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Attachment 6- Limits of Quantitation (LOQs)
| National Lead Lab Accreditation Program (NLLAP) Sample Analysis |
| Method |
| LIMITS |
| Units |
| Lead Prep/Paint Chip |
| Accredited NLLAP Method |
| Lead Prep/Soil |
| Accredited NLLAP Method |
| Lead Prep/Wipe |
| Accredited NLLAP Method |
| 10 |
| micrograms |
| Organic/Inorganic Compound Groups |
| Method |
| LIMITS |
| Units |
Ethyl Alcohol
Isopropyl Alcohol
Tert-Butyl Alcohol
n-Butyl Alcohol
sec-Butyl Alcohol
Isobutyl Alcohol n-Propyl Alcohol
Allyl Alcohol
Diacetone Alcohol
Cyclohexanol
Isoamyl Alcohol
Methyl Isobutyl Carbinol
2-Methoxyethanol
2-Ethoxyethanol
2-Butoxyethanol
Hydrogen Bromide
Hydrogen Chloride
Hydrogen Cyanide
Hydrogen Fluoride
Nitric Acid
Phosphoric Acid
Sulfuric Acid
Cyclohexane
Cyclohexene
n-Decane
n-Dodecane
n-Heptane
n-Hexane
Methylcyclohexane
n-Nonane
n-Octane
n-Pentane
n-Undecane
| Hydrocarbons, Aromatic |
| NIOSH |
| 1501 |
Benzene
Ethyl Benzene
Styrene
Toluene
Xylenes (Total)
| Hydrocarbons, Halogenated |
| NIOSH |
| 1003 |
Carbon Tetrachloride
Chlorobenzene
Chloroform
1,1-Dichloroethane
1,2-Dichloroethane
Hexachloroethane
Tetrachloroethylene
Trichloroethylene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
1,2-Dichlorobenzene (o-)
1,4-Dichlorobenzene (p-)
1,6-HDI
HMDI
IPDI
MDI
2,4-TDI
2,6-TDI
Acetone
2-Hexanone
Cyclohexnone
Methyl Isobutyl ketone
Diisobutyl Ketone
2-pentanone
Camphor
Mesityl oxide
5-methyl-3-heptanone
Methyl-(n-amyl)-ketone
Ethyl buytl ketone
| Inorganic Acids |
| NIOSH |
| 7903 |
Hydrogen Bromide
Hydrogen Chloride
Hydrogen Fluoride
Nitric Acid
Phosphoric Acid
Sulfuric Acid
| Metals |
| NIOSH/OSHA |
| 7300/125 |
Aluminum
Antimony
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Selenium
Silver
Strontium
Thallium
Titanium
Vanadium
Zinc
| Metals Wipe Sample |
| NIOSH/EPA/ ASTM |
| 9102/6010/ 1613 |
Aluminum
Antimony
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Strontium
Vanadium
Zinc
n-Amyl Acetate
2-Ethoxyethyl acetate
n-Propyl acetate
1-Butyl Acetate
Methyl isoamyl acetate sec-Butyl Acetate
Isobutyl Acetate
n-Butyl Acetate
Isoamyl Acetate
Ethyl acrylate
| Organophosphorus Pesticides |
| OSHA |
| 62 |
Chlorpyrifos
Diazinon
Dichlorvos
Malathion
Parathion
| Isoflurane |
| OSHA |
| 103 |
| 5 |
| micrograms |
| Sevoflurane |
| OSHA |
| 103 |
| 5 |
| micrograms |
| Desflurane |
| OSHA |
| 106 |
| 5 |
| micrograms |
| Naphthas |
| NIOSH |
| 1550 |
| 100 |
| micrograms |
| 1- Bromopropane |
| OSHA |
| PV 2061 |
| 1-methoxy-2-propanol |
| OSHA |
| 99 |
| 1,2,4-Trimethyl benzene |
| OSHA |
| 07 |
| 2,4-Dichlorophenoxyacetic Acid (2, 4-D) |
| NIOSH |
| 5001 |
| 2,4-Dinitrotoluene (2,4-DNT) |
| OSHA |
| 44 |
| 0.04 |
| micrograms |
| 2-Methoxyethylacate |
| NIOSH |
| 1451 |
| 2-Methoxymethylethoxy propanol (PPG-2 methyl ether) |
| OSHA |
| 101 |
| Acetic Acid |
| OSHA |
| ID 186 |
| 10 |
| micrograms |
| Acetonitrile |
| NIOSH |
| 1606 |
| 10 |
| micrograms |
| Acrolein |
| OSHA |
| 52 |
| 1 |
| micrograms |
| Amines, Aliphatic |
| NIOSH |
| 2010 |
| Ammonia |
| OSHA -ID |
| 186 |
| 25 |
| micrograms |
| Asbestos Fiber Count |
| NIOSH |
| 7400 |
| 7 |
| fibers/mm2 |
| Asbestos by TEM |
| NIOSH |
| 7402 |
| 7 |
| fibers/mm2 |
| Asbestos by TEM Full Quant - Bulk |
| TEMELAP |
| 198.4 |
| NA |
| NA |
Anthracene
Benzo(a)pyrene
Chrysene
Phenanthrene
Pyrene
Benzene Solubles (all of the above)
| Bulk Asbestos |
| EPA |
| 600.0/R93/116 |
| Organic/Inorganic Compound Groups |
| Method |
| Butyl Acetate |
| NIOSH |
| 1450 |
| 50 |
| micrograms |
| Butyl Cellosolve Acetate |
| OSHA |
| 83 |
| Carbon Disulfide |
| NIOSH |
| 1600 |
| 20 |
| micrograms |
| Chlordane |
| NIOSH |
| 5510 |
| 0.1 |
| micrograms |
| Chromium, Hexavalent (Cr VI) |
| OSHA- ID |
| 215 |
| 0.045 |
| micrograms |
Anthracene
Benzo(a)pyrene
Chrysene
Phenanthrene
Pyrene
Benzene Solubles
| Cresol, Modified |
| OSHA |
| 32 |
| 1.1 |
| micrograms |
| Cyanide |
| NIOSH |
| 6010 |
| 1 |
| micrograms |
| Cyanide |
| NIOSH |
| 7904 |
| 2.5 |
| micrograms |
| Dibromoethane |
| NIOSH |
| 1008 |
| 0.01 |
| micrograms |
| DichlorodifluoroMethane |
| NIOSH |
| 1018 |
| Diethylene glycol methyl ether (Methyl Carbitol) |
| OSHA |
| Mod. 101 |
| Dimethyformamide |
| NIOSH |
| 2004 |
| Dioctyl Phthalate |
| NIOSH |
| 5020 |
| Diproplene glycol methyl ether |
| OSHA |
| 53 |
| Di-sec-octylphalate |
| NIOSH |
| 5020 |
| Elemental Carbon |
| NIOSH |
| 5040 |
| 0.3 |
| micrograms |
| Endrin |
| NIOSH |
| 5519 |
| 0.02 |
| micrograms |
| Epichlorohydrin |
| NIOSH |
| 1010 |
| 1 |
| micrograms |
| Ethanolamine |
| NIOSH/OSHA |
| 2007/60 |
| Ethyl 2-Cyanoacrylate |
| OSHA |
| 55 |
| 0.8 |
| micrograms |
| Ethyl Acetate |
| NIOSH |
| 1457 |
| 50 |
| micrograms |
| Ethyl Ether |
| NIOSH |
| 1610 |
| 20 |
| micrograms |
| Ethylene Dibromide |
| NIOSH |
| 1008 |
| 0.1 |
| micrograms |
| Ethylene Glycol |
| NIOSH |
| 5523 |
| 5 |
| micrograms |
| Ethylene glycol dinitrate (EGDN) |
| NIOSH |
| 2507 |
| 0.3 |
| micrograms |
| Ethylene Oxide (ETO) |
| 3M & NIOSH |
| 1614 |
| 0.5 |
| micrograms |
| Fiber Count "B Counting Rules" |
| NIOSH |
| 7400 |
| Fluoride (Water soluble particulate and Gaseous) |
| NIOSH |
| 7902 |
| 10 |
| micrograms |
| Fluorides (Total Aero&Gas ) (Hydrogen Fluoride & Fluoride (F)) |
| NIOSH |
| 7902 |
| 400 |
| micrograms |
| Formaldehyde |
| NIOSH |
| 2016 |
| 0.5 |
| micrograms |
| Formaldehyde |
| NIOSH/OSHA |
| 2016/ID-205 |
| Gluteraldehyde |
| NIOSH |
| 2532 |
| 0.3 |
| micrograms |
| Glycols (each glycol) |
| NIOSH |
| 5523 |
| Hydroquinone |
| NIOSH |
| 5004 |
| 3 |
| micrograms |
| Hydrogen Sulfide |
| NIOSH |
| 6013 |
| 11 |
| micrograms |
| Isobutyl Isobutyrate |
| NIOSH |
| 1550/1501 |
| Isophorone |
| NIOSH |
| 2508 |
| 50 |
| micrograms |
| Isophorone diisocyanate (IPDI) |
| OSHA |
| PV2034 |
| Isopropyl Acetate |
| NIOSH |
| 1454 |
| Methanol (Methyl Alcohol) |
| NIOSH |
| 2000 |
| 30 |
| micrograms |
| Organic/Inorganic Compounds |
| Method |
| Methyl Acetate |
| NIOSH |
| 1458 |
| 20 |
| micrograms |
| Methyl Chloroform |
| NIOSH |
| 1003 |
| Methyl Ethyl Ketone (MEK) |
| NIOSH/OSHA |
| 250016 |
| Methyl ethyl ketone peroxide (MEKP) |
| NIOSH/OSHA |
| 3508/77 |
| Methyl Isocyanate |
| OSHA |
| 54 |
| Methyl Methacrylate |
| NIOSH |
| 2537 |
| 20 |
| micrograms |
| Methylene Chloride |
| NIOSH |
| 1005 |
| 20 |
| micrograms |
| Mineral Oil |
| NIOSH |
| 5026 |
| 100 |
| micrograms |
| Nitric Oxide/Nitrogen Dioxide |
| OSHA |
| ID-190/ ID-182 |
| Nitrogen Dioxide |
| NIOSH |
| 6014 |
| N-Methyl-2-pyrrolidone |
| NIOSH |
| 1302 |
| Oil Mist |
| NIOSH |
| 500 |
| 100 |
| micrograms |
| Ozone |
| OSHA |
| ID-214 |
| 5 |
| micrograms |
| Particulates N.O.R (Resp) |
| NIOSH |
| 0600 |
| 100 |
| micrograms |
| Particulates N.O.R (Total) |
| NIOSH |
| 0500 |
| 100 |
| micrograms |
| PCBs (Aroclor 1221, 1260, 1262, 1268, 1016, 1242, 1254, 1248) |
| NIOSH |
| 5503 |
| Pentachlorophenol |
| OSHA |
| 39 |
| 2 |
| micrograms |
| Phenol |
| OSHA |
| 32 |
| 10 |
| micrograms |
| Phenyl Glycidyl Ether |
| NIOSH |
| 1619 |
| Phosphorus, White/Yellow |
| NIOSH |
| 7905 |
| 0.05 |
| micrograms |
| Potassium Hydroxide |
| NIOSH |
| 7401 |
| 30 |
| micrograms |
| Propyl Bromide |
| OSHA |
| IMIS R290 |
| Silica, Crystalline (Respirable) |
| NIOSH |
| 7500 |
| 10 |
| micrograms |
| Silica, Crystalline (Total) |
| NIOSH |
| 7500 |
| 10 |
| micrograms |
| Sodium Hydroxide |
| NIOSH |
| 7401 |
| 30 |
| micrograms |
| Sulfuric Acid |
| OSHA |
| ID-113 |
| Tetrahydrofuran |
| NIOSH |
| 1609 |
| 100 |
| micrograms |
| 2,4,6-Trinitrotoluene (TNT) |
| OSHA |
| 44 |
| 0.05 |
| micrograms |
| Trichloroethylene (TCE) |
| NIOSH |
| 1022 |
| 20 |
| micrograms |
| Trichlorofluoromethane |
| NIOSH |
| 1006 |
| Triethanolamine |
| OSHA |
| PV2141 |
| Triethylenetetramine |
| NIOSH |
| 2540 |
| Vinyl Chloride |
| NIOSH |
| 1007 |
| Welding Fumes, Total |
| NIOSH |
| 0500 |
| 100 |
| micrograms |
| Biological Analysis |
| Method |
| Biological Micro Examination (bulk and wipes) |
| Micro |