ASSET_LAB_Sample_results.pdf

PDF 722 KB Posted

Attached to
Soil Transportation and Disposal Federal contract opportunity
Solicitation number
FA4861-18-Q-C021
Issued by
Department of the Air Force Air Combat Command

About this file

From the source

This is the soil analysis report.

View the file

Other files for this federal contract opportunity

Other files attached to Soil Transportation and Disposal, newest first.
File Type Posted
FA4861-18-Q-C021.pdf PDF

On GovTribe

Work with this file on GovTribe

  • Download the original file
  • Contacts named in this file
  • Similar government files
  • Ask GovTribe AI about this file
Try for free Login

Text version

The file's text, extracted by GovTribe without its formatting.

NEVADA|P:702.307.2659 F:702.307.2691

3151 W. Post Rd., Las Vegas, NV 89118 ELAP Cert 2676 | NV Cert NV00922

ORELAP/NELAP Cert 4046 “Serving Clients with Passion and Professionalism”

CALIFORNIA|P:562.219.7435 F:562.219.7436

11110 Artesia Blvd., Ste B, Cerritos, CA 90703

ELAP Cert 2921

EPA ID CA01638

February 06, 2018

Nellis Air Force Base David Zeider

Attention: David Zeider

RE:

Workorder No.: N028315FAX: (702) 652-2021

TEL: (702) 652-3159

6020 Beale Ave.

Las Vegas, NV 89191

Thank you for the opportunity to service the needs of your company.

Please feel free to call me at (702) 307-2659 if I can be of further assistance to your company.

Sincerely, Quennie Manimtim

Laboratory Director

Enclosed are the results for sample(s) received on January 29, 2018 by ASSET Laboratories . The sample(s) are tested for the parameters as indicated in the enclosed chain of custody in accordance with the applicable laboratory certifications.

The cover letter is an integral part of this analytical report. This Laboratory Report cannot be reproduced in part or in its entirety without written permission from the client and Advanced Technology Laboratories - Las Vegas.

ELAP Cert 2676 | NV Cert NV00922

ORELAP/NELAP Cert 4046 “Serving Clients with Passion and Professionalism”

CALIFORNIA|P:562.219.7435 F:562.219.7436

11110 Artesia Blvd., Ste B, Cerritos, CA 90703

06-Feb-18Date:ASSET Laboratories

Project:

CLIENT: Nellis Air Force Base

Lab Order: N028315

CASE NARRATIVE

SAMPLE RECEIVING/GENERAL COMMENTS:

Samples were received intact with proper chain of custody documentation.

Cooler temperature and sample preservation were verified upon receipt of samples if applicable.

Information on sample receipt conditions including discrepancies can be found in attached Sample Receipt Checklist Form.

Samples were analyzed within method holding time.

ELAP Cert 2676 | NV Cert NV00922

ORELAP/NELAP Cert 4046 “Serving Clients with Passion and Professionalism”

CALIFORNIA|P:562.219.7435 F:562.219.7436

11110 Artesia Blvd., Ste B, Cerritos, CA 90703

CLIENT: Nellis Air Force Base

Lab Order: N028315 Work Order Sample Summary

Lab Sample ID Client Sample ID Collection DateMatrix Date Received

Contract No:

Date Reported

N028315-001A 1 1/29/2018 4:00:00 PM 1/29/2018 2/6/2018Soil

N028315-002A 2 1/29/2018 4:04:00 PM 1/29/2018 2/6/2018Soil

N028315-003A 3 1/29/2018 4:06:00 PM 1/29/2018 2/6/2018Soil

N028315-004A 4 1/29/2018 4:11:00 PM 1/29/2018 2/6/2018Soil

N028315-005A 5 1/29/2018 4:16:00 PM 1/29/2018 2/6/2018Soil

N028315-006A 6 1/29/2018 4:17:00 PM 1/29/2018 2/6/2018Soil

N028315-007A 7 1/29/2018 4:22:00 PM 1/29/2018 2/6/2018Soil

N028315-008A 8 1/29/2018 4:26:00 PM 1/29/2018 2/6/2018Soil

N028315-009A 9 1/29/2018 4:28:00 AM 1/29/2018 2/6/2018Soil

N028315-010A 10 1/29/2018 4:34:00 PM 1/29/2018 2/6/2018Soil

N028315-011A 11 1/29/2018 4:38:00 PM 1/29/2018 2/6/2018Soil

N028315-012A 12 1/29/2018 4:41:00 PM 1/29/2018 2/6/2018Soil

N028315-013A 13 1/29/2018 4:44:00 PM 1/29/2018 2/6/2018Soil

N028315-014A 14 1/29/2018 4:47:00 PM 1/29/2018 2/6/2018Soil

ELAP Cert 2676 | NV Cert NV00922

ORELAP/NELAP Cert 4046 “Serving Clients with Passion and Professionalism”

CALIFORNIA|P:562.219.7435 F:562.219.7436

11110 Artesia Blvd., Ste B, Cerritos, CA 90703

Client Sample ID: 1 Collection Date: 1/29/2018 4:00:00 PM

Matrix: SOIL

Analyses Result Qual Units Date Analyzed

CLIENT: Nellis Air Force Base Lab Order: N028315

DF

Lab ID: N028315-001

ASSET Laboratories Print Date: 06-Feb-18

PQL

ANALYTICAL RESULTS

DIESEL & MOTOR OIL RANGE ORGANICS BY GC/FID

EPA 8015B

Analyst: JJS

EPA 3550B

RunID: NV00922-GC3_180130A 66605QC Batch: PrepDate 1/30/2018

DRO 1/30/2018 07:21 PM9.9 mg/Kg 1600 ORO 1/30/2018 07:21 PM9.9 mg/Kg 152 Surr: p-Terphenyl 1/30/2018 07:21 PM38-152 %REC 192.5

GASOLINE RANGE ORGANICS BY GC/FID

EPA 8015B

Analyst: QBMRunID: NV00922-GC4_180130A E18VS016QC Batch: PrepDate

GRO 1/30/2018 10:38 PM1.0 mg/Kg 11.3 Surr: Chlorobenzene - d5 1/30/2018 10:38 PM46-157 %REC 180.0

Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded ND Not Detected at the Reporting Limit S Spike/Surrogate outside of limits due to matrix interference Results are wet unless otherwise specified

DO Surrogate Diluted Out

ELAP Cert 2676 | NV Cert NV00922

ORELAP/NELAP Cert 4046 “Serving Clients with Passion and Professionalism”

CALIFORNIA|P:562.219.7435 F:562.219.7436

11110 Artesia Blvd., Ste B, Cerritos, CA 90703

Client Sample ID: 2 Collection Date: 1/29/2018 4:04:00 PM

Matrix: SOIL

Analyses Result Qual Units Date Analyzed

CLIENT: Nellis Air Force Base Lab Order: N028315

DF

Lab ID: N028315-002

ASSET Laboratories Print Date: 06-Feb-18

PQL

ANALYTICAL RESULTS

DIESEL & MOTOR OIL RANGE ORGANICS BY GC/FID

EPA 8015B

Analyst: JJS

EPA 3550B

RunID: NV00922-GC3_180130A 66605QC Batch: PrepDate 1/30/2018

DRO 1/30/2018 07:47 PM9.9 mg/Kg 13600 ORO 1/30/2018 07:47 PM9.9 mg/Kg 184 Surr: p-Terphenyl 1/30/2018 07:47 PM38-152 %REC 194.2

GASOLINE RANGE ORGANICS BY GC/FID

EPA 8015B

Analyst: QBMRunID: NV00922-GC4_180201A E18VS017QC Batch: PrepDate

GRO 2/1/2018 06:45 PM50 mg/Kg 50580 Surr: Chlorobenzene - d5 2/1/2018 06:45 PM46-157 %REC 5073.5

Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded ND Not Detected at the Reporting Limit S Spike/Surrogate outside of limits due to matrix interference Results are wet unless otherwise specified

ELAP Cert 2676 | NV Cert NV00922

ORELAP/NELAP Cert 4046 “Serving Clients with Passion and Professionalism”

CALIFORNIA|P:562.219.7435 F:562.219.7436

11110 Artesia Blvd., Ste B, Cerritos, CA 90703

Client Sample ID: 3 Collection Date: 1/29/2018 4:06:00 PM

Matrix: SOIL

Analyses Result Qual Units Date Analyzed

CLIENT: Nellis Air Force Base Lab Order: N028315

DF

Lab ID: N028315-003

ASSET Laboratories Print Date: 06-Feb-18

PQL

ANALYTICAL RESULTS

DIESEL & MOTOR OIL RANGE ORGANICS BY GC/FID

EPA 8015B

Analyst: JJS

EPA 3550B

RunID: NV00922-GC3_180130A 66605QC Batch: PrepDate 1/30/2018

DRO 1/30/2018 08:13 PM9.9 mg/Kg 13400 ORO 1/30/2018 08:13 PM9.9 mg/Kg 1130 Surr: p-Terphenyl 1/30/2018 08:13 PM38-152 %REC 192.3

GASOLINE RANGE ORGANICS BY GC/FID

EPA 8015B

Analyst: QBMRunID: NV00922-GC4_180201A E18VS017QC Batch: PrepDate

GRO 2/1/2018 07:18 PM50 mg/Kg 50290 Surr: Chlorobenzene - d5 2/1/2018 07:18 PM46-157 %REC 5066.8

Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded ND Not Detected at the Reporting Limit S Spike/Surrogate outside of limits due to matrix interference Results are wet unless otherwise specified

ELAP Cert 2676 | NV Cert NV00922

ORELAP/NELAP Cert 4046 “Serving Clients with Passion and Professionalism”

CALIFORNIA|P:562.219.7435 F:562.219.7436

11110 Artesia Blvd., Ste B, Cerritos, CA 90703

Client Sample ID: 4 Collection Date: 1/29/2018 4:11:00 PM

Matrix: SOIL

Analyses Result Qual Units Date Analyzed

CLIENT: Nellis Air Force Base Lab Order: N028315

DF

Lab ID: N028315-004

ASSET Laboratories Print Date: 06-Feb-18

PQL

ANALYTICAL RESULTS

DIESEL & MOTOR OIL RANGE ORGANICS BY GC/FID

EPA 8015B

Analyst: JJS

EPA 3550B

RunID: NV00922-GC3_180130A 66605QC Batch: PrepDate 1/30/2018

DRO 1/30/2018 08:39 PM9.9 mg/Kg 119 ORO 1/30/2018 08:39 PM9.9 mg/Kg 152 Surr: p-Terphenyl 1/30/2018 08:39 PM38-152 %REC 182.7

GASOLINE RANGE ORGANICS BY GC/FID

EPA 8015B

Analyst: QBMRunID: NV00922-GC4_180130A E18VS016QC Batch: PrepDate

GRO 1/30/2018 08:24 PM1.0 mg/Kg 1ND Surr: Chlorobenzene - d5 1/30/2018 08:24 PM46-157 %REC 1121

Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded ND Not Detected at the Reporting Limit S Spike/Surrogate outside of limits due to matrix interference Results are wet unless otherwise specified

ELAP Cert 2676 | NV Cert NV00922

ORELAP/NELAP Cert 4046 “Serving Clients with Passion and Professionalism”

CALIFORNIA|P:562.219.7435 F:562.219.7436

11110 Artesia Blvd., Ste B, Cerritos, CA 90703

Client Sample ID: 5 Collection Date: 1/29/2018 4:16:00 PM

Matrix: SOIL

Analyses Result Qual Units Date Analyzed

CLIENT: Nellis Air Force Base Lab Order: N028315

DF

Lab ID: N028315-005

ASSET Laboratories Print Date: 06-Feb-18

PQL

ANALYTICAL RESULTS

DIESEL & MOTOR OIL RANGE ORGANICS BY GC/FID

EPA 8015B

Analyst: JJS

EPA 3550B

RunID: NV00922-GC3_180130A 66605QC Batch: PrepDate 1/30/2018

DRO 1/30/2018 09:05 PM10 mg/Kg 166 ORO 1/30/2018 09:05 PM10 mg/Kg 186 Surr: p-Terphenyl 1/30/2018 09:05 PM38-152 %REC 186.8

GASOLINE RANGE ORGANICS BY GC/FID

EPA 8015B

Analyst: QBMRunID: NV00922-GC4_180130A E18VS016QC Batch: PrepDate

GRO 1/30/2018 05:00 PM1.0 mg/Kg 1ND Surr: Chlorobenzene - d5 1/30/2018 05:00 PM46-157 %REC 168.5

Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded ND Not Detected at the Reporting Limit S Spike/Surrogate outside of limits due to matrix interference Results are wet unless otherwise specified

ELAP Cert 2676 | NV Cert NV00922

ORELAP/NELAP Cert 4046 “Serving Clients with Passion and Professionalism”

CALIFORNIA|P:562.219.7435 F:562.219.7436

11110 Artesia Blvd., Ste B, Cerritos, CA 90703

Client Sample ID: 6 Collection Date: 1/29/2018 4:17:00 PM

Matrix: SOIL

Analyses Result Qual Units Date Analyzed

CLIENT: Nellis Air Force Base Lab Order: N028315

DF

Lab ID: N028315-006

ASSET Laboratories Print Date: 06-Feb-18

PQL

ANALYTICAL RESULTS

DIESEL & MOTOR OIL RANGE ORGANICS BY GC/FID

EPA 8015B

Analyst: JJS

EPA 3550B

RunID: NV00922-GC3_180130A 66605QC Batch: PrepDate 1/30/2018

DRO 1/30/2018 09:31 PM10 mg/Kg 126 ORO 1/30/2018 09:31 PM10 mg/Kg 132 Surr: p-Terphenyl 1/30/2018 09:31 PM38-152 %REC 185.1

GASOLINE RANGE ORGANICS BY GC/FID

EPA 8015B

Analyst: QBMRunID: NV00922-GC4_180130A E18VS016QC Batch: PrepDate

GRO 1/30/2018 08:57 PM1.0 mg/Kg 1ND Surr: Chlorobenzene - d5 1/30/2018 08:57 PM46-157 %REC 146.6

Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded ND Not Detected at the Reporting Limit S Spike/Surrogate outside of limits due to matrix interference Results are wet unless otherwise specified

ELAP Cert 2676 | NV Cert NV00922

ORELAP/NELAP Cert 4046 “Serving Clients with Passion and Professionalism”

CALIFORNIA|P:562.219.7435 F:562.219.7436

11110 Artesia Blvd., Ste B, Cerritos, CA 90703

Client Sample ID: 7 Collection Date: 1/29/2018 4:22:00 PM

Matrix: SOIL

Analyses Result Qual Units Date Analyzed

CLIENT: Nellis Air Force Base Lab Order: N028315

DF

Lab ID: N028315-007

ASSET Laboratories Print Date: 06-Feb-18

PQL

ANALYTICAL RESULTS

DIESEL & MOTOR OIL RANGE ORGANICS BY GC/FID

EPA 8015B

Analyst: JJS

EPA 3550B

RunID: NV00922-GC3_180130A 66605QC Batch: PrepDate 1/30/2018

DRO 1/30/2018 09:58 PM10 mg/Kg 130 ORO 1/30/2018 09:58 PM10 mg/Kg 144 Surr: p-Terphenyl 1/30/2018 09:58 PM38-152 %REC 181.9

GASOLINE RANGE ORGANICS BY GC/FID

EPA 8015B

Analyst: QBMRunID: NV00922-GC4_180130A E18VS016QC Batch: PrepDate

GRO 1/30/2018 06:40 PM1.0 mg/Kg 1ND Surr: Chlorobenzene - d5 1/30/2018 06:40 PM46-157 %REC 197.7

Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded ND Not Detected at the Reporting Limit S Spike/Surrogate outside of limits due to matrix interference Results are wet unless otherwise specified

ELAP Cert 2676 | NV Cert NV00922

ORELAP/NELAP Cert 4046 “Serving Clients with Passion and Professionalism”

CALIFORNIA|P:562.219.7435 F:562.219.7436

11110 Artesia Blvd., Ste B, Cerritos, CA 90703

Client Sample ID: 8 Collection Date: 1/29/2018 4:26:00 PM

Matrix: SOIL

Analyses Result Qual Units Date Analyzed

CLIENT: Nellis Air Force Base Lab Order: N028315

DF

Lab ID: N028315-008

ASSET Laboratories Print Date: 06-Feb-18

PQL

ANALYTICAL RESULTS

DIESEL & MOTOR OIL RANGE ORGANICS BY GC/FID

EPA 8015B

Analyst: JJS

EPA 3550B

RunID: NV00922-GC3_180130A 66605QC Batch: PrepDate 1/30/2018

DRO 1/30/2018 10:24 PM10 mg/Kg 157 ORO 1/30/2018 10:24 PM10 mg/Kg 123 Surr: p-Terphenyl 1/30/2018 10:24 PM38-152 %REC 184.3

GASOLINE RANGE ORGANICS BY GC/FID

EPA 8015B

Analyst: QBMRunID: NV00922-GC4_180201A E18VS017QC Batch: PrepDate

GRO 2/1/2018 08:26 PM5.0 mg/Kg 5ND Surr: Chlorobenzene - d5 2/1/2018 08:26 PM46-157 %REC 578.8

Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded ND Not Detected at the Reporting Limit S Spike/Surrogate outside of limits due to matrix interference Results are wet unless otherwise specified

ELAP Cert 2676 | NV Cert NV00922

ORELAP/NELAP Cert 4046 “Serving Clients with Passion and Professionalism”

CALIFORNIA|P:562.219.7435 F:562.219.7436

11110 Artesia Blvd., Ste B, Cerritos, CA 90703

Client Sample ID: 9 Collection Date: 1/29/2018 4:28:00 AM

Matrix: SOIL

Analyses Result Qual Units Date Analyzed

CLIENT: Nellis Air Force Base Lab Order: N028315

DF

Lab ID: N028315-009

ASSET Laboratories Print Date: 06-Feb-18

PQL

ANALYTICAL RESULTS

DIESEL & MOTOR OIL RANGE ORGANICS BY GC/FID

EPA 8015B

Analyst: JJS

EPA 3550B

RunID: NV00922-GC3_180130A 66605QC Batch: PrepDate 1/30/2018

DRO 1/30/2018 10:50 PM10 mg/Kg 132 ORO 1/30/2018 10:50 PM10 mg/Kg 157 Surr: p-Terphenyl 1/30/2018 10:50 PM38-152 %REC 185.6

GASOLINE RANGE ORGANICS BY GC/FID

EPA 8015B

Analyst: QBMRunID: NV00922-GC4_180130A E18VS016QC Batch: PrepDate

GRO 1/30/2018 07:13 PM1.0 mg/Kg 1ND Surr: Chlorobenzene - d5 1/30/2018 07:13 PM46-157 %REC 154.5

Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded ND Not Detected at the Reporting Limit S Spike/Surrogate outside of limits due to matrix interference Results are wet unless otherwise specified

ELAP Cert 2676 | NV Cert NV00922

ORELAP/NELAP Cert 4046 “Serving Clients with Passion and Professionalism”

CALIFORNIA|P:562.219.7435 F:562.219.7436

11110 Artesia Blvd., Ste B, Cerritos, CA 90703

Client Sample ID: 10 Collection Date: 1/29/2018 4:34:00 PM

Matrix: SOIL

Analyses Result Qual Units Date Analyzed

CLIENT: Nellis Air Force Base Lab Order: N028315

DF

Lab ID: N028315-010

ASSET Laboratories Print Date: 06-Feb-18

PQL

ANALYTICAL RESULTS

DIESEL & MOTOR OIL RANGE ORGANICS BY GC/FID

EPA 8015B

Analyst: JJS

EPA 3550B

RunID: NV00922-GC3_180130A 66605QC Batch: PrepDate 1/30/2018

DRO 2/2/2018 01:41 PM100 mg/Kg 107500 ORO 1/30/2018 11:16 PM10 mg/Kg 1220 Surr: p-Terphenyl 1/30/2018 11:16 PM38-152 %REC 189.4

GASOLINE RANGE ORGANICS BY GC/FID

EPA 8015B

Analyst: QBMRunID: NV00922-GC4_180130A E18VS016QC Batch: PrepDate

GRO 1/30/2018 10:04 PM1.0 mg/Kg 1ND Surr: Chlorobenzene - d5 1/30/2018 10:04 PM46-157 %REC 191.6

Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded ND Not Detected at the Reporting Limit S Spike/Surrogate outside of limits due to matrix interference Results are wet unless otherwise specified

ELAP Cert 2676 | NV Cert NV00922

ORELAP/NELAP Cert 4046 “Serving Clients with Passion and Professionalism”

CALIFORNIA|P:562.219.7435 F:562.219.7436

11110 Artesia Blvd., Ste B, Cerritos, CA 90703

Client Sample ID: 11 Collection Date: 1/29/2018 4:38:00 PM

Matrix: SOIL

Analyses Result Qual Units Date Analyzed

CLIENT: Nellis Air Force Base Lab Order: N028315

DF

Lab ID: N028315-011

ASSET Laboratories Print Date: 06-Feb-18

PQL

ANALYTICAL RESULTS

DIESEL & MOTOR OIL RANGE ORGANICS BY GC/FID

EPA 8015B

Analyst: JJS

EPA 3550B

RunID: NV00922-GC3_180130A 66605QC Batch: PrepDate 1/30/2018

DRO 1/30/2018 04:18 PM200 mg/Kg 2015000 ORO 1/30/2018 02:34 PM10 mg/Kg 1520 Surr: p-Terphenyl 1/30/2018 02:34 PM38-152 %REC 191.0

GASOLINE RANGE ORGANICS BY GC/FID

EPA 8015B

Analyst: QBMRunID: NV00922-GC4_180130A E18VS016QC Batch: PrepDate

GRO 1/30/2018 01:40 PM500 mg/Kg 5001900 Surr: Chlorobenzene - d5 1/30/2018 01:40 PM46-157 %REC 50088.5

Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded ND Not Detected at the Reporting Limit S Spike/Surrogate outside of limits due to matrix interference Results are wet unless otherwise specified

ELAP Cert 2676 | NV Cert NV00922

ORELAP/NELAP Cert 4046 “Serving Clients with Passion and Professionalism”

CALIFORNIA|P:562.219.7435 F:562.219.7436

11110 Artesia Blvd., Ste B, Cerritos, CA 90703

Client Sample ID: 12 Collection Date: 1/29/2018 4:41:00 PM

Matrix: SOIL

Analyses Result Qual Units Date Analyzed

CLIENT: Nellis Air Force Base Lab Order: N028315

DF

Lab ID: N028315-012

ASSET Laboratories Print Date: 06-Feb-18

PQL

ANALYTICAL RESULTS

DIESEL & MOTOR OIL RANGE ORGANICS BY GC/FID

EPA 8015B

Analyst: JJS

EPA 3550B

RunID: NV00922-GC3_180130A 66605QC Batch: PrepDate 1/30/2018

DRO 1/30/2018 04:44 PM1000 mg/Kg 10067000 ORO 1/30/2018 03:00 PM10 mg/Kg 12100 Surr: p-Terphenyl 1/30/2018 03:00 PM38-152 %REC 185.7

GASOLINE RANGE ORGANICS BY GC/FID

EPA 8015B

Analyst: QBMRunID: NV00922-GC4_180130A E18VS016QC Batch: PrepDate

GRO 1/30/2018 02:13 PM500 mg/Kg 5003100 Surr: Chlorobenzene - d5 1/30/2018 02:13 PM46-157 %REC 50068.7

Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded ND Not Detected at the Reporting Limit S Spike/Surrogate outside of limits due to matrix interference Results are wet unless otherwise specified

ELAP Cert 2676 | NV Cert NV00922

ORELAP/NELAP Cert 4046 “Serving Clients with Passion and Professionalism”

CALIFORNIA|P:562.219.7435 F:562.219.7436

11110 Artesia Blvd., Ste B, Cerritos, CA 90703

Client Sample ID: 13 Collection Date: 1/29/2018 4:44:00 PM

Matrix: SOIL

Analyses Result Qual Units Date Analyzed

CLIENT: Nellis Air Force Base Lab Order: N028315

DF

Lab ID: N028315-013

ASSET Laboratories Print Date: 06-Feb-18

PQL

ANALYTICAL RESULTS

DIESEL & MOTOR OIL RANGE ORGANICS BY GC/FID

EPA 8015B

Analyst: JJS

EPA 3550B

RunID: NV00922-GC3_180130A 66605QC Batch: PrepDate 1/30/2018

DRO 1/30/2018 05:10 PM500 mg/Kg 5041000 ORO 1/30/2018 03:26 PM10 mg/Kg 11100 Surr: p-Terphenyl 1/30/2018 03:26 PM38-152 %REC 188.8

GASOLINE RANGE ORGANICS BY GC/FID

EPA 8015B

Analyst: QBMRunID: NV00922-GC4_180130A E18VS016QC Batch: PrepDate

GRO 1/30/2018 02:46 PM500 mg/Kg 5002700 Surr: Chlorobenzene - d5 1/30/2018 02:46 PM46-157 %REC 50078.3

Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded ND Not Detected at the Reporting Limit S Spike/Surrogate outside of limits due to matrix interference Results are wet unless otherwise specified

ELAP Cert 2676 | NV Cert NV00922

ORELAP/NELAP Cert 4046 “Serving Clients with Passion and Professionalism”

CALIFORNIA|P:562.219.7435 F:562.219.7436

11110 Artesia Blvd., Ste B, Cerritos, CA 90703

Client Sample ID: 14 Collection Date: 1/29/2018 4:47:00 PM

Matrix: SOIL

Analyses Result Qual Units Date Analyzed

CLIENT: Nellis Air Force Base Lab Order: N028315

DF

Lab ID: N028315-014

ASSET Laboratories Print Date: 06-Feb-18

PQL

ANALYTICAL RESULTS

DIESEL & MOTOR OIL RANGE ORGANICS BY GC/FID

EPA 8015B

Analyst: JJS

EPA 3550B

RunID: NV00922-GC3_180130A 66605QC Batch: PrepDate 1/30/2018

DRO 1/30/2018 03:52 PM10 mg/Kg 121 ORO 1/30/2018 03:52 PM10 mg/Kg 147 Surr: p-Terphenyl 1/30/2018 03:52 PM38-152 %REC 179.4

GASOLINE RANGE ORGANICS BY GC/FID

EPA 8015B

Analyst: QBMRunID: NV00922-GC4_180130A E18VS016QC Batch: PrepDate

GRO 1/30/2018 06:06 PM1.0 mg/Kg 1ND Surr: Chlorobenzene - d5 1/30/2018 06:06 PM46-157 %REC 165.9

Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded ND Not Detected at the Reporting Limit S Spike/Surrogate outside of limits due to matrix interference Results are wet unless otherwise specified

ELAP Cert 2676 | NV Cert NV00922

ORELAP/NELAP Cert 4046 “Serving Clients with Passion and Professionalism”

CALIFORNIA|P:562.219.7435 F:562.219.7436

11110 Artesia Blvd., Ste B, Cerritos, CA 90703

CLIENT: Nellis Air Force Base Work Order: N028315

ANALYTICAL QC SUMMARY REPORT

TestCode: 8015_S_DM H

Sample ID LCS-66605

Batch ID: 66605 TestNo: EPA 8015B Analysis Date: 1/30/2018

Prep Date: 1/30/2018

Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual

Units: mg/Kg

PQL

Client ID: LCSS

RunNo: 121730

SeqNo: 2913296

LCSSampType: TestCode: 8015_S_DM

EPA 3550B

DRO 1000 83.2 67 11910 0831.808

Surr: p-Terphenyl 80.00 85.7 38 15268.564

Sample ID MB-66605

Batch ID: 66605 TestNo: EPA 8015B Analysis Date: 1/30/2018

Prep Date: 1/30/2018

Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual

Units: mg/Kg

PQL

Client ID: PBS

RunNo: 121730

SeqNo: 2913297

MBLKSampType: TestCode: 8015_S_DM

EPA 3550B

DRO 104.871

ORO 105.043

Surr: p-Terphenyl 80.00 82.9 38 15266.282

Sample ID N028303-005A-MS

Batch ID: 66605 TestNo: EPA 8015B Analysis Date: 1/30/2018

Prep Date: 1/30/2018

Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual

Units: mg/Kg

PQL

Client ID: ZZZZZZ

RunNo: 121730

SeqNo: 2913300

MSSampType: TestCode: 8015_S_DM

EPA 3550B

DRO 1001 79.3 46 14310 9.920803.898

Surr: p-Terphenyl 80.08 82.2 38 15265.815

Sample ID N028303-005A-MSD

Batch ID: 66605 TestNo: EPA 8015B Analysis Date: 1/30/2018

Prep Date: 1/30/2018

Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual

Units: mg/Kg

PQL

Client ID: ZZZZZZ

RunNo: 121730

SeqNo: 2913301

MSDSampType: TestCode: 8015_S_DM

EPA 3550B

DRO 1004 84.4 46 143 2010 9.920 803.9 6.43857.320

Surr: p-Terphenyl 80.32 82.3 38 152 066.126

Qualifiers:

B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded

ND Not Detected at the Reporting Limit R RPD outside accepted recovery limits S Spike/Surrogate outside of limits due to matrix interference DO Surrogate Diluted Out Calculations are based on raw values

ELAP Cert 2676 | NV Cert NV00922

ORELAP/NELAP Cert 4046 “Serving Clients with Passion and Professionalism”

CALIFORNIA|P:562.219.7435 F:562.219.7436

11110 Artesia Blvd., Ste B, Cerritos, CA 90703

CLIENT: Nellis Air Force Base Work Order: N028315

ANALYTICAL QC SUMMARY REPORT

TestCode: 8015GAS_S

Sample ID E180130LCS

Batch ID: E18VS016 TestNo: EPA 8015B Analysis Date: 1/30/2018

Prep Date:

Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual

Units: mg/Kg

PQL

Client ID: LCSS

RunNo: 121721

SeqNo: 2912737

LCSSampType: TestCode: 8015GAS_S

GRO 5.000 95.6 74 1271.0 04.780

Surr: Chlorobenzene - d5 100.0 95.1 46 15795.083

Sample ID E180130LCSD

Batch ID: E18VS016 TestNo: EPA 8015B Analysis Date: 1/30/2018

Prep Date:

Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual

Units: mg/Kg

PQL

Client ID: LCSS02

RunNo: 121721

SeqNo: 2912738

LCSDSampType: TestCode: 8015GAS_S

GRO 5.000 102 74 127 201.0 0 4.780 6.285.090

Surr: Chlorobenzene - d5 100.0 98.3 46 157 098.300

Sample ID E180130MB1

Batch ID: E18VS016 TestNo: EPA 8015B Analysis Date: 1/30/2018

Prep Date:

Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual

Units: mg/Kg

PQL

Client ID: PBS

RunNo: 121721

SeqNo: 2912739

MBLKSampType: TestCode: 8015GAS_S

GRO 1.00.062

Surr: Chlorobenzene - d5 100.0 114 46 157113.846

Qualifiers:

B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded

ND Not Detected at the Reporting Limit R RPD outside accepted recovery limits S Spike/Surrogate outside of limits due to matrix interference

ELAP Cert 2676 | NV Cert NV00922

ORELAP/NELAP Cert 4046 “Serving Clients with Passion and Professionalism”

CALIFORNIA|P:562.219.7435 F:562.219.7436

11110 Artesia Blvd., Ste B, Cerritos, CA 90703

Work Order: N028315

ANALYTICAL QC SUMMARY REPORT

TestCode: 8015GAS_S

Sample ID E180201LCS

Batch ID: E18VS017 TestNo: EPA 8015B Analysis Date: 2/1/2018

Prep Date:

Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual

Units: mg/Kg

PQL

Client ID: LCSS

RunNo: 121794

SeqNo: 2915824

LCSSampType: TestCode: 8015GAS_S

GRO 5.000 104 74 1271.0 05.190

Surr: Chlorobenzene - d5 100.0 98.5 46 15798.516

Sample ID E180201LCSD

Batch ID: E18VS017 TestNo: EPA 8015B Analysis Date: 2/1/2018

Prep Date:

Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual

Units: mg/Kg

PQL

Client ID: LCSS02

RunNo: 121794

SeqNo: 2915825

LCSDSampType: TestCode: 8015GAS_S

GRO 5.000 91.2 74 127 201.0 0 5.190 12.94.562

Surr: Chlorobenzene - d5 100.0 91.5 46 157 091.459

Sample ID E180201MB1

Batch ID: E18VS017 TestNo: EPA 8015B Analysis Date: 2/1/2018

Prep Date:

Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual

Units: mg/Kg

PQL

Client ID: PBS

RunNo: 121794

SeqNo: 2915826

MBLKSampType: TestCode: 8015GAS_S

GRO 1.00.054

Surr: Chlorobenzene - d5 100.0 111 46 157111.151

Sample ID N028315-008AMS

Batch ID: E18VS017 TestNo: EPA 8015B Analysis Date: 2/1/2018

Prep Date:

Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual

Units: mg/Kg

PQL

Client ID: ZZZZZZ

RunNo: 121794

SeqNo: 2915838

MSSampType: TestCode: 8015GAS_S

GRO 25.00 100 27 1445.0 3.11028.210

Surr: Chlorobenzene - d5 500.0 92.6 46 157463.185

Sample ID N028315-008AMSD

Batch ID: E18VS017 TestNo: EPA 8015B Analysis Date: 2/1/2018

Prep Date:

Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual

Units: mg/Kg

PQL

Client ID: ZZZZZZ

RunNo: 121794

SeqNo: 2915839

MSDSampType: TestCode: 8015GAS_S

GRO 25.00 82.3 27 144 205.0 3.110 28.21 17.523.680

Qualifiers:

B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded

ND Not Detected at the Reporting Limit R RPD outside accepted recovery limits S Spike/Surrogate outside of limits due to matrix interference

ELAP Cert 2676 | NV Cert NV00922

ORELAP/NELAP Cert 4046 “Serving Clients with Passion and Professionalism”

CALIFORNIA|P:562.219.7435 F:562.219.7436

11110 Artesia Blvd., Ste B, Cerritos, CA 90703

Work Order: N028315

ANALYTICAL QC SUMMARY REPORT

TestCode: 8015GAS_S

Sample ID N028315-008AMSD

Batch ID: E18VS017 TestNo: EPA 8015B Analysis Date: 2/1/2018

Prep Date:

Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual

Units: mg/Kg

PQL

Client ID: ZZZZZZ

RunNo: 121794

SeqNo: 2915839

MSDSampType: TestCode: 8015GAS_S

Surr: Chlorobenzene - d5 500.0 82.6 46 157 0413.105

Qualifiers:

B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded

ND Not Detected at the Reporting Limit R RPD outside accepted recovery limits S Spike/Surrogate outside of limits due to matrix interference

ASSET Laboratories Please review the checklist below. Any NO signifies non-compliance. Any non-compliance will be noted and must be understood as having an impact on the quality of the data. All tests will be performed as requested regardless of any compliance issues.

If you have any questions or further instruction, please contact our Project Coordinator at (702) 307-2659.

Carrier name: ASSET

Cooler Received/Opened On: 1/29/2018

Rep sample Temp (Deg C): 2.3 IR Gun ID: 2

Temp Blank: Yes No

Last 4 digits of Tracking No.: NA

Cooling process: Ice Ice Pack Dry Ice Other None

Packing Material Used: None

Workorder: N028315

Sample Receipt Checklist

4. Chain of custody present? Yes No

6. Chain of custody signed when relinquished and received? Yes No

7. Chain of custody agrees with sample labels? Yes No

8. Samples in proper container/bottle? Yes No

9. Sample containers intact? Yes No

10. Sufficient sample volume for indicated test? Yes No

11. All samples received within holding time? Yes No

Yes No NA13. Water - VOA vials have zero headspace?

14. Water - pH acceptable upon receipt? Yes No NA Example: pH > 12 for (CN,S); pH<2 for Metals

1. Shipping container/cooler in good condition? Yes No Not Present

2. Custody seals intact, signed, dated on shippping container/cooler? Yes No Not Present

3. Custody seals intact on sample bottles? Yes No Not Present

5. Sampler's name present in COC? Yes No

12. Temperature of rep sample or Temp Blank within acceptable limit? Yes No NA

Yes No NA15. Did the bottle labels indicate correct preservatives used?

16. Were there Non-Conformance issues at login? Yes No NA Was Client notified? Yes No NA

Comments: Collection time taken from sample labels.

Checklist Completed By: YR Reviewed By:

Sample ID Client Sample ID Date Collected

Date Received:

Date Due Matrix Test No

WORK ORDER Summary 29-Jan-18

WorkOrder: N028315

Comments: Results needed Wednesday1/31/18 in the morning.

Client ID: NELAI01 Project: QC Level: RTNE

Hld MS Sub

1/29/2018

Test Name

ASSET Laboratories

Storage

N028315-001A 1 1/29/2018 4:00:00 PM 2/5/2018 Soil EPA 8015B DIESEL & MOTOR OIL RANGE

ORGANICS BY GC/FID

VS/WS

2/5/2018 EPA 8015B GASOLINE RANGE ORGANICS BY

GC/FID

VS/WS

2/5/2018 EPA 3550B SHAKE-OUT METHOD: EXTRACTABLE

FUELS

VS/WS

N028315-002A 2 1/29/2018 4:04:00 PM 2/5/2018 EPA 8015B DIESEL & MOTOR OIL RANGE

ORGANICS BY GC/FID

VS/WS

2/5/2018 EPA 8015B GASOLINE RANGE ORGANICS BY

GC/FID

VS/WS

2/5/2018 EPA 3550B SHAKE-OUT METHOD: EXTRACTABLE

FUELS

VS/WS

N028315-003A 3 1/29/2018 4:06:00 PM 2/5/2018 EPA 8015B DIESEL & MOTOR OIL RANGE

ORGANICS BY GC/FID

VS/WS

2/5/2018 EPA 8015B GASOLINE RANGE ORGANICS BY

GC/FID

VS/WS

2/5/2018 EPA 3550B SHAKE-OUT METHOD: EXTRACTABLE

FUELS

VS/WS

N028315-004A 4 1/29/2018 4:11:00 PM 2/5/2018 EPA 8015B DIESEL & MOTOR OIL RANGE

ORGANICS BY GC/FID

VS/WS

2/5/2018 EPA 8015B GASOLINE RANGE ORGANICS BY

GC/FID

VS/WS

2/5/2018 EPA 3550B SHAKE-OUT METHOD: EXTRACTABLE

FUELS

VS/WS

N028315-005A 5 1/29/2018 4:16:00 PM 2/5/2018 EPA 8015B DIESEL & MOTOR OIL RANGE

ORGANICS BY GC/FID

VS/WS

2/5/2018 EPA 8015B GASOLINE RANGE ORGANICS BY

GC/FID

VS/WS

2/5/2018 EPA 3550B SHAKE-OUT METHOD: EXTRACTABLE

FUELS

VS/WS

N028315-006A 6 1/29/2018 4:17:00 PM 2/5/2018 EPA 8015B DIESEL & MOTOR OIL RANGE

ORGANICS BY GC/FID

VS/WS

2/5/2018 EPA 8015B GASOLINE RANGE ORGANICS BY

GC/FID

VS/WS

1 of 3Page

Date Due Matrix Test No

WORK ORDER Summary 29-Jan-18

WorkOrder: N028315

Comments: Results needed Wednesday1/31/18 in the morning.

Client ID: NELAI01 Project: QC Level: RTNE

Hld MS Sub

1/29/2018

Test Name

ASSET Laboratories

Storage

N028315-006A 6 1/29/2018 4:17:00 PM 2/5/2018 Soil EPA 3550B SHAKE-OUT METHOD: EXTRACTABLE

FUELS

VS/WS

N028315-007A 7 1/29/2018 4:22:00 PM 2/5/2018 EPA 8015B DIESEL & MOTOR OIL RANGE

ORGANICS BY GC/FID

VS/WS

2/5/2018 EPA 8015B GASOLINE RANGE ORGANICS BY

GC/FID

VS/WS

2/5/2018 EPA 3550B SHAKE-OUT METHOD: EXTRACTABLE

FUELS

VS/WS

N028315-008A 8 1/29/2018 4:26:00 PM 2/5/2018 EPA 8015B DIESEL & MOTOR OIL RANGE

ORGANICS BY GC/FID

VS/WS

2/5/2018 EPA 8015B GASOLINE RANGE ORGANICS BY

GC/FID

VS/WS

2/5/2018 EPA 3550B SHAKE-OUT METHOD: EXTRACTABLE

FUELS

VS/WS

N028315-009A 9 1/29/2018 4:28:00 AM 2/5/2018 EPA 8015B DIESEL & MOTOR OIL RANGE

ORGANICS BY GC/FID

VS/WS

2/5/2018 EPA 8015B GASOLINE RANGE ORGANICS BY

GC/FID

VS/WS

2/5/2018 EPA 3550B SHAKE-OUT METHOD: EXTRACTABLE

FUELS

VS/WS

N028315-010A 10 1/29/2018 4:34:00 PM 2/5/2018 EPA 8015B DIESEL & MOTOR OIL RANGE

ORGANICS BY GC/FID

VS/WS

2/5/2018 EPA 8015B GASOLINE RANGE ORGANICS BY

GC/FID

VS/WS

2/5/2018 EPA 3550B SHAKE-OUT METHOD: EXTRACTABLE

FUELS

VS/WS

N028315-011A 11 1/29/2018 4:38:00 PM 1/30/2018 EPA 8015B DIESEL & MOTOR OIL RANGE

ORGANICS BY GC/FID

VS/WS

1/30/2018 EPA 8015B GASOLINE RANGE ORGANICS BY

GC/FID

VS/WS

1/30/2018 EPA 3550B SHAKE-OUT METHOD: EXTRACTABLE

FUELS

VS/WS

N028315-012A 12 1/29/2018 4:41:00 PM 1/30/2018 EPA 8015B DIESEL & MOTOR OIL RANGE

ORGANICS BY GC/FID

VS/WS

2 of 3Page

Date Due Matrix Test No

WORK ORDER Summary 29-Jan-18

WorkOrder: N028315

Comments: Results needed Wednesday1/31/18 in the morning.

Client ID: NELAI01 Project: QC Level: RTNE

Hld MS Sub

1/29/2018

Test Name

ASSET Laboratories

Storage

N028315-012A 12 1/29/2018 4:41:00 PM 1/30/2018 Soil EPA 8015B GASOLINE RANGE ORGANICS BY

GC/FID

VS/WS

1/30/2018 EPA 3550B SHAKE-OUT METHOD: EXTRACTABLE

FUELS

VS/WS

N028315-013A 13 1/29/2018 4:44:00 PM 1/30/2018 EPA 8015B DIESEL & MOTOR OIL RANGE

ORGANICS BY GC/FID

VS/WS

1/30/2018 EPA 8015B GASOLINE RANGE ORGANICS BY

GC/FID

VS/WS

1/30/2018 EPA 3550B SHAKE-OUT METHOD: EXTRACTABLE

FUELS

VS/WS

N028315-014A 14 1/29/2018 4:47:00 PM 2/5/2018 EPA 8015B DIESEL & MOTOR OIL RANGE

ORGANICS BY GC/FID

VS/WS

2/5/2018 EPA 8015B GASOLINE RANGE ORGANICS BY

GC/FID

VS/WS

2/5/2018 EPA 3550B SHAKE-OUT METHOD: EXTRACTABLE

FUELS

VS/WS

N028315-015A FOLDER 1/30/2018 1/30/2018 Folder Folder LAB

1/30/2018 Folder Folder LAB

3 of 3Page

File details come from the government source that posted it.