970 98.5