Attachment - AL-Oxide TCLP 2020.pdf

07/09/20

Technical Report for

OTIE

Joint Base McGuire Dix, Lakehurst,NJ

2019082 PO#12880_CTP0003

SGS Job Number: JD9367

Sampling Date: 06/30/20

Report to:

harold.hornung.1@us.af.mil william.flockhart@us.af.mil gloria.abarca@us.af.mil lynn.sherman@us.af.mil Mitch.Haight@cardno-gs.com;BWhipple@otie.com;JHojdila@otie.com ATTN: Distribution5

Total number of pages in report:

Certifications: NJ(12129), NY(10983), CA, CT, FL, IL, IN, KS, KY, LA, MA, MD, ME, MN, NC, OH VAP (CL0056), AK (UST-103), AZ (AZ0786), PA, RI, SC, TX, UT, VA, WV, DoD ELAP (ANAB L2248)

This report shall not be reproduced, except in its entirety, without the written approval of SGS.

Test results relate only to samples analyzed.

SGS North America Inc. • 2235 Route 130 • Dayton, NJ 08810 • tel: 732-329-0200 • fax: 732-329-3499

Test results contained within this data package meet the requirements of the National Environmental Laboratory Accreditation Program and/or state specific certification programs as applicable.

Client Service contact: Ayesha Kapadia 732-329-0200

Laura Degenhardt General Manager

Dayton, NJ 07/09/20 e-Hardcopy 2.0 Automated Report

SGS is the sole authority for authorizing edits or modifications to this document.

Unauthorized modification of this report is strictly prohibited.

Review standard terms at: http://www.sgs.com/en/terms-and-conditions

The results set forth herein are provided by SGS North America Inc.

Please share your ideas about how we can serve you better at:

EHS.US.CustomerCare@sgs.com

JD9367

mailto:EHS.US.CustomerCare@sgs.com?subject=Customer care improvement idea (report JD9367)

Table of Contents -1-

Sections:

Section 1: Sample Summary Section 2: Case Narrative/Conformance Summary Section 3: Summary of Hits Section 4: Sample Results

4.1: JD9367-1: 063020 ALUM OX

Section 5: Misc. Forms

5.1: Chain of Custody

SGS LabLink@15:37 09-Jul-2020

Sample Summary

OTIE

Job No: JD9367

Joint Base McGuire Dix, Lakehurst,NJ Project No: 2019082 PO#12880_CTP0003

Sample Collected Matrix Client Number Date Time By Received Code Type Sample ID

JD9367-1 06/30/20 08:10 RA 06/30/20 SO Solid 063020 ALUM OX

Soil samples reported on a dry weight basis unless otherwise indicated on result page.

On 06/30/2020, 1 Sample(s), 0 Trip Blank(s) and 0 Field Blank(s) were received at SGS North America Inc. at a maximum corrected temperature of 3.1 C. Samples were intact and chemically preserved, unless noted below. A SGS North America Inc. Job Number of JD9367 was assigned to the project. Laboratory sample ID, client sample ID and dates of sample collection are detailed in the report’s Results Summary Section.

Specified quality control criteria were achieved for this job except as noted below. For more information, please refer to the analytical results and QC summary pages.

Client: OTIE

Site: Joint Base McGuire Dix, Lakehurst,NJ

Job No JD9367

Report Date 7/9/2020 2:10:03 PM

CASE NARRATIVE / CONFORMANCE SUMMARY

Compounds qualified as out of range in the continuing calibration summary report are acceptable as per method requirements when there is a high bias but the sample result is non-detect.

Metals Analysis By Method SW846 6010D Matrix: LEACHATE Batch ID: MP21758

All samples were digested within the recommended method holding time.

All method blanks for this batch meet method specific criteria.

Sample(s) JD9367-1MS, JD9367-1MSD, JD9367-1SDL were used as the QC samples for metals.

Metals Analysis By Method SW846 7470A Matrix: LEACHATE Batch ID: MP21770

All samples were digested within the recommended method holding time.

All method blanks for this batch meet method specific criteria.

Sample(s) JD9367-1MS, JD9367-1MSD were used as the QC samples for metals.

SGS North America Inc. certifies that data reported for samples received, listed on the associated custody chain or analytical task order, were produced to specifications meeting the Quality System precision, accuracy and completeness objectives except as noted.

Estimated non-standard method measurement uncertainty data is available on request, based on quality control bias and implicit for standard methods. Acceptable uncertainty requires tested parameter quality control data to meet method criteria.

SGS North America Inc. is not responsible for data quality assumptions if partial reports are used and recommends that this report be used in its entirety. Data release is authorized by SGS North America Inc indicated via signature on the report cover

Thursday, July 09, 2020 Page 1 of 1

Summary of Hits Page 1 of 1 Job Number: JD9367 Account: OTIE Project: Joint Base McGuire Dix, Lakehurst,NJ Collected: 06/30/20

Lab Sample ID Client Sample ID Result/ Analyte Qual LOQ LOD Units Method

JD9367-1 063020 ALUM OX

Barium 0.79 J 1.0 0.50 mg/l SW846 6010D Cadmium 0.056 0.020 0.010 mg/l SW846 6010D Chromium 1.2 0.050 0.025 mg/l SW846 6010D Lead 11.3 0.50 0.015 mg/l SW846 6010D

Sample Results

Report of Analysis

Dayton, NJ Section 4

Report of Analysis Page 1 of 1

Client Sample ID: 063020 ALUM OX

Lab Sample ID: JD9367-1 Date Sampled: 06/30/20

Matrix: SO - Solid Date Received: 06/30/20

Percent Solids: n/a

Project: Joint Base McGuire Dix, Lakehurst,NJ

Metals Analysis, TCLP Leachate SW846 1311

Analyte Result HW# MCL LOQ LOD DL Units DF Prep Analyzed By Method

Arsenic 0.015 U D004 5.0 0.50 0.015 0.014 mg/l 1 07/02/20 07/06/20 ND SW846 6010D 2

Barium 0.79 J D005 100 1.0 0.50 0.067 mg/l 1 07/02/20 07/06/20 ND SW846 6010D 2

Cadmium 0.056 D006 1.0 0.020 0.010 0.0050 mg/l 1 07/02/20 07/06/20 ND SW846 6010D 2

Chromium 1.2 D007 5.0 0.050 0.025 0.010 mg/l 1 07/02/20 07/06/20 ND SW846 6010D 2

Lead 11.3 D008 5.0 0.50 0.015 0.0090 mg/l 1 07/02/20 07/06/20 ND SW846 6010D 2

Mercury 0.00015 U D009 0.20 0.000200.00015 0.000095mg/l 1 07/06/20 07/06/20 TG SW846 7470A 1

Selenium 0.040 U D010 1.0 0.50 0.040 0.025 mg/l 1 07/02/20 07/06/20 ND SW846 6010D 2

Silver 0.020 U D011 5.0 0.050 0.020 0.0095 mg/l 1 07/02/20 07/06/20 ND SW846 6010D 2

(1) Instrument QC Batch: MA48914

(2) Instrument QC Batch: MA48916

(3) Prep QC Batch: MP21758

(4) Prep QC Batch: MP21770

LOQ = Limit of Quantitation DL = Detection Limit U = Indicates a result < LOD

LOD = Limit of Detection B = Analyte found in associated blank J = Indicates a result >= DL (MDL) but < LOQ

JD9367

4.1

Misc. Forms

Custody Documents and Other Forms

Includes the following where applicable:

• Chain of Custody

Dayton, NJ Section 5

SGS

50 L-- CHAIN OF CUSTODY Page_l_ot _j

SGS North America Inc •• Dayto1 " FED-EXTl'-=klngf """"°""'""""''AL< - /Jf. "Jt::>ll-Jt;..· 'J.

1480 SGS Quote#

SGSJobl l I) 9"'_> {.; 7 -

Client I Reporting lnfonnatlon Pro""" Information Matrix.Codes Company Name: Project Name:

OTIE Lakehurst HW Characterization tJw-DmkngWater GW - Ground Water

Street Addre&10 ..... WW-Water

9601 McAJllater FRWY Suite 310 Allllnn Information Of different from D-..rt to'

SW - Surface Water SO-Soil

Cdy state Zip City State Company Name SL- Sludge

San Antonio TX 78~ SEO-Sediment 01-m

Ptolect Contact E-mail Project# Street Address LIQ - other Liquid

JalmeHojdll Jhojd-.com 2019082 .. AIR-M SOL- Olhef Solid

Phone# Client Purchase Order # City State ZJp WP-Wipe 480-252-6551 12880_ CTPOOOJ FB - Field Blmlk

Samolerls) Name(s) Phone# Proiecl: Man&Qer Attention Ee.Equipment Blank

RB- Rinse Blank Jaime Hojdila

.!! TB-T~Blank

"°""""" NumberofpreservedBottlel J;l

~ i 2 ~ oos .. ...,.. Grab(G) #of ~ i ~

11 0 &imple# Field ID I Poi'lt of Collection MEOHIDIVlal# °"'' T1me by Comp(C) ...... ...... ~ 15 ~ w I- LAB USE ONLY

-( O) O ( '2.o z.o ,4/v"' o:r (/JJ/lu 810 £~ c I )(" ,,,.-- "I

I cs ./

Tum Around Time (Business Days) Deliverable Comments I SnAcial Instructions

Appfoved By (SGS PM): I o.te: D Commerdal "'A"' {Level 1} D NYASP C.legOfy A C:::J DOD.QSM&

0 10 Buslneu D•ys D Commercial "'B" (level 2) D NYASP Clltegory B

1rutiai Assessmoot~T D • ........ Dllvs D NJ Reduced IL-3) D MAMCP c•teoa __ D 3 Business Days• D FuH Tier I (Level •l D CTRCP COtelta __

D 2BullnHsDays• D Commercial '"C"' D StateForms Label Verification 01eu-.D11y" D NJDKQf' D EDD Format ___

D0tt1e• Commetdlll "'A"= Results only; Conunercilil "B" =Results+ QC SUmmary

AJ data available 'Jia Labink • a....__.i needed for 1-3 Buslneu Day TAT Com~I .. C" = Results + QC Summarv + Partial Raw data httn://www __ !}fll?.:.90mf,.,n/terms-and-conditions

I . . ·~..,- ;> /, Ramm. Custadv must be docum911ted below each time HmD'91 chllnne ~•ion, including courier delivAr .

1~-;,re.. ~ -~1< ~~'~fl<>~-./\ l";i't.'"ti "'';,,, f-J,..,.,. ./\ 0oo.1nmo'(L~'1 :r Received By: \) 11 /• ?o.' l> 2

Rellnqu1(,lt by: O.te/Tlme: RecelvHBy: ' Rellnqulahed By: ,- Date/Time: Recllved By: - 3 3 4 4

Relinquished by: 0.ta/Tlme: Recelv.d By:

CuatodySMI# '1_.::t 1 ~ .1 ~ ::;",_ Pr....v.d where applk:llble

LJ2.JA A Cooler Temp. 'C

5 5 AbMl1I D Therm. ID: .'i _ c.;lcl"A

Lak.etust ~d COC HW 1 16.20 I

".1.

JD9367: Chain of Custody

JD9367

5.1

Job Number: JD9367 Client: OTIE

Date / Time Received: 6/30/2020 1:45:00 PM Delivery Method:

Project: JOINT BASE MCGUIRE DIX, LAKEHURST,NJ

4. No. Coolers: 1

Airbill #'s:

Cooler Security

1. Custody Seals Present:

Y or N

2. Custody Seals Intact:

3. COC Present:

4. Smpl Dates/Time OK

2. Cooler temp verification:

Cooler Temperature Y or N

1. Temp criteria achieved:

3. Cooler media:

IR Gun

Ice (Bag)

Quality Control Preservation Y or N N/A

1. Trip Blank present / cooler:

2. Trip Blank listed on COC:

3. Samples preserved properly:

4. VOCs headspace free:

Sample Integrity - Documentation Y or N

1. Sample labels present on bottles:

2. Container labeling complete:

3. Sample container label / COC agree:

Sample Integrity - Condition Y or N

1. Sample recvd within HT:

3. Condition of sample:

2. All containers accounted for:

Sample Integrity - Instructions

1. Analysis requested is clear:

2. Bottles received for unspecified tests

3. Sufficient volume recvd for analysis:

4. Compositing instructions clear:

5. Filtering instructions clear:

Intact

Y or N

Comments

Y or N N/A

Cooler Temps (Raw Measured) °C:

Cooler Temps (Corrected) °C:

Cooler 1: (3.4);

Cooler 1: (3.1);

SM089-03

Rev. Date 12/7/17

SGS Sample Receipt Summary

Test Strip Lot #s: pH 1-12: 229517 pH 12+: 208717 Other: (Specify)

JD9367: Chain of Custody

JD9367

5.1