ATTACHMENT5.doc

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Attached to
Fertilizer Federal contract opportunity
Solicitation number
W912EF-16-Q-0075
Issued by
Department of the Army Corps of Engineers Engineering District Walla Walla

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Attachment 5

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ATTACHMENT 5.

Sample Preparation, Analysis Methods and Standards for Total Metal Concentration.

Metal

Atomic Absorption

Inductively

Coupled

Plasma Mass

Spectroscopy

(ICP/MS)

ppm

Standard for Fertilizer

Arsenic (As)
---
6020
<1.0000
Cadmium (Cd)
---
6020
<1.0000
Cobalt (Co)
---
6020
<1.0000
Lead (Pb)
---
6020
<1.0000
Molybdenum (Mo)
---
6020
<1.0000
Nickel (Ni)
---
6020
<1.0000
Selenium (Se)
---
6020
<1.0000
Zinc (Zn)
---
6020
<1.0000
Mercury (Hg)
7470A*, 7471A*

<0.5000

Sample Preparation
---
3050B

Copies of SW-846 Third Edition and all associated updates are available from: The Government Printing Office, Superintendent of Documents, Washington, DC 20402, (202) 512-1800, and from the Department of Commerce, National Technical Information Center, 5285 Port Royal Road, Springfield, VA 22161, (703) 487-4650 or 800-553-NTIS. The online version of this document is located at: http://www.epa.gov/waste/hazard/testmethods/sw846/online/index.htm.

*Sample preparation method 3050B cannot be used for an analysis of mercury. Instead, the sample preparation methods are described under procedures for analysis methods 7470A and 7471A.

** Updated methods of analysis acceptable to the EPA may be utilized, provided that the required level of detection required in the above table ate met.

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