36C24218B0247-018.pdf

Subsurface Investigation Report

US Department of Veterans Affairs

VA Hudson Valley HCS

2094 Albany Post Road

Montrose, NY 10548

STV, INC. 3015409

TABLES

VA Hudson Valley HCS

APPENDIX A

FIELD INVESTIGATION PHOTOGRAPHS

STV

INC.

225 PARK AVENUE SOUTH NEW YORK, NEW YORK 10003

PHOTO LOG� Inspector’s Report SITE: VA Hudson Valley HCS, 2094 Albany Post Road, Montrose, NY 10548

SITE OF PHOTOS: March 7 and June 24, 2013 PHOTOGRAPHER: BC

PHOTO 1: View of Site looking east.

PHOTO 2: View of Site looking west.

SITE OF PHOTOS: March, 7 and June 24, 2013 PHOTOGRAPHER: BC

PHOTO 3: View of geophysical survey on March 7, 2013.

PHOTO 4: View of the advancement of soil boring, SB�2.

SITE OF PHOTOS: June 24, 2013 PHOTOGRAPHER: BC

PHOTO 5: View of advancement of soil boring, SB�3.

PHOTO 6: View of the advancement of soil boring, SB�4.

SITE OF PHOTOS: June 24, 2013 PHOTOGRAPHER: BC

PHOTO 7: View of fill material at soil boring, SB�4.

PHOTO 8: View of the advancement of soil boring, SB�5.

SITE OF PHOTOS: June 24, 2013 PHOTOGRAPHER: BC

PHOTO 9: View of fill material at soil boring, SB�5.

PHOTO 10: View of the advancement of soil boring, SB�6.

VA Hudson Valley HCS

APPENDIX B

GEOPHYSICAL SURVEY REPORT

DIVERSIFIED GEOPHYSICS, INC.

Subsurface Geophysical Investigations 150 Nassau Terminal Road, New Hyde Park, NY 11040

(516) 326.0586 voice (516) 616.6194 fax www.DiversifiedGeophysics.com

17 April 2013

Mr. Brian Connolly, Project Scientist STV, Inc.

225 Park Avenue South New York, NY 10003

Re: Site Geophysics –Montrose VA Hospital VIA Email

Dear Mr. Connolly:

On Thursday, March 7 th , 2013, Diversified Geophysics, Inc. (DGI) performed a geophysical investigation on the property known as the Montrose VA Hospital, located at 2094 Albany Post Road, in Montrose, NY, 10548. DGI personnel met with STV personnel at the site, and followed your directions throughout the investigation.

The purpose of this investigation was to locate, trace and mark the presence of any subsurface utilities, documented or undocumented structures and/or anomalies within the areas of investigation (AOI’s), in advance of the boring program. Six (6) proposed sampling locations were investigated for obstructions and cleared for drilling.

The geophysical investigation was comprised of a series of Ground Penetrating Radar (GPR) traverses and site-wide radio frequency/electromagnetic (RF/EM) scans. GPR surveys collect anomaly data which can be interpreted in real-time. The geometry of the anomalies located can assist in determining the type of subsurface object producing the anomaly. Linear anomalies can be interpreted to be buried utilities, conduits, trolley tracks, etc., if the return data has the appropriate signature. RF/EM scans are made by using instrumentation that has a transmitter and receiver. The transmitter can be used to send electromagnetic waves of known frequencies along buried metallic conduits housing utilities, or through the utilities themselves. The receiver is used to trace the signal (audibly and/or graphically) and locate the direction of travel, in some cases, the depth of the utility below the surface. Receivers can also be used in stand-alone mode to detect frequencies in the range of 60Hz, often emitted by active electrical services in the United States. In addition, some RF/EM instruments can detect frequencies emitted by gas and water services. These utilities absorb and radiate VLF radio waves. Both technologies, GPR and RF/EM complement one another to provide the most useful data set necessary for the locating, tracing and characterization of subsurface anomalies.

Ground Penetrating Radar (GPR) data was collected with Sensors and Software 250 MHz Noggin

Plus SmartCart

The average penetration depth for this investigation was set from zero (0) to ten (10) feet. In some areas, this was increased from zero (0) to twenty (20) feet.

During this investigation, Noggin

Plus GPR traverse lines were made in sets that ran parallel and perpendicular to the footprints of the individual AOI’s, as illustrated on Figure 2. of this narrative (west and south of building 20; east, west and south of building 23; and within the landfill between the east and north gate-lines to a point 40 feet west of the storm structure, and south to the materials and equipment line). In addition, areas of the east parking area located to the south of building 19 were investigated and all accessible manhole covers were opened to evaluate the disposition of the plumbing –sanitary sewer or storm sewer. GPR scans represent anomalies graphically as hyperbolas, their crests indicating position and depth below the surface to the target. In general, when scanning for linear targets such as utilities, single-line scans are designed to traverse possible targets in directions perpendicular to the long-axis of the target. When a series of parallel scans detect anomalies at similar positions and depths, these results are interpreted to be evidence of a utility or conduit.

Single line GPR traverses in both the X and Y direction were collected throughout all accessible areas of the property.

Subsurface Geophysical Investigations 150 Nassau Terminal Road, New Hyde Park, NY 11040

A radio frequency/electromagnetic (RF/EM) survey was conducted throughout the entire area of investigation. The receiver of a Ridgid

SeekTech (SR-60) Pipe and Cable Locator was used in a stand-alone mode (without the transmitter) to locate utilities emitting frequencies in the 60Hz range (active electric). The Ridgid receiver was also used with a transmitter box (ST-33Q) in an attempt to trace water and drainage services.

Results:

All drainage conduits were traced and marked on the surface in the AOI to the west of buildings 20 and 23. Storm drainage was traced through the east fence of the former landfill area, where it entered a concrete vault located in the northeastern corner of the landfill property. Visual examination of the vault revealed that the plumbing exited the west wall of the enclosure, and may have continued through to a second concrete vault located approximately 60 feet to the southwest. Access issues prevented the tracing of this section of the storm drainage with the GPR.

Attempts were made to determine the direction of travel of storm drainage conduits entering and exiting a grated concrete structure located centrally in the former landfill area (approximately 160 feet west of the entry gate).

Anecdotal information indicated that a communication existed between the two drainage vaults to the northeast;

and that a 40 foot length of drainage pipe exited the structure on a southwest trend. GPR data sets collected throughout the AOI did not reveal any linear target returns that could be interpreted as indication of the presence of storm drainage pipe. The extremely disturbed, heterogeneous nature of the substrate was a factor in the lack of interpretable data. An additional complication, flagging and paint markings from a former geophysical study indicated a drainage conduit paralleling the north fence-line of the landfill from the second interior vault (from the east fence) to a point due north of the central storm structure. GPR traverses across this area to the north of the central drainage structure did not reveal linear anomalies that could be interpreted to be drainage conduit.

RF technology was used throughout the former landfill in an attempt to trace storm drainage. RF technology could not be used to induce a signal through a steel tape placed into the storm drainage conduit, due to the presence of water in the piping –(which would result in the loss of a traceable return signal). Signals were transmitted both inductively (by placing the transmitter box above a known or suspected section of drainage pipe), or conductively by placing the transmitter box directly on an accessible, exposed section of drainage pipe. Weak signal returns in the area to the west of the central drainage structure did appear to reveal a preferred direction to the southwest;

and similar results were encountered along the line of travel marked during the former geophysical survey (which resulted in finding the paint marks and flagging). Due to the amount of metallic debris buried in the landfill, tracing the RF signal was compromised.

Andrew D. Silver Vice President/Engineering Geologist Diversified Geophysics, Inc.

Subsurface Geophysical Investigations 150 Nassau Terminal Road, New Hyde Park, NY 11040

Figure 1. Satellite View Of Site.

Subsurface Geophysical Investigations 150 Nassau Terminal Road, New Hyde Park, NY 11040

Figure 2. Geophysical Survey Plan

Subsurface Geophysical Investigations 150 Nassau Terminal Road, New Hyde Park, NY 11040

Figure 3. Utility Trace (Not To Scale) Blue –Water; Red –Electric; Green –Drainage; Magenta –Anecdotal Information Positions; Dashed Lines –GPR/RF Data Returns Having Indications Of Linear Anomalies Or Linear Signal Traces

Subsurface Geophysical Investigations 150 Nassau Terminal Road, New Hyde Park, NY 11040

Photo 1. View North. West Side Building 20 Showing Drainage MH And Electric

Photo 2. View North. West Of Building 23 Showing Drainage And Electric

Subsurface Geophysical Investigations 150 Nassau Terminal Road, New Hyde Park, NY 11040

Photo 3. View North Of Road And Vault Positioning. Bldg. 23 To Right Of Yard Drainage

Photo 4. View Northeast Of Storm Drain MH Due South Of Bldg. 20

Subsurface Geophysical Investigations 150 Nassau Terminal Road, New Hyde Park, NY 11040

Photo 5. View Northwest Of Linear Anomaly Exiting MH In Photo 4.

Photo 6. View West From East End Of Former Landfill

Subsurface Geophysical Investigations 150 Nassau Terminal Road, New Hyde Park, NY 11040

Photo 7. View Of Northeast Corner Of Landfill Showing Drainage Vault

VA Hudson Valley HCS

APPENDIX C

LABORATORY ANALYTICAL REPORTS

ANALYTICAL REPORT

Job Number: 460-58470-1

Job Description: Montrose VA Hospital

For:

STV Incorporated

225 Park Avenue South New York, NY 10003

Attention: Mr. Brian Connolly

Approved for release.

Kristina Blocker Project Manager I

7/10/2013 1:19 PM

Designee for Melissa Haas, Project Manager I

128 Long Hill Cross Road, Shelton, CT, 06484 melissa.haas@testamericainc.com

07/10/2013

The test results in this report meet all NELAP requirements unless specified within the case narrative. Pursuant to NELAP, this report may not be reproduced, except in full, without the written approval of the laboratory. All questions regarding this report should be directed to the TestAmerica Edison Project Manager.

TestAmerica Edison Certifications and Approvals: Connecticut: CTDOH #PH-0200, New Jersey: NJDEP (NELAP) #12028, New York: NYDOH (NELAP) #11452, NYDOH (ELAP) #11452, Pennsylvania: PADEP (NELAP) 68-00522 and Rhode Island: RIDOH LAO00132

TestAmerica Laboratories, Inc.

TestAmerica Edison 777 New Durham Road, Edison, NJ 08817

Tel (732) 549-3900 Fax (732) 549-3679 www.testamericainc.com

07/10/2013Page 1 of 289 mailto:melissa.haas@testamericainc.com http://www.testamericainc.com http://

Job Number: 460-58470-1

Job Description: Montrose VA Hospital

I certify that this data package is in compliance with the terms and conditions of the contract, both technically and for completeness, for other than the conditions detailed within the body of this report. Release of the data contained in this sample data package and in the electronic data deliverable has been authorized by the Laboratory Manager or his/her designee, as verified by the following signature.

Approved for release.

Kristina Blocker Project Manager I

7/10/2013 1:19 PM

Designee for

Melissa Haas

07/10/2013Page 2 of 289

Table of Contents Cover Title Page

Report Narrative

Executive Summary

Method Summary

Method / Analyst Summary

Sample Summary

Sample Results

Sample Datasheets

Data Qualifiers

QC Results

Qc Association Summary

Surrogate Recovery Report

Qc Reports

Client Chain of Custody

Sample Receipt Checklist

07/10/2013Page 3 of 289

CASE NARRATIVE

Client: STV Incorporated

Project: Montrose VA Hospital

Report Number: 460-58470-1

This case narrative is in the form of an exception report, where only the anomalies related to this report, method specific performance and/or QA/QC issues are discussed. If there are no issues to report, this narrative will include a statement that documents that there are no relevant data issues.

It should be noted that samples with elevated Reporting Limits (RLs) as a result of a dilution may not be able to satisfy customer reporting limits in some cases. Such increases in the RLs are unavoidable but acceptable consequence of sample dilution that enables quantification of target analytes or interferences which exceed the calibration range of the instrument.

Calculations are performed before rounding to avoid round-off errors in calculated results.

All holding times were met and proper preservation noted for the methods performed on these samples, unless otherwise detailed in the individual sections below.

RECEIPT

The samples were received on 06/25/2013; the samples arrived in good condition, properly preserved and on ice. The temperature of the coolers at receipt was 2.5° C.

Note: All samples which require thermal preservation are considered acceptable if the arrival temperature is within 2C of the required temperature or method specified range. For samples with a specified temperature of 4C, samples with a temperature ranging from just above freezing temperature of water to 6C shall be acceptable. Samples that are hand delivered immediately following collection may not meet these criteria, however they will be deemed acceptable according to NELAC standards, if there is evidence that the chilling process has begun, such as arrival on ice, etc.

IGNITABILITY

Samples 460-58470-3, 460-58470-6, 460-58470-9, 460-58470-12, 460-58470-15, 460-58470-18 and 460-58470-19 were analyzed for

Ignitability in accordance with EPA SW-846 Method 1030. The samples were analyzed on 06/28/2013.

No difficulties were encountered during the burn rate analyses.

All quality control parameters were within the acceptance limits.

TCLP METALS

Samples 460-58470-3, 460-58470-6, 460-58470-9, 460-58470-12, 460-58470-15, 460-58470-18 and 460-58470-19 were analyzed for

TCLP metals in accordance with EPA SW-846 Methods 1311/ 6010B. The samples were leached on 06/26/2013 and 06/27/2013, and prepared and analyzed on 06/28/2013.

As a standard practice all TCLP samples are diluted 5X prior to analysis. Further dilutions may be required dependent upon analyte levels in the samples. Refer to the analytical results forms for dilutions.

No difficulties were encountered during the TCLP metals analyses.

All quality control parameters were within the acceptance limits.

TOTAL METALS

Samples 460-58470-1, 460-58470-2, 460-58470-4, 460-58470-5, 460-58470-7, 460-58470-8, 460-58470-10, 460-58470-11, 460-58470-13, 460-58470-14, 460-58470-16, 460-58470-17 and 460-58470-19 were analyzed for total metals in accordance with EPA

SW-846 Method 6010B. The samples were prepared and analyzed on 06/26/2013 and 06/27/2013.

Samples 460-58470-1(4X), 460-58470-2(4X), 460-58470-4(4X), 460-58470-5(4X), 460-58470-7(4X), 460-58470-8(4X), 460-58470-10(4X), 460-58470-11(4X), 460-58470-13(4X), 460-58470-14(4X), 460-58470-16(4X), 460-58470-17(4X) and

460-58470-19(4X) required dilution prior to analysis. The reporting limits have been adjusted accordingly.

As a standard practice all soil samples and related QC samples (i.e., MB, LCS, Dup, MS, SD) are diluted 2X-4X prior to analysis. Further dilutions may be required dependent upon analyte levels in the samples. Refer to the analytical results forms for dilutions.

N difficulties were encountered during the metals analyses.

All quality control parameters were within the acceptance limits.

07/10/2013Page 4 of 289

TCLP MERCURY

Samples 460-58470-3, 460-58470-6, 460-58470-9, 460-58470-12, 460-58470-15, 460-58470-18 and 460-58470-19 were analyzed for

TCLP mercury in accordance with EPA SW-846 Methods 1311/7470A. The samples were leached on 06/26/2013 and 06/27/2013, and prepared and analyzed on 06/28/2013.

No difficulties were encountered during the TCLP mercury analyses.

All quality control parameters were within the acceptance limits.

TOTAL MERCURY

Samples 460-58470-1, 460-58470-2, 460-58470-4, 460-58470-5, 460-58470-7, 460-58470-8, 460-58470-10, 460-58470-11, 460-58470-13, 460-58470-14, 460-58470-16, 460-58470-17 and 460-58470-19 were analyzed for total mercury in accordance with EPA

SW-846 Method 7471A. The samples were prepared and analyzed on 06/26/2013 and 06/27/2013.

No difficulties were encountered during the Hg analyses.

All quality control parameters were within the acceptance limits.

ORGANOCHLORINE PESTICIDES

Samples 460-58470-1, 460-58470-2, 460-58470-4, 460-58470-5, 460-58470-7, 460-58470-8, 460-58470-10, 460-58470-11, 460-58470-13, 460-58470-14, 460-58470-16, 460-58470-17 and 460-58470-19 were analyzed for organochlorine pesticides in accordance with EPA SW-846 Method 8081A. The samples were prepared on 06/26/2013 and 06/27/2013 and analyzed on 06/27/2013 and 07/01/2013.

DCB Decachlorobiphenyl failed the surrogate recovery criteria high for MB 460-167885/1-A. DCB Decachlorobiphenyl failed the surrogate recovery criteria high for 460-58552-A-6-F MS. DCB Decachlorobiphenyl failed the surrogate recovery criteria high for

460-58463-E-1-H MSD. Refer to the QC report for details.

No other difficulties were encountered during the pesticides analyses.

All other quality control parameters were within the acceptance limits.

POLYCHLORINATED BIPHENYLS

Samples 460-58470-1, 460-58470-2, 460-58470-4, 460-58470-5, 460-58470-7, 460-58470-8, 460-58470-10, 460-58470-11, 460-58470-13, 460-58470-14, 460-58470-16, 460-58470-17 and 460-58470-19 were analyzed for polychlorinated biphenyls in accordance with EPA SW-846 Method 8082. The samples were prepared and analyzed on 06/26/2013 and 06/27/2013.

The closing calibration verification (CCV) for Aroclor 1260 associated with batch 167906 recovered above the upper control limit on the secondary column. The samples associated with this CCV were non-detects for the affected analytes; therefore, the data have been reported.

No other difficulties were encountered during the PCBs analyses.

All other quality control parameters were within the acceptance limits.

CHLORINATED HERBICIDES

Samples 460-58470-1, 460-58470-2, 460-58470-4, 460-58470-5, 460-58470-7, 460-58470-8, 460-58470-10, 460-58470-11, 460-58470-13, 460-58470-14, 460-58470-16, 460-58470-17 and 460-58470-19 were analyzed for chlorinated herbicides in accordance with EPA SW-846 Method 8151A. The samples were prepared on 06/26/2013 and analyzed on 06/27/2013 and 06/28/2013.

The closing calibration verification (CCV) for analytical batch 168029 recovered outside control limits for 2,4,5-TP. The data have been qualified and reported.

Refer to the QC report for details.

No other difficulties were encountered during the herbicides analyses.

All other quality control parameters were within the acceptance limits.

VOLATILE ORGANIC COMPOUNDS (GC-MS)

Samples 460-58470-1, 460-58470-2, 460-58470-4, 460-58470-5, 460-58470-7, 460-58470-8, 460-58470-10, 460-58470-11, 460-58470-13, 460-58470-14, 460-58470-16, 460-58470-17 and 460-58470-19 were analyzed for volatile organic compounds (GC-MS) in accordance with EPA SW-846 Method 8260B. The samples were prepared on 06/27/2013 and analyzed on 07/04/2013, 07/05/2013 and

07/06/2013.

The following sample was diluted to bring the concentration of target analytes within the calibration range: SB-3A (2-4') (460-58470-7).

Elevated reporting limits (RLs) are provided.

07/10/2013Page 5 of 289

No other difficulties were encountered during the volatiles analyses.

All other quality control parameters were within the acceptance limits.

SEMIVOLATILE ORGANIC COMPOUNDS (GC-MS)

Samples 460-58470-1, 460-58470-2, 460-58470-4, 460-58470-5, 460-58470-7, 460-58470-8, 460-58470-10, 460-58470-11, 460-58470-13, 460-58470-14, 460-58470-16, 460-58470-17 and 460-58470-19 were analyzed for semivolatile organic compounds

(GC-MS) in accordance with EPA SW-846 Method 8270C. The samples were prepared on 06/25/2013 and 06/26/2013 and analyzed on

06/29/2013, 07/01/2013 and 07/02/2013.

1,2,4,5-Tetrachlorobenzene and Hexachlorocyclopentadiene failed the recovery criteria low for LCS 460-167865/2-A.

4-Chloro-3-methylphenol and 4-Nitroaniline failed the recovery criteria high. Refer to the QC report for details.

Samples 460-58470-1(5X), 460-58470-2(5X), 460-58470-4(2X), 460-58470-5(2X) and 460-58470-13(2X) required dilution prior to analysis. The reporting limits have been adjusted accordingly.

No other difficulties were encountered during the semivolatiles analyses.

All other quality control parameters were within the acceptance limits.

REACTIVE CYANIDE

Samples 460-58470-3, 460-58470-6, 460-58470-9, 460-58470-12, 460-58470-15, 460-58470-18 and 460-58470-19 were analyzed for reactive cyanide in accordance with EPA SW-846 Method 7.3.3/9014. The samples were prepared and analyzed on 06/27/2013.

No difficulties were encountered during the reactive cyanide analyses.

All quality control parameters were within the acceptance limits.

REACTIVE SULFIDE

Samples 460-58470-3, 460-58470-6, 460-58470-9, 460-58470-12, 460-58470-15, 460-58470-18 and 460-58470-19 were analyzed for reactive sulfide in accordance with EPA SW-846 Method 7.3.4/9034. The samples were prepared and analyzed on 06/27/2013.

No difficulties were encountered during the reactive sulfide analyses.

All quality control parameters were within the acceptance limits.

CORROSIVITY (PH)

Samples 460-58470-3, 460-58470-6, 460-58470-9, 460-58470-12, 460-58470-15, 460-58470-18 and 460-58470-19 were analyzed for corrosivity (pH) in accordance with EPA SW-846 Method 9045C. The samples were analyzed on 06/27/2013.

This analysis is normally performed in the field and has a method-defined holding time of 15 minutes. The following sample(s) has been qualified with the "HF" flag to indicate analysis was performed in the laboratory outside the 15 minute timeframe: REP062413

(460-58470-19), SB-1 (0-10') (460-58470-3), SB-2 (0-7') (460-58470-6), SB-3 (0-8') (460-58470-9), SB-4 (0-10') (460-58470-12), SB-5

(0-10') (460-58470-15), SB-6 (0-10) (460-58470-18)

No difficulties were encountered during the corrosivity (pH) analyses.

All quality control parameters were within the acceptance limits.

PERCENT SOLIDS/PERCENT MOISTURE

Samples 460-58470-1 through 460-58470-19 were analyzed for percent solids/percent moisture in accordance with EPA Method

CLPISM01.2 (Exhibit D). The samples were analyzed on 06/26/2013.

No difficulties were encountered during the %solids/moisture analyses.

All quality control parameters were within the acceptance limits.

07/10/2013Page 6 of 289

EXECUTIVE SUMMARY - Detections

Client: STV Incorporated Job Number: 460-58470-1

Analyte Result

Reporting

Limit Units Method

Lab Sample ID Client Sample ID

Qualifier

460-58470-1 SB-1A (1-3')

10 ug/Kg 8260B110Acetone

1.0 ug/Kg 8260B2.3Carbon disulfide

10 ug/Kg 8260B342-Butanone

1800 ug/Kg 8270C400 JNaphthalene

1800 ug/Kg 8270C1700 JAcenaphthene

1800 ug/Kg 8270C730 JDibenzofuran

1800 ug/Kg 8270C1300 JFluorene

1800 ug/Kg 8270C20000Fluoranthene

1800 ug/Kg 8270C3500Anthracene

1800 ug/Kg 8270C1800Carbazole

1800 ug/Kg 8270C14000Phenanthrene

1800 ug/Kg 8270C15000Pyrene

1800 ug/Kg 8270C8200Chrysene

180 ug/Kg 8270C4300Benzo[k]fluoranthene

1800 ug/Kg 8270C4800Benzo[g,h,i]perylene

180 ug/Kg 8270C8900Benzo[b]fluoranthene

180 ug/Kg 8270C7700Benzo[a]pyrene

180 ug/Kg 8270C7500Benzo[a]anthracene

180 ug/Kg 8270C4100Indeno[1,2,3-cd]pyrene

180 ug/Kg 8270C940Dibenz(a,h)anthracene

1.0 mg/Kg 6010B2.3Arsenic

40.4 mg/Kg 6010B126Barium

2.0 mg/Kg 6010B11.1Chromium

1.0 mg/Kg 6010B19.8Lead

0.017 mg/Kg 7471A0.054Mercury

1.0 % Moisture5.7Percent Moisture

1.0 % Moisture94.3Percent Solids

TestAmerica Edison 07/10/2013Page 7 of 289

Analyte Result

Reporting

Limit Units Method

Lab Sample ID Client Sample ID

Qualifier

460-58470-2 SB-1B (8-10')

11 ug/Kg 8260B24Acetone

1.1 ug/Kg 8260B0.36 JCarbon disulfide

11 ug/Kg 8260B3.7 J2-Butanone

1.1 ug/Kg 8260B1.7Cyclohexane

1.1 ug/Kg 8260B2.9Methylcyclohexane

1800 ug/Kg 8270C800 JNaphthalene

1800 ug/Kg 8270C320 J2-Methylnaphthalene

1800 ug/Kg 8270C3100Acenaphthene

1800 ug/Kg 8270C1300 JDibenzofuran

1800 ug/Kg 8270C2000Fluorene

1800 ug/Kg 8270C26000Fluoranthene

1800 ug/Kg 8270C4800Anthracene

1800 ug/Kg 8270C2700Carbazole

1800 ug/Kg 8270C22000Phenanthrene

1800 ug/Kg 8270C22000Pyrene

1800 ug/Kg 8270C13000Chrysene

180 ug/Kg 8270C6600Benzo[k]fluoranthene

1800 ug/Kg 8270C7800Benzo[g,h,i]perylene

180 ug/Kg 8270C15000Benzo[b]fluoranthene

180 ug/Kg 8270C12000Benzo[a]pyrene

180 ug/Kg 8270C13000Benzo[a]anthracene

180 ug/Kg 8270C6800Indeno[1,2,3-cd]pyrene

180 ug/Kg 8270C2000Dibenz(a,h)anthracene

0.99 mg/Kg 6010B7.5Arsenic

39.6 mg/Kg 6010B136Barium

2.0 mg/Kg 6010B38.4Chromium

0.99 mg/Kg 6010B21.0Lead

0.018 mg/Kg 7471A0.033Mercury

1.0 % Moisture6.4Percent Moisture

1.0 % Moisture93.6Percent Solids

460-58470-3 SB-1 (0-10')

SU 9045C8.44 HFCorrosivity

1.0 % Moisture5.6Percent Moisture

1.0 % Moisture94.4Percent Solids

TCLP

1000 ug/L 6010B792 JBarium

TestAmerica Edison 07/10/2013Page 8 of 289

Analyte Result

Reporting

Limit Units Method

Lab Sample ID Client Sample ID

Qualifier

460-58470-4 SB-2A (2-4')

9.7 ug/Kg 8260B11Acetone

0.97 ug/Kg 8260B0.37 JCarbon disulfide

9.7 ug/Kg 8260B192-Butanone

720 ug/Kg 8270C84 JPyrene

720 ug/Kg 8270C100 JChrysene

720 ug/Kg 8270C54 JBenzo[g,h,i]perylene

72 ug/Kg 8270C85Benzo[b]fluoranthene

72 ug/Kg 8270C78Benzo[a]pyrene

72 ug/Kg 8270C26 JIndeno[1,2,3-cd]pyrene

72 ug/Kg 8270C18 JDibenz(a,h)anthracene

1.1 mg/Kg 6010B3.6Arsenic

42.6 mg/Kg 6010B95.8Barium

2.1 mg/Kg 6010B14.2Chromium

1.1 mg/Kg 6010B13.4Lead

0.017 mg/Kg 7471A0.017Mercury

1.0 % Moisture7.9Percent Moisture

1.0 % Moisture92.1Percent Solids

460-58470-5 SB-2B (5-7')

8.1 ug/Kg 8260B38Acetone

0.81 ug/Kg 8260B0.36 JCarbon disulfide

8.1 ug/Kg 8260B2.3 J2-Butanone

0.81 ug/Kg 8260B0.47 JCyclohexane

0.81 ug/Kg 8260B0.21 JToluene

0.81 ug/Kg 8260B0.26 JMethylcyclohexane

740 ug/Kg 8270C100 JFluoranthene

740 ug/Kg 8270C86 JPyrene

740 ug/Kg 8270C91 JChrysene

74 ug/Kg 8270C23 JBenzo[k]fluoranthene

74 ug/Kg 8270C89Benzo[b]fluoranthene

74 ug/Kg 8270C68 JBenzo[a]pyrene

74 ug/Kg 8270C23 JIndeno[1,2,3-cd]pyrene

0.97 mg/Kg 6010B3.4Arsenic

38.8 mg/Kg 6010B188Barium

1.9 mg/Kg 6010B19.6Chromium

0.97 mg/Kg 6010B19.1Lead

0.019 mg/Kg 7471A0.15Mercury

1.0 % Moisture10.5Percent Moisture

1.0 % Moisture89.5Percent Solids

TestAmerica Edison 07/10/2013Page 9 of 289

Analyte Result

Reporting

Limit Units Method

Lab Sample ID Client Sample ID

Qualifier

460-58470-6 SB-2 (0-7')

SU 9045C8.18 HFCorrosivity

1.0 % Moisture13.2Percent Moisture

1.0 % Moisture86.8Percent Solids

TCLP

1000 ug/L 6010B1060Barium

TestAmerica Edison 07/10/2013Page 10 of 289

Analyte Result

Reporting

Limit Units Method

Lab Sample ID Client Sample ID

Qualifier

460-58470-7 SB-3A (2-4')

110 ug/Kg 8260B29 JTrichloroethene

110 ug/Kg 8260B120Benzene

110 ug/Kg 8260B37 JTetrachloroethene

110 ug/Kg 8260B900Toluene

110 ug/Kg 8260B78 JEthylbenzene

220 ug/Kg 8260B430m&p-Xylene

110 ug/Kg 8260B200o-Xylene

110 ug/Kg 8260B200Cyclohexane

110 ug/Kg 8260B33001,4-Dichlorobenzene

110 ug/Kg 8260B1301,2-Dichlorobenzene

110 ug/Kg 8260B3401,2,4-Trimethylbenzene

110 ug/Kg 8260B82 J1,3,5-Trimethylbenzene

110 ug/Kg 8260B38 JIsopropylbenzene

110 ug/Kg 8260B110N-Propylbenzene

110 ug/Kg 8260B38 Jp-Isopropyltoluene

110 ug/Kg 8260B32 Jsec-Butylbenzene

110 ug/Kg 8260B97 Jn-Butylbenzene

110 ug/Kg 8260B620Methylcyclohexane

400 ug/Kg 8270C250 JNaphthalene

400 ug/Kg 8270C190 J2-Methylnaphthalene

400 ug/Kg 8270C65 JDibenzofuran

400 ug/Kg 8270C730Fluoranthene

400 ug/Kg 8270C92 JAnthracene

400 ug/Kg 8270C52 JCarbazole

400 ug/Kg 8270C520Phenanthrene

400 ug/Kg 8270C560Pyrene

400 ug/Kg 8270C420Chrysene

40 ug/Kg 8270C160Benzo[k]fluoranthene

400 ug/Kg 8270C140 JBenzo[g,h,i]perylene

40 ug/Kg 8270C520Benzo[b]fluoranthene

40 ug/Kg 8270C350Benzo[a]pyrene

40 ug/Kg 8270C350Benzo[a]anthracene

40 ug/Kg 8270C130Indeno[1,2,3-cd]pyrene

40 ug/Kg 8270C45Dibenz(a,h)anthracene

1.2 mg/Kg 6010B6.3Arsenic

46.2 mg/Kg 6010B157Barium

1.2 mg/Kg 6010B0.71 JCadmium

2.3 mg/Kg 6010B16.2Chromium

1.2 mg/Kg 6010B80.2Lead

0.020 mg/Kg 7471A0.24Mercury

1.0 % Moisture18.3Percent Moisture

1.0 % Moisture81.7Percent Solids

TestAmerica Edison 07/10/2013Page 11 of 289

Analyte Result

Reporting

Limit Units Method

Lab Sample ID Client Sample ID

Qualifier

460-58470-8 SB-3B (5-7')

12 ug/Kg 8260B190Acetone

1.2 ug/Kg 8260B2.1Carbon disulfide

12 ug/Kg 8260B402-Butanone

1.2 ug/Kg 8260B0.36 JBenzene

1.2 ug/Kg 8260B0.58 JChlorobenzene

1.2 ug/Kg 8260B0.79 JCyclohexane

1.2 ug/Kg 8260B0.45 JToluene

1.2 ug/Kg 8260B0.50 J1,2-Dichlorobenzene

1.2 ug/Kg 8260B0.17 J1,4-Dichlorobenzene

1.2 ug/Kg 8260B0.69 JMethylcyclohexane

380 ug/Kg 8270C83 J2-Methylphenol

380 ug/Kg 8270C83 J4-Methylphenol

380 ug/Kg 8270C62 JNaphthalene

380 ug/Kg 8270C49 J2-Methylnaphthalene

380 ug/Kg 8270C120 JAcenaphthene

380 ug/Kg 8270C57 JDibenzofuran

380 ug/Kg 8270C83 JFluorene

380 ug/Kg 8270C1900Fluoranthene

380 ug/Kg 8270C250 JAnthracene

380 ug/Kg 8270C150 JCarbazole

380 ug/Kg 8270C1300Phenanthrene

380 ug/Kg 8270C1600Pyrene

380 ug/Kg 8270C1000Chrysene

38 ug/Kg 8270C460Benzo[k]fluoranthene

380 ug/Kg 8270C660Benzo[g,h,i]perylene

38 ug/Kg 8270C1300Benzo[b]fluoranthene

38 ug/Kg 8270C1100Benzo[a]pyrene

38 ug/Kg 8270C940Benzo[a]anthracene

380 ug/Kg 8270C92 JButyl benzyl phthalate

380 ug/Kg 8270C360 JBis(2-ethylhexyl) phthalate

38 ug/Kg 8270C600Indeno[1,2,3-cd]pyrene

38 ug/Kg 8270C190Dibenz(a,h)anthracene

1.1 mg/Kg 6010B3.9Arsenic

42.3 mg/Kg 6010B181Barium

1.1 mg/Kg 6010B0.66 JCadmium

2.1 mg/Kg 6010B28.3Chromium

1.1 mg/Kg 6010B61.5Lead

2.1 mg/Kg 6010B2.6Silver

0.019 mg/Kg 7471A0.88Mercury

1.0 % Moisture12.5Percent Moisture

1.0 % Moisture87.5Percent Solids

TestAmerica Edison 07/10/2013Page 12 of 289

Analyte Result

Reporting

Limit Units Method

Lab Sample ID Client Sample ID

Qualifier

460-58470-9 SB-3 (0-8')

SU 9045C7.99 HFCorrosivity

1.0 % Moisture13.0Percent Moisture

1.0 % Moisture87.0Percent Solids

TCLP

1000 ug/L 6010B683 JBarium

460-58470-10 SB-4A (6-8')

13 ug/Kg 8260B27Acetone

1.3 ug/Kg 8260B7.1Carbon disulfide

13 ug/Kg 8260B5.0 J2-Butanone

1.3 ug/Kg 8260B0.52 JCyclohexane

1.3 ug/Kg 8260B0.39 JToluene

1.3 ug/Kg 8260B0.15 JMethylcyclohexane

410 ug/Kg 8270C52 JNaphthalene

410 ug/Kg 8270C270 JAcenaphthene

410 ug/Kg 8270C130 JDibenzofuran

410 ug/Kg 8270C300 JFluorene

410 ug/Kg 8270C3800Fluoranthene

410 ug/Kg 8270C890Anthracene

410 ug/Kg 8270C330 JCarbazole

410 ug/Kg 8270C2900Phenanthrene

410 ug/Kg 8270C3100Pyrene

410 ug/Kg 8270C2100Chrysene

41 ug/Kg 8270C820Benzo[k]fluoranthene

410 ug/Kg 8270C870Benzo[g,h,i]perylene

41 ug/Kg 8270C2300Benzo[b]fluoranthene

41 ug/Kg 8270C1800Benzo[a]pyrene

41 ug/Kg 8270C1900Benzo[a]anthracene

41 ug/Kg 8270C810Indeno[1,2,3-cd]pyrene

41 ug/Kg 8270C270Dibenz(a,h)anthracene

1.1 mg/Kg 6010B2.1Arsenic

43.0 mg/Kg 6010B279Barium

2.2 mg/Kg 6010B27.4Chromium

1.1 mg/Kg 6010B25.2Lead

0.019 mg/Kg 7471A0.062Mercury

1.0 % Moisture19.2Percent Moisture

1.0 % Moisture80.8Percent Solids

TestAmerica Edison 07/10/2013Page 13 of 289

Analyte Result

Reporting

Limit Units Method

Lab Sample ID Client Sample ID

Qualifier

460-58470-11 SB-4B (8-10')

0.91 ug/Kg 8260B0.58 JMethylene Chloride

9.1 ug/Kg 8260B340Acetone

0.91 ug/Kg 8260B0.98Carbon disulfide

9.1 ug/Kg 8260B512-Butanone

360 ug/Kg 8270C120 JFluoranthene

360 ug/Kg 8270C110 JPyrene

360 ug/Kg 8270C85 JChrysene

36 ug/Kg 8270C34 JBenzo[k]fluoranthene

360 ug/Kg 8270C41 JBenzo[g,h,i]perylene

36 ug/Kg 8270C110Benzo[b]fluoranthene

36 ug/Kg 8270C53Benzo[a]pyrene

36 ug/Kg 8270C66Benzo[a]anthracene

36 ug/Kg 8270C35 JIndeno[1,2,3-cd]pyrene

36 ug/Kg 8270C11 JDibenz(a,h)anthracene

1.0 mg/Kg 6010B2.3Arsenic

41.6 mg/Kg 6010B501Barium

2.1 mg/Kg 6010B29.9Chromium

1.0 mg/Kg 6010B20.1Lead

0.018 mg/Kg 7471A0.042Mercury

1.0 % Moisture7.6Percent Moisture

1.0 % Moisture92.4Percent Solids

460-58470-12 SB-4 (0-10')

SU 9045C9.29 HFCorrosivity

1.0 % Moisture8.3Percent Moisture

1.0 % Moisture91.7Percent Solids

TCLP

1000 ug/L 6010B1250Barium

25.0 ug/L 6010B97.6Lead

TestAmerica Edison 07/10/2013Page 14 of 289

Analyte Result

Reporting

Limit Units Method

Lab Sample ID Client Sample ID

Qualifier

460-58470-13 SB-5A (2-4')

1.1 ug/Kg 8260B2.5Methylene Chloride

11 ug/Kg 8260B180Acetone

1.1 ug/Kg 8260B0.50 JCarbon disulfide

11 ug/Kg 8260B442-Butanone

2.3 ug/Kg 8260B0.69 Jm&p-Xylene

1.1 ug/Kg 8260B0.56 Jo-Xylene

1.1 ug/Kg 8260B0.49 JCyclohexane

1.1 ug/Kg 8260B0.24 JToluene

1.1 ug/Kg 8260B0.18 JMethylcyclohexane

1.1 ug/Kg 8260B1.61,2,4-Trimethylbenzene

1.1 ug/Kg 8260B0.48 J1,3,5-Trimethylbenzene

740 ug/Kg 8270C190 JNaphthalene

740 ug/Kg 8270C520 J2-Methylnaphthalene

740 ug/Kg 8270C130 JPhenanthrene

740 ug/Kg 8270C160 JChrysene

74 ug/Kg 8270C110Benzo[b]fluoranthene

74 ug/Kg 8270C64 JBenzo[a]pyrene

74 ug/Kg 8270C58 JBenzo[a]anthracene

74 ug/Kg 8270C19 JIndeno[1,2,3-cd]pyrene

1.0 mg/Kg 6010B2.9Arsenic

41.3 mg/Kg 6010B195Barium

2.1 mg/Kg 6010B18.1Chromium

1.0 mg/Kg 6010B18.0Lead

0.019 mg/Kg 7471A0.044Mercury

1.0 % Moisture10.3Percent Moisture

1.0 % Moisture89.7Percent Solids

460-58470-14 SB-5B (7.5-9.5')

1.1 ug/Kg 8260B0.60 JMethylene Chloride

11 ug/Kg 8260B29Acetone

1.1 ug/Kg 8260B0.24 JCarbon disulfide

11 ug/Kg 8260B4.1 J2-Butanone

1.1 ug/Kg 8260B0.19 J1,2,4-Trimethylbenzene

43.7 mg/Kg 6010B550Barium

2.2 mg/Kg 6010B23.4Chromium

1.1 mg/Kg 6010B6.9Lead

1.0 % Moisture8.4Percent Moisture

1.0 % Moisture91.6Percent Solids

TestAmerica Edison 07/10/2013Page 15 of 289

Analyte Result

Reporting

Limit Units Method

Lab Sample ID Client Sample ID

Qualifier

460-58470-15 SB-5 (0-10')

SU 9045C7.63 HFCorrosivity

1.0 % Moisture9.2Percent Moisture

1.0 % Moisture90.8Percent Solids

TCLP

1000 ug/L 6010B1300Barium

25.0 ug/L 6010B36.8Lead

460-58470-16 SB-6A (1-3')

8.4 ug/Kg 8260B140Acetone

0.84 ug/Kg 8260B0.27 JCarbon disulfide

8.4 ug/Kg 8260B112-Butanone

0.84 ug/Kg 8260B0.34 JToluene

0.84 ug/Kg 8260B0.21 JMethylcyclohexane

370 ug/Kg 8270C92 JFluoranthene

370 ug/Kg 8270C90 JPyrene

370 ug/Kg 8270C62 JChrysene

370 ug/Kg 8270C56 JBenzo[g,h,i]perylene

37 ug/Kg 8270C89Benzo[b]fluoranthene

37 ug/Kg 8270C71Benzo[a]pyrene

37 ug/Kg 8270C59Benzo[a]anthracene

37 ug/Kg 8270C41Indeno[1,2,3-cd]pyrene

37 ug/Kg 8270C14 JDibenz(a,h)anthracene

1.0 mg/Kg 6010B2.7Arsenic

41.7 mg/Kg 6010B441Barium

2.1 mg/Kg 6010B25.4Chromium

1.0 mg/Kg 6010B14.2Lead

0.018 mg/Kg 7471A0.028Mercury

1.0 % Moisture10.3Percent Moisture

1.0 % Moisture89.7Percent Solids

TestAmerica Edison 07/10/2013Page 16 of 289

Analyte Result

Reporting

Limit Units Method

Lab Sample ID Client Sample ID

Qualifier

460-58470-17 SB-6B (5.5-7.5)

9.5 ug/Kg 8260B150Acetone

0.95 ug/Kg 8260B0.45 JCarbon disulfide

9.5 ug/Kg 8260B102-Butanone

0.95 ug/Kg 8260B0.90 J1,2,4-Trimethylbenzene

37 ug/Kg 8270C28 JBenzo[b]fluoranthene

37 ug/Kg 8270C17 JBenzo[a]pyrene

37 ug/Kg 8270C11 JIndeno[1,2,3-cd]pyrene

1.1 mg/Kg 6010B4.1Arsenic

43.1 mg/Kg 6010B291Barium

1.1 mg/Kg 6010B0.44 JCadmium

2.2 mg/Kg 6010B21.5Chromium

1.1 mg/Kg 6010B23.6Lead

0.018 mg/Kg 7471A0.19Mercury

1.0 % Moisture11.7Percent Moisture

1.0 % Moisture88.3Percent Solids

460-58470-18 SB-6 (0-10)

SU 9045C7.58 HFCorrosivity

1.0 % Moisture11.5Percent Moisture

1.0 % Moisture88.5Percent Solids

TCLP

1000 ug/L 6010B1210Barium

25.0 ug/L 6010B59.2Lead

TestAmerica Edison 07/10/2013Page 17 of 289

Analyte Result

Reporting

Limit Units Method

Lab Sample ID Client Sample ID

Qualifier

460-58470-19 REP062413

0.97 ug/Kg 8260B0.51 JMethylene Chloride

360 ug/Kg 8270C120 JFluoranthene

360 ug/Kg 8270C68 JPhenanthrene

360 ug/Kg 8270C130 JPyrene

360 ug/Kg 8270C74 JChrysene

36 ug/Kg 8270C39Benzo[k]fluoranthene

360 ug/Kg 8270C54 JBenzo[g,h,i]perylene

36 ug/Kg 8270C89Benzo[b]fluoranthene

36 ug/Kg 8270C75Benzo[a]pyrene

36 ug/Kg 8270C70Benzo[a]anthracene

36 ug/Kg 8270C50Indeno[1,2,3-cd]pyrene

36 ug/Kg 8270C12 JDibenz(a,h)anthracene

1.0 mg/Kg 6010B2.1Arsenic

39.9 mg/Kg 6010B465Barium

2.0 mg/Kg 6010B22.4Chromium

1.0 mg/Kg 6010B11.2Lead

0.018 mg/Kg 7471A0.017 JMercury

SU 9045C7.64 HFCorrosivity

1.0 % Moisture8.0Percent Moisture

1.0 % Moisture92.0Percent Solids

TCLP

1000 ug/L 6010B2080Barium

TestAmerica Edison 07/10/2013Page 18 of 289

METHOD SUMMARY

Preparation MethodMethodLab LocationDescription

Matrix: Solid

Volatile Organic Compounds (GC/MS) TAL EDI SW846 8260B

Closed System Purge and Trap TAL EDI SW846 5035

Semivolatile Organic Compounds (GC/MS) TAL EDI SW846 8270C

Automated Soxhlet Extraction TAL EDI SW846 3541

Organochlorine Pesticides (GC) TAL EDI SW846 8081A

Microwave Extraction TAL EDI SW846 3546

Polychlorinated Biphenyls (PCBs) by Gas Chromatography TAL EDI SW846 8082

Microwave Extraction TAL EDI SW846 3546

Herbicides (GC) TAL EDI SW846 8151A

Extraction (Herbicides) TAL EDI SW846 8151A

Metals (ICP) TAL EDI SW846 6010B

Preparation, Metals TAL EDI SW846 3050B

Metals (ICP) TAL EDI SW846 6010B

TCLP Extraction TAL EDI SW846 1311

Preparation, Total Metals TAL EDI SW846 3010A

Mercury (CVAA) TAL EDI SW846 7470A

TCLP Extraction TAL EDI SW846 1311

Preparation, Mercury TAL EDI SW846 7470A

Mercury (CVAA) TAL EDI SW846 7471A

Preparation, Mercury TAL EDI SW846 7471A

Ignitability, Solids TAL EDI SW846 1030

Cyanide, Reactive TAL EDI SW846 9014

Cyanide, Reactive TAL EDI SW846 7.3.3

Sulfide, Reactive TAL EDI SW846 9034

Sulfide, Reactive TAL EDI SW846 7.3.4 pH TAL EDI SW846 9045C

Percent Moisture TAL EDI EPA Moisture

Lab References:

TAL EDI = TestAmerica Edison

Method References:

EPA = US Environmental Protection Agency

SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.

TestAmerica Edison 07/10/2013Page 19 of 289

METHOD / ANALYST SUMMARY

Method Analyst Analyst ID

Del Polito, Vita VDSW846 8260B

Martinez, Eddie EMSW846 8260B

Asfaw, Abebaye A. AAASW846 8270C

Crocco, Michael MCSW846 8270C

Rana, Vidhi VRSW846 8270C

Manlangit, Ferdie FMSW846 8081A

Kapoor, Sita SKSW846 8082

Patel, Jignesh JPSW846 8082

Kapoor, Sita SKSW846 8151A

Chang, Churn Der CDCSW846 6010B

Sheikh, Razia B RBSSW846 7470A

Sheikh, Razia B RBSSW846 7471A

Hu, Youhao YHSW846 1030

Vu, Huan HVSW846 9014

Vu, Huan HVSW846 9034

Hu, Youhao YHSW846 9045C

Robinson, Ian IREPA Moisture

TestAmerica Edison

07/10/2013Page 20 of 289

SAMPLE SUMMARY

Client Sample IDLab Sample ID Client Matrix Sampled Received

Date/Time Date/Time

460-58470-1 SB-1A (1-3') Solid 06/24/2013 1100 06/25/2013 1530

460-58470-2 SB-1B (8-10') Solid 06/24/2013 1100 06/25/2013 1530

460-58470-3 SB-1 (0-10') Solid 06/24/2013 1115 06/25/2013 1530

460-58470-4 SB-2A (2-4') Solid 06/24/2013 1245 06/25/2013 1530

460-58470-5 SB-2B (5-7') Solid 06/24/2013 1245 06/25/2013 1530

460-58470-6 SB-2 (0-7') Solid 06/24/2013 1300 06/25/2013 1530

460-58470-7 SB-3A (2-4') Solid 06/24/2013 0315 06/25/2013 1530

460-58470-8 SB-3B (5-7') Solid 06/24/2013 1315 06/25/2013 1530

460-58470-9 SB-3 (0-8') Solid 06/24/2013 1320 06/25/2013 1530

460-58470-10 SB-4A (6-8') Solid 06/24/2013 1345 06/25/2013 1530

460-58470-11 SB-4B (8-10') Solid 06/24/2013 1345 06/25/2013 1530

460-58470-12 SB-4 (0-10') Solid 06/24/2013 1400 06/25/2013 1530

460-58470-13 SB-5A (2-4') Solid 06/24/2013 1415 06/25/2013 1530

460-58470-14 SB-5B (7.5-9.5') Solid 06/24/2013 1415 06/25/2013 1530

460-58470-15 SB-5 (0-10') Solid 06/24/2013 1430 06/25/2013 1530

460-58470-16 SB-6A (1-3') Solid 06/24/2013 1500 06/25/2013 1530

460-58470-17 SB-6B (5.5-7.5) Solid 06/24/2013 1500 06/25/2013 1530

460-58470-18 SB-6 (0-10) Solid 06/24/2013 1515 06/25/2013 1530

460-58470-19 REP062413 Solid 06/24/2013 0000 06/25/2013 1530

TestAmerica Edison 07/10/2013Page 21 of 289

SAMPLE RESULTS

TestAmerica Edison

07/10/2013Page 22 of 289

Analytical Data

Client Sample ID:

Lab Sample ID:

SB-1A (1-3')

Client Matrix: % Moisture: 5.7

460-58470-1

Solid

Date Sampled: 06/24/2013 1100

Date Received: 06/25/2013 1530

8260B Volatile Organic Compounds (GC/MS)

Dilution:

06/27/2013 1614

07/04/2013 0507

1.0

8260B

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID:

O75346.D

5.16 g

5 mL

CVOAMS12

Analysis Date:

Prep Date:

Analysis Batch:

Prep Batch:

460-169013

460-168028

Analysis Method:

Prep Method:

Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL

1.0 U 1.00.16Chloromethane

1.0 U 1.00.44Bromomethane

1.0 U 1.00.35Vinyl chloride

1.0 U 1.00.34Chloroethane

1.0 U 1.00.15Methylene Chloride

110 101.7Acetone

2.3 1.00.15Carbon disulfide

1.0 U 1.00.16Trichlorofluoromethane

1.0 U 1.00.201,1-Dichloroethene

1.0 U 1.00.111,1-Dichloroethane

1.0 U 1.00.13trans-1,2-Dichloroethene

1.0 U 1.00.11cis-1,2-Dichloroethene

1.0 U 1.00.25Chloroform

34 100.652-Butanone

1.0 U 1.00.191,2-Dichloroethane

1.0 U 1.00.131,1,1-Trichloroethane

1.0 U 1.00.15Carbon tetrachloride

1.0 U 1.00.15Benzene

1.0 U 1.00.17Bromoform

1.0 U 1.00.29Styrene

2.1 U 2.10.61m&p-Xylene

1.0 U 1.00.20o-Xylene

1.0 U 1.00.17Ethylbenzene

1.0 U 1.00.19Chlorobenzene

1.0 U 1.00.13Cyclohexane

1.0 U 1.00.11Isopropylbenzene

10 U 100.132-Hexanone

1.0 U 1.00.11MTBE

1.0 U 1.00.11Freon TF

1.0 U 1.00.33Methyl acetate

51 U 51131,4-Dioxane

1.0 U 1.00.12Trichloroethene

1.0 U 1.00.14Toluene

1.0 U 1.00.10trans-1,3-Dichloropropene

10 U 100.214-Methyl-2-pentanone

1.0 U 1.00.14cis-1,3-Dichloropropene

1.0 U 1.00.101,2-Dichlorobenzene

1.0 U 1.00.161,3-Dichlorobenzene

1.0 U 1.00.111,4-Dichlorobenzene

1.0 U 1.00.201,2,4-Trichlorobenzene

1.0 U 1.00.161,2,3-Trichlorobenzene

1.0 U 1.00.151,2-Dichloropropane

1.0 U 1.00.10Methylcyclohexane

1.0 U 1.00.12Tetrachloroethene

1.0 U 1.00.451,2-Dibromo-3-Chloropropane

1.0 U 1.00.0931,1,2,2-Tetrachloroethane

TestAmerica Edison 07/10/2013Page 23 of 289

Client Sample ID:

Lab Sample ID:

SB-1A (1-3')

Client Matrix: % Moisture: 5.7

460-58470-1

Solid

Date Sampled: 06/24/2013 1100

Date Received: 06/25/2013 1530

8260B Volatile Organic Compounds (GC/MS)

Dilution:

06/27/2013 1614

07/04/2013 0507

1.0

8260B

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID:

O75346.D

5.16 g

5 mL

CVOAMS12

Analysis Date:

Prep Date:

Analysis Batch:

Prep Batch:

460-169013

460-168028

Analysis Method:

Prep Method:

Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL

1.0 U 1.00.141,1,2-Trichloroethane

1.0 U 1.00.10Dibromochloromethane

1.0 U 1.00.151,2-Dibromoethane

1.0 U 1.00.23Dichlorodifluoromethane

1.0 U 1.00.11Bromochloromethane

1.0 U 1.00.33Bromodichloromethane

1.0 U 1.00.151,2,4-Trimethylbenzene

1.0 U 1.00.121,3,5-Trimethylbenzene

1.0 U 1.00.15N-Propylbenzene

1.0 U 1.00.14p-Isopropyltoluene

1.0 U 1.00.13sec-Butylbenzene

1.0 U 1.00.12tert-Butylbenzene

1.0 U 1.00.082n-Butylbenzene

Surrogate %Rec Acceptance LimitsQualifier

107 70 - 1301,2-Dichloroethane-d4 (Surr)

105 70 - 130Toluene-d8 (Surr)

99 70 - 130Bromofluorobenzene

98 70 - 130Dibromofluoromethane (Surr)

TestAmerica Edison 07/10/2013Page 24 of 289

Client Sample ID:

Lab Sample ID:

SB-1A (1-3')

Client Matrix: % Moisture: 5.7

460-58470-1

Solid

Date Sampled: 06/24/2013 1100

Date Received: 06/25/2013 1530

8260B Volatile Organic Compounds (GC/MS)

Dilution:

06/27/2013 1614

07/04/2013 0507

1.0

8260B

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID:

O75346.D

5.16 g

5 mL

CVOAMS12

Analysis Date:

Prep Date:

Analysis Batch:

Prep Batch:

460-169013

460-168028

Analysis Method:

Prep Method:

Tentatively Identified Compounds

QualifierEst. Result (ug/Kg)RTAnalyteCas Number

0Number TIC's Found:

NoneTentatively Identified Compound

TestAmerica Edison 07/10/2013Page 25 of 289

Client Sample ID:

Lab Sample ID:

SB-1B (8-10')

Client Matrix: % Moisture: 6.4

460-58470-2

Solid

Date Sampled: 06/24/2013 1100

Date Received: 06/25/2013 1530

8260B Volatile Organic Compounds (GC/MS)

Dilution:

06/27/2013 1614

07/04/2013 0532

1.0

8260B

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID:

O75347.D

4.83 g

5 mL

CVOAMS12

Analysis Date:

Prep Date:

Analysis Batch:

Prep Batch:

460-169013

460-168028

Analysis Method:

Prep Method:

Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL

1.1 U 1.10.18Chloromethane

1.1 U 1.10.48Bromomethane

1.1 U 1.10.38Vinyl chloride

1.1 U 1.10.36Chloroethane

1.1 U 1.10.17Methylene Chloride

24 111.9Acetone

0.36 J 1.10.17Carbon disulfide

1.1 U 1.10.18Trichlorofluoromethane

1.1 U 1.10.211,1-Dichloroethene

1.1 U 1.10.121,1-Dichloroethane

1.1 U 1.10.14trans-1,2-Dichloroethene

1.1 U 1.10.12cis-1,2-Dichloroethene

1.1 U 1.10.27Chloroform

3.7 J 110.702-Butanone

1.1 U 1.10.201,2-Dichloroethane

1.1 U 1.10.141,1,1-Trichloroethane

1.1 U 1.10.17Carbon tetrachloride

1.1 U 1.10.17Benzene

1.1 U 1.10.19Bromoform

1.1 U 1.10.31Styrene

2.2 U 2.20.65m&p-Xylene

1.1 U 1.10.21o-Xylene

1.1 U 1.10.19Ethylbenzene

1.1 U 1.10.20Chlorobenzene

1.7 1.10.14Cyclohexane

1.1 U 1.10.12Isopropylbenzene

11 U 110.142-Hexanone

1.1 U 1.10.12MTBE

1.1 U 1.10.12Freon TF

1.1 U 1.10.35Methyl acetate

55 U 55141,4-Dioxane

1.1 U 1.10.13Trichloroethene

1.1 U 1.10.15Toluene

1.1 U 1.10.11trans-1,3-Dichloropropene

11 U 110.224-Methyl-2-pentanone

1.1 U 1.10.15cis-1,3-Dichloropropene

1.1 U 1.10.111,2-Dichlorobenzene

1.1 U 1.10.181,3-Dichlorobenzene

1.1 U 1.10.121,4-Dichlorobenzene

1.1 U 1.10.211,2,4-Trichlorobenzene

1.1 U 1.10.181,2,3-Trichlorobenzene

1.1 U 1.10.171,2-Dichloropropane

2.9 1.10.11Methylcyclohexane

1.1 U 1.10.13Tetrachloroethene

1.1 U 1.10.491,2-Dibromo-3-Chloropropane

1.1 U 1.10.0991,1,2,2-Tetrachloroethane

TestAmerica Edison 07/10/2013Page 26 of 289

Client Sample ID:

Lab Sample ID:

SB-1B (8-10')

Client Matrix: % Moisture: 6.4

460-58470-2

Solid

Date Sampled: 06/24/2013 1100

Date Received: 06/25/2013 1530

8260B Volatile Organic Compounds (GC/MS)

Dilution:

06/27/2013 1614

07/04/2013 0532

1.0

8260B

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID:

O75347.D

4.83 g

5 mL

CVOAMS12

Analysis Date:

Prep Date:

Analysis Batch:

Prep Batch:

460-169013

460-168028

Analysis Method:

Prep Method:

Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL

1.1 U 1.10.151,1,2-Trichloroethane

1.1 U 1.10.11Dibromochloromethane

1.1 U 1.10.171,2-Dibromoethane

1.1 U 1.10.24Dichlorodifluoromethane

1.1 U 1.10.12Bromochloromethane

1.1 U 1.10.35Bromodichloromethane

1.1 U 1.10.171,2,4-Trimethylbenzene

1.1 U 1.10.131,3,5-Trimethylbenzene

1.1 U 1.10.17N-Propylbenzene

1.1 U 1.10.15p-Isopropyltoluene

1.1 U 1.10.14sec-Butylbenzene

1.1 U 1.10.13tert-Butylbenzene

1.1 U 1.10.088n-Butylbenzene

Surrogate %Rec Acceptance LimitsQualifier

103 70 - 1301,2-Dichloroethane-d4 (Surr)

109 70 - 130Toluene-d8 (Surr)

99 70 - 130Bromofluorobenzene

97 70 - 130Dibromofluoromethane (Surr)

TestAmerica Edison 07/10/2013Page 27 of 289

Client Sample ID:

Lab Sample ID:

SB-1B (8-10')

Client Matrix: % Moisture: 6.4

460-58470-2

Solid

Date Sampled: 06/24/2013 1100

Date Received: 06/25/2013 1530

8260B Volatile Organic Compounds (GC/MS)

Dilution:

06/27/2013 1614

07/04/2013 0532

1.0

8260B

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID:

O75347.D

4.83 g

5 mL

CVOAMS12

Analysis Date:

Prep Date:

Analysis Batch:

Prep Batch:

460-169013

460-168028

Analysis Method:

Prep Method:

Tentatively Identified Compounds

QualifierEst. Result (ug/Kg)RTAnalyteCas Number

0Number TIC's Found:

TestAmerica Edison 07/10/2013Page 28 of 289

Client Sample ID:

Lab Sample ID:

SB-2A (2-4')

Client Matrix: % Moisture: 7.9

460-58470-4

Solid

Date Sampled: 06/24/2013 1245

Date Received: 06/25/2013 1530

8260B Volatile Organic Compounds (GC/MS)

Dilution:

06/27/2013 1614

07/06/2013 0354

1.0

8260B

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID:

O75438.D

5.6 g

5 mL

CVOAMS12

Analysis Date:

Prep Date:

Analysis Batch:

Prep Batch:

460-169261

460-168028

Analysis Method:

Prep Method:

Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL

0.97 U 0.970.16Chloromethane

0.97 U 0.970.42Bromomethane

0.97 U 0.970.33Vinyl chloride

0.97 U 0.970.32Chloroethane

0.97 U 0.970.15Methylene Chloride

11 9.71.6Acetone

0.37 J 0.970.15Carbon disulfide

0.97 U 0.970.16Trichlorofluoromethane

0.97 U 0.970.181,1-Dichloroethene

0.97 U 0.970.111,1-Dichloroethane

0.97 U 0.970.13trans-1,2-Dichloroethene

0.97 U 0.970.11cis-1,2-Dichloroethene

0.97 U 0.970.23Chloroform

19 9.70.612-Butanone

0.97 U 0.970.171,2-Dichloroethane

0.97 U 0.970.131,1,1-Trichloroethane

0.97 U 0.970.15Carbon tetrachloride

0.97 U 0.970.15Benzene

0.97 U 0.970.16Bromoform

0.97 U 0.970.27Styrene

1.9 U 1.90.57m&p-Xylene

0.97 U 0.970.18o-Xylene

0.97 U 0.970.16Ethylbenzene

0.97 U 0.970.17Chlorobenzene

0.97 U 0.970.13Cyclohexane

0.97 U 0.970.11Isopropylbenzene

9.7 U 9.70.132-Hexanone

0.97 U 0.970.11MTBE

0.97 U 0.970.11Freon TF

0.97 U 0.970.31Methyl acetate

48 U 48121,4-Dioxane

0.97 U 0.970.12Trichloroethene

0.97 U 0.970.14Toluene

0.97 U 0.970.097trans-1,3-Dichloropropene

9.7 U 9.70.194-Methyl-2-pentanone

0.97 U 0.970.14cis-1,3-Dichloropropene

0.97 U 0.970.0971,2-Dichlorobenzene

0.97 U 0.970.161,3-Dichlorobenzene

0.97 U 0.970.111,4-Dichlorobenzene

0.97 U 0.970.181,2,4-Trichlorobenzene

0.97 U 0.970.161,2,3-Trichlorobenzene

0.97 U 0.970.151,2-Dichloropropane

0.97 U 0.970.097Methylcyclohexane

0.97 U 0.970.12Tetrachloroethene

0.97 U 0.970.431,2-Dibromo-3-Chloropropane

0.97 U 0.970.0871,1,2,2-Tetrachloroethane

TestAmerica Edison 07/10/2013Page 29 of 289

Client Sample ID:

Lab Sample ID:

SB-2A (2-4')

Client Matrix: % Moisture: 7.9

460-58470-4

Solid

Date Sampled: 06/24/2013 1245

Date Received: 06/25/2013 1530

8260B Volatile Organic Compounds (GC/MS)

Dilution:

06/27/2013 1614

07/06/2013 0354

1.0

8260B

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID:

O75438.D

5.6 g

5 mL

CVOAMS12

Analysis Date:

Prep Date:

Analysis Batch:

Prep Batch:

460-169261

460-168028

Analysis Method:

Prep Method:

Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL

0.97 U 0.970.141,1,2-Trichloroethane

0.97 U 0.970.097Dibromochloromethane

0.97 U 0.970.151,2-Dibromoethane

0.97 U 0.970.21Dichlorodifluoromethane

0.97 U 0.970.11Bromochloromethane

0.97 U 0.970.31Bromodichloromethane

0.97 U 0.970.151,2,4-Trimethylbenzene

0.97 U 0.970.121,3,5-Trimethylbenzene

0.97 U 0.970.15N-Propylbenzene

0.97 U 0.970.14p-Isopropyltoluene

0.97 U 0.970.13sec-Butylbenzene

0.97 U 0.970.12tert-Butylbenzene

0.97 U 0.970.078n-Butylbenzene

Surrogate %Rec Acceptance LimitsQualifier

103 70 - 1301,2-Dichloroethane-d4 (Surr)

104 70 - 130Toluene-d8 (Surr)

98 70 - 130Bromofluorobenzene

96 70 - 130Dibromofluoromethane (Surr)

TestAmerica Edison 07/10/2013Page 30 of 289

Client Sample ID:

Lab Sample ID:

SB-2A (2-4')

Client Matrix: % Moisture: 7.9

460-58470-4

Solid

Date Sampled: 06/24/2013 1245

Date Received: 06/25/2013 1530

8260B Volatile Organic Compounds (GC/MS)

Dilution:

06/27/2013 1614

07/06/2013 0354

1.0

8260B

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID:

O75438.D

5.6 g

5 mL

CVOAMS12

Analysis Date:

Prep Date:

Analysis Batch:

Prep Batch:

460-169261

460-168028

Analysis Method:

Prep Method:

Tentatively Identified Compounds

QualifierEst. Result (ug/Kg)RTAnalyteCas Number

0Number TIC's Found:

TestAmerica Edison 07/10/2013Page 31 of 289

Client Sample ID:

Lab Sample ID:

SB-2B (5-7')

Client Matrix: % Moisture: 10.5

460-58470-5

Solid

Date Sampled: 06/24/2013 1245

Date Received: 06/25/2013 1530

8260B Volatile Organic Compounds (GC/MS)

Dilution:

06/27/2013 1614

07/06/2013 0418

1.0

8260B

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID:

O75439.D

6.87 g

5 mL

CVOAMS12

Analysis Date:

Prep Date:

Analysis Batch:

Prep Batch:

460-169261

460-168028

Analysis Method:

Prep Method:

Analyte DryWt…